High-efficiency hydrophilic interaction chromatography by coupling 25 cm × 4.6 mm ID × 5 μm silica columns and operation at 80 °C

Journal of Chromatography A

Volumn 1217, Issue 4, 2010, Pages 514-521

  Louw, Stefan ^a   Lynen, Frédéric ^a   Hanna Brown, Melissa ^b   Sandra, Pat ^a  

^a GHENT UNIVERSITY   (Belgium)

^b PFIZER GLOBAL RESEARCH AND DEVELOPMENT   (United Kingdom)

Author keywords

High efficiency; Hydrophilic interaction chromatography; Kinetic plots; Speed; Temperature

Indexed keywords

COLUMN LENGTHS; COLUMN TEMPERATURE; EXPERIMENTAL DATA; GENOTOXIC; HIGH EFFICIENCY; HYDROPHILIC INTERACTION CHROMATOGRAPHY; KINETIC PLOTS; LONG COLUMN; PHARMACEUTICAL INDUSTRY; PRESSURE SYSTEM; REVERSED-PHASE LIQUID CHROMATOGRAPHY; SEPARATION EFFICIENCY; SILICA COLUMN; SILICA PARTICLES; TEST MIXTURES; THEORETICAL PLATES;

CHROMATOGRAPHIC ANALYSIS; DRUG PRODUCTS; DRUG PRODUCTS PLANTS; FLUORINE CONTAINING POLYMERS; FUNCTIONAL GROUPS; HYDROPHILICITY; SILICA; SPEED;

LIQUID CHROMATOGRAPHY;

ADENINE; BENZODIAZEPINE; KETOPROFEN; SILICON DIOXIDE; TOXIC SUBSTANCE;

ANALYTICAL PARAMETERS; ARTICLE; COLUMN CHROMATOGRAPHY; CONTROLLED STUDY; FLOW RATE; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; HIGH TEMPERATURE PROCEDURES; HYDROPHILIC INTERACTION CHROMATOGRAPHY; INTERMETHOD COMPARISON; IONIZATION; KINETIC PLOT; LOW TEMPERATURE PROCEDURES; PLOTS AND CURVES; PRIORITY JOURNAL; SEPARATION TECHNIQUE; VELOCITY;

CHROMATOGRAPHY; HOT TEMPERATURE; MUTAGENS; PHARMACEUTICAL PREPARATIONS; SILICON DIOXIDE; WATER;

EID: 72949092320     PISSN: 00219673     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.chroma.2009.11.078     Document Type: Article

References (43)

1. MacNair J.E., Lewis K.C., and Jorgenson J.W. Anal. Chem. 69 (1997) 983
2. Wu N.J., Lippert J.A., and Lee M.L. J. Chromatogr. A 911 (2001) 1
3. de Villiers A., Lestremau F., Szucs R., Gelebart S., David F., and Sandra P. J. Chromatogr. A 1127 (2006) 60
4. Trones R., Iveland A., and Greibrokk T. J. Microcol. Sep. 7 (1995) 505
5. Lestremau F., Cooper A., Szucs R., David F., and Sandra P. J. Chromatogr. A 1109 (2006) 191
6. Donato P., Dugo P., Cacciola F., Dugo G., and Mondello L. J. Sep. Sci. 32 (2009) 1129
7. Heinisch S., Desmet G., Clicq D., and Rocca J.L. J. Chromatogr. A 1203 (2008) 124
8. Grata E., Guillarme D., Glauser G., Boccard J., Carrupt P.A., Veuthey J.L., Rudaz S., and Wolfender J.L. J. Chromatogr. A 1216 (2009) 5660
9. Wang X.D., Li W.Y., and Rasmussen H.T. J. Chromatogr. A 1083 (2005) 58
10. Gilar M., Olivova P., Daly A.E., and Gebler J.C. Anal. Chem. 77 (2005) 6426
11. Cubbon S., Bradbury T., Wilson J., and Thomas-Oates J. Anal. Chem. 79 (2007) 8911
12. Mihailova A., Malerod H., Wilson S.R., Karaszewski B., Hauser R., Lundanes E., and Greibrokk T. J. Sep. Sci. 31 (2008) 459
13. Louw S., Pereira A.S., Lynen F., Hanna-Brown M., and Sandra P. J. Chromatogr. A 1208 (2008) 90
14. Alpert A.J. J. Chromatogr. 499 (1990) 177
15. Hemström P., and Irgum K. J. Sep. Sci. 29 (2006) 1784
16. D.V. McCalley, LC-GC N. Am., April 2008, http://chromatographyonline.findanalytichem.com/lcgc/Articles/Hydrophilic-Interaction-Chromatography/ArticleStandard/Article/detail/512613.
17. Ikegami T., Tomomatsu K., Takubo H., Horie K., and Tanaka N. J. Chromatogr. A 1184 (2008) 474
18. Hao Z., Xiao B., and Weng N. J. Sep. Sci. 31 (2008) 1449
19. McCalley D.V. J. Chromatogr. A 1193 (2008) 85
20. Cabooter D., Lestremau F., Lynen F., Sandra P., and Desmet G. J. Chromatogr. A 1212 (2008) 23
21. Guillarme D., Nguyen D.T.T., Rudaz S., and Veuthey J.-L. J. Chromatogr. A 1149 (2007) 20
22. Heinisch S., and Rocca J.L. J. Chromatogr. A 1216 (2009) 642
23. Vanhoenacker G., and Sandra P. J. Sep. Sci. 29 (2006) 1822
24. Vanhoenacker G., and Sandra P. Anal. Bioanal. Chem. 390 (2008) 245
25. Dolan J.W. J. Chromatogr. A 965 (2002) 195
26. Lestremau F., de Villiers A., Lynen F., Cooper A., Szucs R., and Sandra P. J. Chromatogr. A 1138 (2007) 120
27. McNeff C.V., Yan B., Stoll D.R., and Henry R.A. J. Sep. Sci. 30 (2007) 1672
28. Sandra P., and Vanhoenacker G. J. Sep. Sci. 30 (2007) 241
29. In: Pesek J. (Ed). J. Sep. Sci. 30 (2007) 1099
30. Sandra K., Verleysen K., Labeur C., Vanneste L., D'Hondt F., Thomas G., Kas K., Gevaert K., Vandekerckhove J., and Sandra P. J. Sep. Sci. 30 (2007) 658
31. S. Louw, A.S. Pereira, F. Lynen, M. Hanna-Brown, P. Sandra, J. Chromatogr. A, in preparation.
32. Poppe H. J. Chromatogr. A 778 (1997) 3
33. Desmet G., Clicq D., and Gzil P. Anal. Chem. 77 (2005) 4058
34. Desmet G., Gzil P., and Clicq D. LC-GC Eur. 18 (2005) 403
35. Cabooter D., Heinisch S., Rocca J.L., Clicq D., and Desmet G. J. Chromatogr. A 1143 (2007) 121
36. Desmet G. LC-GC Eur. 21 (2008) 310
37. Cabooter D., Lestremau F., de Villiers A., Broeckhoven K., Lynen F., Sandra P., and Desmet G. J. Chromatogr. A 1216 (2009) 3895
38. Chen H., and Horvath C. Anal. Methods Instrum. 1 (1993) 213
39. Li J.W., and Carr P.W. Anal. Chem. 69 (1997) 2530
40. Liu M., Chen E.X., Ji R., and Semin D. J. Chromatogr. A 1188 (2008) 255
41. Guo Y., and Gaiki S. J. Chromatogr. A 1074 (2005) 71
42. de Villiers A., Lynen F., and Sandra P. J. Chromatogr. A 1216 (2009) 3431
43. Dobo K.L., Greene N., Cyr M.O., Caron S., and Ku W.W. Regul. Toxicol. Pharmacol. 44 (2006) 282