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Crystallographic data are as follows. General information: all data sets collected with Mo Kα radiation (graphite monochromator, λ, 0.71073 Å) at T= 100(2) K. 2a-1.5(toluene, C54.50H 68CrN6O6Si2Zr, monoclinic, space group Pn, a, 11.239(5) A, b, 22.213(12) A, c, 22.686(11) Å, β, 92.84(1)°, V= 5657(5) Å3, Z= 4, μ= 0.470 mm-1, F000, 2308; θ range 0.9-32.3°; reflections, 143 033 measured, 36479 independent (Rint, 0.0461, 30 388 observed (I > 2σ(I, final R indices (F0 > 4σ(F 0, R(F, 0.0387, Rw(F2, 0.0970; inversion twin, ratio 0.541, 3: C43H56FeN 6O5Si2Zr, monclinic, space group P2 1/n, a, 12.7
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2) = 0.1055.
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42
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73649124637
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References of structures in CSD, Cambridge, Version 5.30, Update 3 (May 20081: containing Cr=C(OR) bonds, 284 examples, from 1.879 to 2.194 A; containing Fe=C bonds, 140 examples, from 1.797 to 2.024 Å; containing Mn=C bonds, 85 examples, from 1.820 to 2.121 Å
-
References of structures in CSD, Cambridge, Version 5.30, Update 3 (May 20081: containing Cr=C(OR) bonds, 284 examples, from 1.879 to 2.194 A; containing Fe=C bonds, 140 examples, from 1.797 to 2.024 Å; containing Mn=C bonds, 85 examples, from 1.820 to 2.121 Å.
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84981963904
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