Preparation and characterization of p-tert-butylcalix[4]arene modified sol-gel column for open-tubular capillary electrochromatography

Journal of Liquid Chromatography and Related Technologies

Volumn 32, Issue 18, 2009, Pages 2627-2641

  Hu, Kai ^a   Tian, Yulu ^a   Yang, Hui ^a   Zhang, Junqiang ^a   Xie, Jing ^a   Ye, Baoxian ^a   Wu, Yangjie ^a   Zhang, Shusheng ^a  

^a ZHENGZHOU UNIVERSITY   (China)

Author keywords

Calixarene; Open tubular capillary electrochromatography; Quantum chemistry calculation; Sol gel method

Indexed keywords

ANALYTES; BASE SET; BENZENEDIOL; BINAPHTHYL; CALIX[4]ARENES; CALIXARENE; CALIXARENES; ELECTROOSMOTIC FLOW; OPEN-TUBULAR CAPILLARY ELECTROCHROMATOGRAPHY; P-TERT-BUTYLCALIX[4]ARENE; POSITIONAL ISOMERS; QUANTUM CHEMISTRY CALCULATION; QUANTUM CHEMISTRY CALCULATIONS; SEPARATION MODES; SEPARATION PERFORMANCE; SOL-GEL COATINGS; SOL-GEL COLUMN; SOL-GEL METHOD; SOL-GEL METHODS;

AMINES; CAPILLARY FLOW; CHROMATOGRAPHY; ELECTROOSMOSIS; GELATION; GELS; INFRARED SPECTROSCOPY; ISOMERS; QUANTUM THEORY; SOL-GELS; SOLS; SPECTROSCOPIC ANALYSIS;

SOL-GEL PROCESS;

4 TERT BUTYLCALIX[4]ARENE; BENZENE DERIVATIVE; BENZENEDIOL DERIVATIVE; BUTYLATED HYDROXYANISOLE; CALIXARENE; UNCLASSIFIED DRUG;

ARTICLE; CAPILLARY ELECTROCHROMATOGRAPHY; CAPILLARY ELECTROPHORESIS; CHEMICAL STRUCTURE; CHIRALITY; CONTROLLED STUDY; ELECTROOSMOSIS; FILM COATING; INFRARED SPECTROSCOPY; ISOMERIZATION; MOLECULAR INTERACTION; PH; QUANTUM CHEMISTRY; REPRODUCIBILITY; SYNTHESIS;

EID: 70350629595     PISSN: 10826076     EISSN: 1520572X     Source Type: Journal    
DOI: 10.1080/10826070903245557     Document Type: Article

References (23)

1. Pfeffer, W.D.; Yeung, E.S. Open-tubular liquid chromatography with surfactant enhanced electroosmotic flow. Anal. Chem. 1990, 62, 2178-2182.
2. Armstrong, D.W.; Tang, Y.; Ward. T. Derivatized cyclodextrins Immobilized on fused-silica capillaries for enantiomeric via capillary electrophoresis, gas chromatography, or supercritical fluid chromatography. Anal. Chem. 1993, 65, 1114-1117.
3. Matyska, M.T.; Peske, J.J.; Katrekar, A. Open tubular capillary electrochromatography using etched fused-silica tubing modified with chemically bonded liquid crystals. Anal. Chem. 1999, 71, 5508-5514.
4. Pesek, J.J.; Matyska, M.T.; Dawson, G.B. Open tubular capillary electrochromatography of synthetic peptides on etched chemically modified columns. Anal. Chem. 2004, 76, 23-30.
5. Guo, Y.; Colon, L.A. A stationary phase for open-tubular liquid chromatography and electrochromatography using sol-gel technology. Anal. Chem. 1995, 67, 2511-2516.
6. Rodriguez, S.A.; Colon, L.A. Investigations of a sol-gel derived stationary phase for open-tubular capillary electrochromatography. Anal. Chim. Acta 1999, 397, 207-214.
7. Hayes, J.D.; Malik, A. Sol-gel open-tubular ODS columns with reversed Electroosmotic flow for capillary electrochromatography. Anal. Chem. 2001, 73, 987-996.
8. Zhao, Y.X.; Zhao, R.; Shangguan, D.H. A new type of capillary column for open-tubular electrochromatography. Electrophoresis 2002, 23, 2990-2995.
9. Narang, P.; Colon, L.A. Sol-gel-derived fluorinated stationary phase for open tubular electrochromatography. J. Chromatogr. A 1997, 773, 65-72.
10. Li, W.; Fries, D.; Alli, A.; Malik, A. Positively charged sol-gel coatings for on-line preconcentration of amino acids in capillary electrophoresis. Anal. Chem. 2004, 76, 218-227.
11. Narumi, F.; Iki, N.; Suzuki, T. Syntheses of chirally modified thiacalix[4] arenes with enantiomeric amines and their application to chiral stationary phases for gas chromatography. Enantiomer. 2000, 5 (1), 83-93.
12. Ding, C.; Qu, K.; Li, Y.; Hu, K.; Liu, H.; Ye, B.; Wu, Y.; Zhang, S. Preparation and characterization of six calixarene bonded stationary phases for high performance liquid chromatography. J. Chromatogr. A 2007, 1170, 73-81.
13. Pena, M.S.; Zhang, Y.; Thibodeaux, S. Synthesis of a water-soluble chiral N-acylcalix[4]arene amino acid derivative. Tetrahedron Lett. 1996, 37, 5841-5844.
14. Pena, M.S.; Zhang, Y.; Warner, I.M. Enantiomeric Separations by use of calixarene electrokinetic chromatography. Anal. Chem. 1997, 69, 3239-3242.
15. Grady, T.; Joyce, T.; Smyth, M.R. Chiral resolution of the enantiomers of phenylglycinol using (S)-di-naphthylprolinol calix[4]arene by capillary electrophoresis and fluorescence spectroscopy. Anal. Commun. 1998, 35, 123-125. (Pubitemid 128482572)
16. Wang, Z.X.; Chen, Y.; Yuan, H.S. Preparation and characterization of calixarene-coated capillaries for capillary electrophoresis. Electrophoresis 2000, 21, 1620-1624.
17. Zeng, Z.R.; Xie, C.H.; Li, H.B. Open-tubular capillary electrochromatgraphy using capillary columns chemically bonded with the new host molecules calix[6]crown, calyx[6]arene. Electrophoresis 2002, 23, 1272-1278.
18. Wu, X.J.; Liu, H.X.; Liu, H.; Zhang, S.; Haddad, P.R. Preparation and characterization of p-tert-butylcalix[8]arene bonded capillaries for open-tubular capillary electrochromatography. Anal. Chim. Acta 2003, 478 (2), 191-197.
19. Tian, Y.; Li, H.B.; Zeng, Z.R. A novel sol-gel calix[4]arene-modified capillary column for open-tubular capillary electrochromatography. Electrophoresis 2006, 27, 3381-3390.
20. Gutsche, C.D.; Iqbal, M. p-tert-Butylcalix[4]arene. Org. Synth. 1990, 68, 234-237.
21. Ding, C.; Han, P.; Song, J.; Liu, H.; Zhang, S.; Ye, B.; Wu, Y. Development of high performance liquid chromatography and nonaqueous capillary electrophoresis methods for the separation of calixarene derivatives. Anal. Chim. Acta 2006, 566, 246-252.
22. Yang, H.; Zhang, R.; Lu, Y.; Ye, B.; Wu, Y.; Zhang, S. Separation and determination of calixarenes and related derivatives by capillary zone electrophoresis using acetonitrile as a modifier. Chromatographia 2008, 68 (1-2), 123-127.
23. Hu, K.; Qu, K.; Li, Y.; Ding, C.; Wang, X.; Zhang, J.; Ye, B.; Zhang, S. Investigation of retention mechanism of naphthol and benzenediol on calix[4]arene stationary phase based on quantum chemistry calculation. J. Sep. Sci. 2008, 31, 2430-2433.