Sensitive LC MS quantitative analysis of carbohydrates by Cs+ attachment

Journal of the American Society for Mass Spectrometry

Volumn 16, Issue 11, 2005, Pages 1805-1811

  Rogatsky, Eduard ^a   Jayatillake, Harsha ^a   Goswami, Gayotri ^a   Tomuta, Vlad ^a   Stein, Daniel ^a  

^a ALBERT EINSTEIN COLLEGE OF MEDICINE   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

BIOASSAY; CESIUM COMPOUNDS; CHEMICAL ANALYSIS; IONIZATION; ISOTOPES; LIQUID CHROMATOGRAPHY; MASS SPECTROMETRY; MEDICAL APPLICATIONS; PLASMAS; SEPARATION;

ELECTROSPRAY IONIZATION; HUMAN PLASMAS; ISOTOPE DILUTION ASSAY; QUASI-MOLECULAR IONS;

CARBOHYDRATES;

AMINO ACID; CARBOHYDRATE; CESIUM; ISOTOPE;

ADDITION REACTION; ARTICLE; CARBOHYDRATE ANALYSIS; DILUTION; ELECTROSPRAY MASS SPECTROMETRY; HUMAN; LIQUID CHROMATOGRAPHY; MASS SPECTROMETRY; MOLECULAR WEIGHT; PLASMA; QUANTITATIVE ANALYSIS; SENSITIVITY ANALYSIS;

BLOOD CHEMICAL ANALYSIS; CARBOHYDRATES; CESIUM; CHROMATOGRAPHY, LIQUID; HUMANS; MICROCHEMISTRY; SPECTROMETRY, MASS, ELECTROSPRAY IONIZATION; STAINING AND LABELING;

EID: 26944455186     PISSN: 10440305     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.jasms.2005.07.017     Document Type: Article

References (34)

1. K.-Y. Tserng, S.C. Kalhan Estimation of glucose carbon recycling and glucose turnover with [U-13C] glucose Am. J. Physiol 245 1983 E476 E482
2. R.R. Wolfe Radioactive and stable isotope tracers in biomedicine Principles and practice of kinetic analysis 1992 Wiley-Liss New York 424 426
3. M. Beylot, C. Martin, B. Beaufrere, J.P. Riou, R. Mornex Determination of steady state and nonsteady state glycerol kinetics in humans using deuterium-labeled tracer J. Lipid Res 28 1987 414 422
4. N.V. Esteban, D.J. Liberato, J.B. Sidbury, A.L. Yergey Stable isotope dilution thermospray liquid chromatography/mass spectrometry method for determination of sugars and sugar alcohols in humans Anal. Chem 59 1987 1674 1677
5. S. Reid, C. Shackleton, K. Wu, S. Kaempfer, M.K. Hellerstein Liquid chromatography/mass spectrometry of plasma glucose and secreted glucuronate for metabolic studies in humans Biomed. Environ. Mass Spectrom 19 1990 535 540
6. A. Takatsu, S. Nishi Stable isotope dilution method for the determination of serum glucose using discharge-assisted thermospray liquid chromatography/mass spectrometry Biol. Mass Spectrom 20 1991 415 418
7. F. Magni, L. Arnoldi, L. Monti, P. Piatti, G. Pozza, K.M. Galli Determination of plasma glycerol isotopic enrichment by gas chromatography-mass spectrometry An alternative glycerol derivative Anal. Biochem 211 1993 327 328
8. C.D. Gilker, G.R. Pesola, D.E. Matthews A mass spectrometric method for measuring glycerol levels and enrichments in plasma using 13C and 2H stable isotopic tracers Anal. Biochem 205 1992 172 178
9. M.T. Ackermans, A.F. Ruiter, E. Endert Determination of glycerol concentrations and glycerol isotopic enrichments in human plasma by gas chromatography/mass spectrometry Anal. Biochem 258 1998 80 86
10. P.J. Flakoll, M. Zheng, S. Vaughan, M.J. Borel Determination of stable isotopic enrichment and concentration of glycerol in plasma via gas chromatography-mass spectrometry for the estimation of lipolysis in vivo J. Chromatogr. B 744 2000 47 54
11. T.S. McIntosh, H.M. Davis, D.E. Matthews A liquid chromatography-mass spectrometry method to measure stable isotopic tracer enrichments of glycerol and glucose in human serum Anal. Biochem 300 2002 163 169
12. R.C. Schoemaker, J. Burggraaf, A.F. Cohen Assessment of hepatic blood flow using continuous infusion of high clearance drugs Br. J. Clin. Pharmacol 45 2000 463 469
13. D.E. Matthews, D.M. Bier Stable isotope methods for nutritional investigation Annu. Rev. Nutr 3 1983 309 339
14. S.C. Kalhan Stable isotope tracers for studies of glucose metabolism J. Lab. Clin. Med 116 1990 615 622
15. K.Y. Tserng, S.C. Kalhan Estimation of glucose carbon recycling and glucose turnover with [U-13C] glucose Am. J. Physiol 245 1983 E76 E82
16. M. Tetsuo, C. Zhang, H. Matsumoto, I. Matsumoto Gas chromatographic-mass spectrometric analysis of urinary sugar and sugar alcohols during pregnancy J. Chromatogr. B 731 1999 111 120
17. Y. Kato, Y. Numajiri Chloride attachment negative-ion mass spectra of sugars by combined liquid chromatography and atmospheric pressure chemical ionization mass spectrometry J. Chromatogr 562 1991 81 97
18. H.P. Tannenbaum, J.D. Roberts, R.C. Dougherty Negative chemical ionization mass spectrometry - chloride attachment spectra Anal. Chem 47 1975 49 54
19. H. Kumaguai Application of liquid chromatography/mass spectrometry to the analysis of sugars and sugar-alcohol Agilent Technologies 2001 Application Note no. 5988-4236EN, 10/2001
20. P.O. Staneke, G. Groothuis, S. Ingemann, N.M.M. Nibbering Formation, stability, and structure of radical anions of chloroform, tetrachloromethane, and fluorotrichloromethane in the gas phase Int. J. Mass Spectrom. Ion Processes 142 1995 83 93
21. M. Kusakavitch Investigation of discoloration of chloroform solution 2004 Poster 370 at the Eastern Analytical Symposium Somerset, NJ November
22. H. Liang, R. Foltz, P. Bennett Sensitive and selective LC/MS/MS method for determination of endogenous polyols in human nerve tissues 2004 Poster ThPK 220 at the 52nd Conference of American Society of Mass Spectrometry Nashville, TN June
23. J. Zhu, R. Cole Ranking of gas-phase acidities and chloride affinities of monosaccharides and linkage specificity in collision-induced decompositions of negative ion electrospray-generated chloride adducts of oligosaccharides J. Am. Soc. Mass Spectrom 112 2001 1193 1204
24. A. Antonopoulos, P. Bonnet, E. Botek, J.L. Debrun, B. Hakim, B. Herbreteau, L. Morin-Allory Study of the attachment of Na+ on glucose and on some of its methylated derivatives Rapid Commun. Mass Spectrom 17 2003 122 125
25. E. Botek, J.L. Debrun, B. Hakim, L. Morin-Alory Attachment of alkali cations on β-D-glucopyranose Matrix-assisted laser desorption/ionization time of flight studies and ab initio calculations Rapid Commun. Mass Spectrom 15 2001 273 276
26. L.C. Ngoka, J.-F. Gal, C.B. Lebrilla Effects of cations and charge types on the meta-stable decay rates of oligosaccharides Anal. Chem 66 1994 692 698
27. M. Kohler, J. Leary LC/MS/MS of carbohydrates with postcolumn addition of metal chlorides using triaxial electrospray probe Anal. Chem 67 1995 3501 3508
28. E. Rogatsky, D.T. Stein A novel, highly robust method of carbohydrate prepurification by 2D LC prior to LC/MS or GC/MS J. Chromatogr. A 1073 2005 11 16
29. C.S. Young, J.W. Dolan Success with evaporative light scattering detection, Part II Tips and techniques LC/GC North Am 22 2004 244 250
30. A. Schoor, N. Erdmann, U. Effmert, S. Mikkat Determination of the cyanobacterial osmolyte glucosylglycerol by high-performance liquid chromatography J. Chromatogr. A 704 1995 89 97
31. K. Tseng, L.L. Lindsay, S. Penn, J.L. Hedrick, C.B. Lebrilla Characterization of neutral oligosaccharide-alditols from Xenopus laevis egg jelly coats by matrix-assisted laser desorption Fourier transform mass spectrometry Anal. Biochem 250 1997 18 28
32. J.W. Hager Recent trends in mass spectrometer development Anal. Bioanal. Chem 378 2004 845 850
33. C. Bruggink, R. Maurer, H. Herrmann, S. Cavalli, F. Hoefler Analysis of carbohydrates by anion exchange chromatography and mass spectrometry J. Chromatogr. A 1085 2005 104 109
34. C. Guignard, L. Jouve, M.B. Bogeat-Triboulot, E. Dreyer, J.-F. Hausman, L. Hoffmann Analysis of carbohydrates in plants by high-performance anion-exchange chromatography coupled with electrospray mass spectrometry J. Chromatogr. A 1085 2005 137 142