Precise determination of glucose-d2/glucose ratio in human serum and plasma by APCI LC-MS/MS

Scandinavian Journal of Clinical and Laboratory Investigation

Volumn 69, Issue 8, 2009, Pages 837-842

  Ullah, Shahid ^a   Wahren, John ^a   Beck, Olof ^a  

^a KAROLINSKA INSTITUTE   (Sweden)

Author keywords

Deuterium glucose; Glucose; Glucose turnover; Human serum; Liquid chromatography mass spectrometry

Indexed keywords

6,6 D 2 GLUCOSE; ACETONITRILE; AMMONIUM ACETATE; DEUTERIUM; GLUCOSE; GLUCOSE DERIVATIVE; ION; UNCLASSIFIED DRUG; WATER;

ARTICLE; ATMOSPHERIC PRESSURE; CHROMATOGRAPHY; CONTROLLED STUDY; FLOW RATE; GLUCONEOGENESIS; GLUCOSE ASSAY; GLUCOSE BLOOD LEVEL; HUMAN; LIQUID CHROMATOGRAPHY; MASS SPECTROMETRY; MONITORING; PRECIPITATION; PRIORITY JOURNAL; SUPERNATANT; TANDEM MASS SPECTROMETRY; TEMPERATURE; TURNOVER TIME;

ATMOSPHERIC PRESSURE; BLOOD GLUCOSE; CHROMATOGRAPHY, LIQUID; DEUTERIUM; FREEZING; HUMANS; MALE; MASS SPECTROMETRY; QUALITY CONTROL; REPRODUCIBILITY OF RESULTS; SOLUTIONS; YOUNG ADULT;

EID: 72749094284     PISSN: 00365513     EISSN: 15027686     Source Type: Journal    
DOI: 10.3109/00365510903307954     Document Type: Article

References (19)

1. Magni F, Paroni R, Bonini PA, Kienle MG. Determination of serum glucose by isotope dilution mass spectrometry: Candidate defi nitive method. Clin Chem 1992;38: 381-385
2. Hannestad U, Lundblad A. Accurate and precise isotope dilution mass spectrometry method for determining glucose in whole blood. Clin Chem 1997;43:794-800.
3. Vester HW, Archibald E, Myers GL. Assessment of trueness of glucose measurement instrument with different specimen matrices. Clin Chim Acta 2005;358:68-74.
4. Svanfeldt M, Thorell A, Hausel J, Soop M, Rooyakers O, Nygren J, Ljungqvist O. Randomized clinical trial of the effect of preoperative oral carbohydrate treatment on postoperative whole-body protein and glucose kinetics. Br J Surg 2007;94:1342-1350
5. Kury D, Keller U. Trimethylsilyl-O-methyloxime derivatives for the measurement of (6,6- 2H2)-D-glucose-enriched plasma samples by gas chromatography-mass spectrometry. J Chromatogr 1991;572:302-306
6. McIntosh TS, Davis HM, Matthews DE. Aliquid chromatography-mass spectrometry method to measure stable isotope tracer enrichments of glycerol and glucose in human serum. Anal Biochem 2002;300:163-169
7. + attachment. Am Soc Mass Spectrom 2005;16:1805-1811
8. Dube G, Henrion A, Ohlendorf R, Vidal C. Application of the combination of isotope ratio monitoring with isotope dilution mass spectrometry to the determination of glucose in serum. Rapid Commun Mass Spectrom 2001;15: 1322-1326
9. Bruggink C, Maurer R, Herrmann H, Cavalli S, Hoefl er F. Analysis of carbohydrates by anion exchange chromatography and mass spectrometry. J Chromatogr A 2005;1085:104-109
10. Guignard C, Jouve L, Bogeat-Triboulot MB, Dreyer E, Hausman JF, Hoffmann L. Analysis of carbohydrates in plants by high-performance anion exchange chromatography coupled with electrospray mass spectrometry. J Chromatogr A 2005;1085:137-142
11. Christopher RT, Justin TB, Sanford AA, Joseph JG, David NF. Analysis of tear glucose concentration with electrospray ionization mass spectrometry. Am Soc Mass Spectrom 2007;18:332-336
12. Wan ECH, Yu JZ. Determination of sugar compounds in atmospheric aerosols by liquid chromatography combined with positive electrospray ionization mass spectrometry. J Chromatogr A 2006;1107:175-181
13. Liang HR, Takagaki T, Foltz RL, Bennett P. Quantitative determination of endogenous sorbitol and fructose in human erythrocytes by atmospheric pressure chemical ionization LC-MS/MS. J Chromatogr B 2005;824:36-44.
14. Zhu J, Cole RB. Ranking of gas-phase acidities and chloride affi nities of monosaccharides and linkage specifi city in collision induced decompositions of negative ion electrospraygenerated chloride adducts of oligosaccharides. Am Soc Mass Spectrom 2001;12:1193-1204
15. Wan EC, Yu JZ. Analysis of sugars and sugar polyols in atmospheric aerosols by chloride attachments in liquid chromatography/negative ion electrospray mass spectrometry. Environ Sci Technol 2007;41:2459-2466
16. Rogatsky E, Tomuta V, Daniel S. LC/MS quantitative study of glucose by iodine attachment. Anal Chim Acta 2007; 591:155-160
17. Burrin JM, Price CP. Measurement of blood glucose. Ann Clin Biochem 1985;22:327-342
18. Finegood DT, Bergman RN, Vranic M. Modeling error and apparent isotope discrimination confound estimation of endogenous glucose production during euglycemic glucose clamps. Diabetes 1988;37:1025-1034
19. Bossolan G, Trinidade CEP, Barreiros RC. Blood galactose and glucose levels in mothers, cord blood, and 48-hourold breast-fed full-term infants. Neonatology 2007;91: 121-126