Preparation of a super-long two column chromatography system and its application in separating glycosylated puerarin

Biomedical Chromatography

Volumn 23, Issue 12, 2009, Pages 1344-1349

  Zhu, Shouchuang ^a   Xu, Haidong ^a   Yu, Cigang ^a   Ding, Juanfang ^a   Chen, Ting ^a   Jiang, Jierong ^a   Dai, Yijun ^a   Liu, Guiyou ^a   Huang, Guodong ^a   Chai, Nan ^a   Jiang, Xuhua ^a   Yuan, Sheng ^a  

^a NANJING NORMAL UNIVERSITY   (China)

Author keywords

Column chromatography; Macroporous resins; Number of theoretical plates; Puerarin; Super long two column chromatography system

Indexed keywords

CARBOHYDRATES; REINFORCEMENT; RESINS; WASHING;

ITS APPLICATIONS; LONG COLUMN; MACROPOROUS RESIN; NUMBER OF THEORETICAL PLATE; PUERARIN; RECOVERY RATE; SUPER LONGS; SUPER-LONG TWO-COLUMN CHROMATOGRAPHY SYSTEM; SYSTEM APPLICATIONS; THEORETICAL PLATES;

COLUMN CHROMATOGRAPHY;

ALCOHOL; POLYVINYLCHLORIDE; PUERARIN; PUERARIN 7 O GLUCOSIDE; RESIN; UNCLASSIFIED DRUG; WATER;

ANALYTIC METHOD; ARTICLE; BACTERIUM; COLUMN CHROMATOGRAPHY; CONTROLLED STUDY; DRUG STRUCTURE; ELUTION; EQUIPMENT DESIGN; FERMENTATION; FLOW RATE; MICROBACTERIUM OXYDANS; POROSITY; PROTEIN GLYCOSYLATION; SEPARATION TECHNIQUE; SUPER LONG TWO COLUMN CHROMATOGRAPHY;

EID: 71649110384     PISSN: 02693879     EISSN: 10990801     Source Type: Journal    
DOI: 10.1002/bmc.1259     Document Type: Article

References (22)

1. Cervellati R, Renzulli C, Guerra MC and Speroni E. Evaluation of antioxidant activity of some natural polyphenolic compounds using the Briggs-Rauscher reaction method. Journal of Agriculture and Food Chemistry 2002; 50: 7504. (Pubitemid 35453707)
2. Chen XM and Yang ZL. Purification of flavone and puerarin in kudzuvine root. Strait Pharmaceutical Journal, 2006; 18: 24.
3. Dubois M, Gilles K, Hamilton JK, Rebers PA and Smith F. A colorimetric method for the determination of sugars. Nature 1951; 168: 167.
4. Dubois M, Gilles KA, Hamilton JK, Rebers PA and Smith F. Colorimetric method for determination of sugars and related substances. Analytical Chemistry 1956; 28: 350.
5. Fu BQ, Liu J, Li H, Li L, Lee FSC and Wang XR. The application of macroporous resins in the separation of licorice flavonoids and glycyrrhizic acid. Journal of Chromatography A 2005; 1089: 18. (Pubitemid 41073551)
6. Fu YJ, Zu YG, Liu W, Efferth T, Zhang NJ, Liu XN and Kong Y. Optimization of luteolin separation from pigeonpea [Cajanus cajan (L.) Millsp.] leaves by macroporous resins. Journal of Chromatography A 2006; 1137: 145. (Pubitemid 44828071)
7. Fu YJ, Zu YG, Liu W, Hou CL, Chen LY, Li SM, Shi XG and Tong MH. Preparative separation of vitexin and isovitexin from pigeonpea extracts with macroporous resins. Journal of Chromatography A 2007; 1139: 206. (Pubitemid 44937275)
8. Gao M, Huang W and Liu CZ. Separation of scutellarin from crude extracts of Erigeron breviscapus (vant.) Hand. Mazz. by macroporous resins. Journal of Chromatography B 2007; 858: 22. (Pubitemid 47513591)
9. Hadden N, Baumann F, MacDonald F, Munk M, Stevenson R and Gere D, Zamaroni F and Majos R. Basic Liquid Chromatography. Varian Aerograph: California. 1971.
10. He HB, Shi MQ and Yang J. The correlation between angiogenesis and abnormal expression of SERCA2a, phospholamban and the endothelin pathway in heart failure, and improvement by puerarin. Phytotherapy Research 2008; 22: 948.
11. Jia G and Lu X. Enrichment and purification of madecassoside and asiaticoside from Centella asiatica extracts with macroporous resins. Journal of Chromatography A 2008; doi:10.1016/j.chroma.2008.04.024
12. Jiang JR, Yuan S, Ding JF, Zhu SC, Xu HD, Xu WP, Ye H, Dai YJ and Cong XD. Conversion of puerarin into its 7-O-glycoside derivatives by Microbacterium oxydans (CGMCC 1788) to improve its water solubility and pharmacokinetic properties. Applied Microbiology and Biotechnol 2008; 81: 647-657.
13. Li D, Park SH, Shim JH, Lee HS, Tang SY, Park CS and Park KH. In vitro enzymatic modification of puerarin to puerarin glycosides by maltogenic amylase. Carbohydrate Research 2004; 339: 2789. (Pubitemid 39473221)
14. Liu M and Zhang PY. Research and application of puerarin. Journal of the Practice of Traditional Chinese Medicine 2007; 23: 674.
15. Pan HP and Li G. Protecting mechanism of puerarin on the brain neurocyte of rat in acute local ischemia brain injury and local cerebral ischemia-reperfusion injury. Yakugaku Zasshi - Journal of the Pharmaceutical Society of Japan 2008; 128: 1689
16. Pan J, Chen Q, Xie HM, Zhang J and Wang GX. Character of macroporous resin adsorbing and separating flavone in kudzuvine root. Transactions of the CSAE 1999; 15: 236.
17. Said AS. Theory and Mathematics of Chromatography. Huethig: Heideberg, 1981.
18. Wong R and Rabie B. Effect of puerarin on bone formation. Osteoarthritis and Cartilage 2007; 15: 894.
19. Xu HN and He CH. Separation and purification of puerarin with solvent extraction. Separation and Purification Technology 2007; 56: 397.
20. Yang RL, LI N, Bo X, Geroge C, Chou Y and Min ZD. Preparation and activity of derivated puerarin. Chinese Pharmaceutical University 1999; 30: 81.
21. Ye H, Yuan S and Cong XD. Biotransformation of puerarin into 3-hydroxypuerarin by Trichoderma harzianum, NJ01. Enzyme Microbial Technology 2007; 40: 594. (Pubitemid 46329054)
22. Zhang SY, Chen G and Wei PF. The effect of puerarin on serum nitric oxide concentration and myocardial eNOS expression in rats with myocardial infarction. Journal of Asian Natural Products Research 2008; 10: 323.