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-1) for 1: 3123(w), 2103(s), 2077(w), 2051(w), 1509(w), 1418(w), 1290(m), 1162(w), 1065(w), 1000(w).
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31
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72149135088
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note
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-3 lies 0.82 Å from atom Cu(5). Data collections of 1 were performed with Mo Kα radiation (λ = 0.71073 Å) on a Siemens Smart CCD Diffractometer. The structure was solved by direct methods and refined with full-matrix least-squares technique using SHELXL-97 program [46]. All non- hydrogen atoms were refined anistropically. Positions of the hydrogen atoms attached to carbon atoms were fixed at their ideal positions.
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0004150157
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Program for X-ray Crystal Structure Solution and Refinement, University of Göttingen
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G.M. Sheldrick, SHELXL-97 and SHELXS-97, Program for X-ray Crystal Structure Solution and Refinement, University of Göttingen, 1997.
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