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Volumn 8, Issue 7, 2008, Pages 2076-2079

Self-assembly of two novel cadmium(II) complexes: One from tripodal imine-phenol ligand and the other from in situ partial degradation of dipolar imine-phenol ligand

(7) Zhou, Xiu Xia a Cai, Yue Peng a Zhu, Shi Zheng b Zhan, Qing Guang a Liu, Mao Sheng a Zhou, Zheng Yuan a Chen, Li a

a SOUTH CHINA NORMAL UNIVERSITY (China)

b SHANGHAI INSTITUTE OF ORGANIC CHEMISTRY (China)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 57849153121 PISSN: 15287483 EISSN: 15287505 Source Type: Journal
DOI: 10.1021/cg8002228 Document Type: Article

Times cited : (64)

References (36)

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- Preparation of Cd3L12 (1, An ammount of 231 mg (0.75 mmol) of Cd(NO2)-4H2O and 140 mg (0.50 mmol) of H3L1 were added to 15 mL of methanol, and the mixture was stirred for 30 min at room temperature. After filtration, the filtrate was kept at room temperature for several days to give colorless crystals upon slow evaporation of the solvent. The crystals were filtered and dried in air. Yield: 28, based on Cd, Anal. Calcd for C54H 54Cd3N8O6: C, 51.89; H, 4.48; N, 8.87. Found: C, 51.91; H, 4.33; N, 8.98. IR (KBr, cm-1, v 2969-2846 (m, 1630 (s, 1534 (m, 1465(m, 1446(w, 1411(s, 1325(w, 1261(w, 1220(m, 1099(s, 1003(m, 927(m, 809(s, 733(m, 622(s, 575(w, 469(w, b) Compound 2 was obtained using the same reaction procedure as described in compound 1 taking H2L2 in place of H3L 1
- -1): v 3411(br,s), 2923(w), 1634(m), 1567(s),1470(w), 1411(w), 1385(w), 1343(w), 1110(w), 1020(w), 927(w), 653(m).

27
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- Crystal data for 1: C54H54N8O 6Cd3, MW, 1248.25, rhombohedral, R3̄, a, 13.15130(10) Å, c, 05.8357(5) Å, V= 3869.80(9) Å3, Z, 3, F(000, 1878, GOF, 1.015, R1, 0.0297, wR2, 0.0631 [I > 2σ(I, For 2: C13H 21N3O7Cd, MW, 443.73, monoclinic, C2/c, a, 20.903(4) Åb, 20.726(3) Å, c, 8.3230(14) Å, β, 104.681(8)°, V, 3488.1(10) Å3, Z, 8, F(000, 1792, GOF, 1.022, R1, 0.0239, wR2, 0.0592 [I > 2σ(I, CCDC-653375 (1) and 657168 (2) contain the supplementary crystallographic data for this paper
- 3, Z = 8, F(000) = 1792, GOF = 1.022, R1 = 0.0239, wR2 = 0.0592 [I > 2σ(I)]. CCDC-653375 (1) and 657168 (2) contain the supplementary crystallographic data for this paper.

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