Determination of fluoxetine and norfluoxetine enantiomers in human plasma by polypyrrole-coated capillary in-tube solid-phase microextraction coupled with liquid chromatography-fluorescence detection

Journal of Chromatography A

Volumn 1216, Issue 49, 2009, Pages 8590-8597

  Silva, Bruno José Gonçalves ^a   Lanças, Fernando Mauro ^a   Queiroz, Maria Eugênia Costa ^a  

^a UNIVERSITY OF SÃO PAULO   (Brazil)

Author keywords

Chiral separation; Fluoxetine; In tube solid phase microextraction; Liquid chromatography; Polypyrrole film

Indexed keywords

A-COEFFICIENT; ABSORBANCES; ANALYSIS IN PLASMA; ANALYTES; CHIRAL SEPARATION; CHIRALCEL OD; CHROMATOGRAPHIC METHODS; COATED CAPILLARIES; COATED FILMS; CORRELATION COEFFICIENT; CYCLE NUMBER; DYNAMIC RANGE; EXTRACTION EFFICIENCIES; FLUOXETINE; HEXAFLUOROPHOSPHATES; HIGH PRECISION; HUMAN PLASMAS; IN-TUBE SOLID-PHASE MICROEXTRACTION; IN-TUBE SPME; ISOCRATIC MODES; LIMIT OF QUANTIFICATIONS; LIQUID CHROMATOGRAPHY-FLUORESCENCE DETECTION; MOBILE PHASE; NORFLUOXETINE; PLASMA PROTEIN; PLASMA SAMPLES; POLYPYRROLE FILM; POROUS SURFACE; QUANTIFICATION LIMIT; SAMPLE PH; SODIUM PHOSPHATE; SOLID-PHASE MICROEXTRACTION;

ACETONITRILE; CHIRALITY; CHROMATOGRAPHIC ANALYSIS; CHROMATOGRAPHY; DYNAMIC RESPONSE; ENANTIOMERS; FLUORESCENCE; HIGH PRESSURE LIQUID CHROMATOGRAPHY; LIQUIDS; PLASMAS; POLYPYRROLES; POTASSIUM; SEPARATION; SODIUM; SODIUM COMPOUNDS; SURFACE STRUCTURE; TUBES (COMPONENTS);

SOLVENT EXTRACTION;

ACETONITRILE; ANTIDEPRESSANT AGENT; FLUOROPHOSPHATE; FLUOXETINE; NORFLUOXETINE; POLYPYRROLE; SODIUM DIHYDROGEN PHOSPHATE;

ACCURACY; AGED; ARTICLE; BLOOD ANALYSIS; BLOOD SAMPLING; CLINICAL EFFECTIVENESS; COATED PARTICLE; CONTROLLED STUDY; DEPRESSION; DRUG DETERMINATION; DRUG MONITORING; DRUG STRUCTURE; ENANTIOMER; FLOW RATE; FLUORESCENCE; HUMAN; IN TUBE SOLID PHASE MICROEXTRACTION; INTERMETHOD COMPARISON; PH; PRIORITY JOURNAL; PROCESS DEVELOPMENT; PROCESS OPTIMIZATION; PROTEIN BLOOD LEVEL; QUANTITATIVE ANALYSIS; REPRODUCIBILITY; REVERSED PHASE LIQUID CHROMATOGRAPHY; SENSITIVITY AND SPECIFICITY; SOLID PHASE MICROEXTRACTION; VALIDATION PROCESS;

CHROMATOGRAPHY, LIQUID; FLUOXETINE; HUMANS; POLYMERS; PYRROLES; SOLID PHASE MICROEXTRACTION; SPECTROMETRY, FLUORESCENCE; STEREOISOMERISM;

EID: 70350754641     PISSN: 00219673     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.chroma.2009.10.034     Document Type: Article

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