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Volumn 175, Issue , 2001, Pages 357-366

Cross-linking of poly(methyl methacrylate) by oxozirconate and oxotitanate clusters

Author keywords

[No Author keywords available]

Indexed keywords

CROSS-LINKED POLYMERS; IMPEDANCE SPECTRUM; INORGANIC-ORGANIC HYBRID POLYMERS; RADICAL POLYMERIZATION; SOLVENT UPTAKE; THERMAL STABILITY;

EID: 70449462013     PISSN: 10221360     EISSN: 15213900     Source Type: Journal    
DOI: 10.1002/1521-3900(200110)175:1<357::AID-MASY357>3.0.CO;2-D     Document Type: Article
Times cited : (27)

References (25)
  • 17
    • 70449504832 scopus 로고    scopus 로고
    • note
    • A typical procedure is as follows: To a solution of 2.62 g (26.2 mmol) methyl methacrylate (filtered over alumina to remove the stabilizer) and 0.91 g (0.54 mmol) of 1 in 6 ml benzene, 21 mg (0.09 mmol) of dibenzoylperoxide were added. When heated to 65 °C, the solution became turbid after 2-3 h and then solidified. Heating was continued for 9-10 h, and then the solvent was removed at 70 °C / 8 mbar. The remaining benzene was extracted with ethyl acetate, and then the solvent was again removed under reduced pressure. The olefin : initiator : solvent ratio was kept constant when the cluster: olefin ratio was varied.


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.