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70350339594
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Crystal data for 1: Pl, a = 7.247(2), b = 11.120(4), c = 19.703(6) Â, a = 92.536(4), ß = 93.095(4), y = 94.991(4)°, V= 1577.5(9) Â3, Z = 2, Rl = 0.0822 (wRl = 0.1776) for I > Iσ(I)
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Crystal data for 1: Pl, a = 7.247(2), b = 11.120(4), c = 19.703(6) Â, a = 92.536(4), ß = 93.095(4), y = 94.991(4)°, V= 1577.5(9) Â3, Z = 2, Rl = 0.0822 (wRl = 0.1776) for I > Iσ(I).
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Crystal data for 2: Pl1In, a = 7.3947(11), ž> = 21.661(3), c = 43.789(7) À, β = 90.909(3)°, V=7013.2(18) À3, Z = S, Rl = 0.0778 (wR2 = 0.1043) for 1>2a(7). CCDC 730559 (1) and CCDC 730560 (2) contain the supplementary crystallographic data for this paper. These data can be obtained free of charge from The Cambridge Crystallographic Data Centre via www. ccdc.cam.ac.uk/data-request/cif.
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