SCOPUS 정보 검색 플랫폼

Volumn 48, Issue 23, 2009, Pages 10862-10864

Unprecedent isolation of a mixture of conformational and linkage isomers in a thiosemicarbazone cobalt mesocate

(6) Pedrido, Rosa a Romero, María J a González Noya, Ana M a Bermejo, Manuel R a Martínez Calvo, Miguel a Zaragoza, Guillermo b

a UNIVERSITY OF SANTIAGO DE COMPOSTELA (Spain)

b Unidade de Difraccion de Raios X (Spain)

Author keywords

[No Author keywords available]

Indexed keywords

COBALT; LIGAND; ORGANOMETALLIC COMPOUND; THIOSEMICARBAZONE DERIVATIVE;

ARTICLE; CHEMICAL STRUCTURE; CHEMISTRY; CONFORMATION; HYDROGEN BOND; STEREOISOMERISM;

COBALT; HYDROGEN BONDING; LIGANDS; MODELS, MOLECULAR; MOLECULAR CONFORMATION; ORGANOMETALLIC COMPOUNDS; STEREOISOMERISM; THIOSEMICARBAZONES;

EID: 72949107215 PISSN: 00201669 EISSN: None Source Type: Journal
DOI: 10.1021/ic901657z Document Type: Article

Times cited : (9)

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- Co2(La)2)]·CH3CN: (Co2C34H47N13S4, MW, 883.95, crystal dimensions: 0.30 × 0.27 × 0.09 mm3, triclinic, P1, a, 11.6780(2) Å, b, 12.6479(2) Å, c, 14.2948(3) A&ring, α, 86.6190(10)°, β, 84.3870(10)°, γ, 74.3150(10)°, V, 2021.84(6) Å3, Z, 2, μ, 1.071 mm -1, F(000, 920. Radiation γ(Mo Kα, 0.71073 Å, T, 100(2) K, reflns collected/unique 72704/15393 (Rint, 0.0328, R, 0.0455, wR, 0,1092, GOF, 1.075, max/min residual density 0.615/-0.486 e.A-3. All non-hydrogen atoms were anisotropically refined. The hydrogen atoms positions (H26 H36 H66 H86) were located in a difference map and refined isotropically, U isoH, 1.2U
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