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47
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70350030409
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note
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10O 686.3230, found 686.3237.
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48
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70350030406
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Synthesis of complex [Zn2(L3)]4, To a solution of L3 (160 mg, 0.29 mmol) in 10 ml of hot ethanol was added methanolic solution of Zn(NO3)2·6H2O 88 mg, 0.58 mmol, the mixture was stirred at reflux for 30 min. After cooling to rt, the resulted white precipitate was collected by filtration, washed with cold ethanol, and dried to give 0.20 g of the dizinc complex. Anal. Calcd for C41H41N13O12Zn2: C, 47.41; H, 3.98; N, 17.53. Found: C, 47.02; H, 4.03; N, 17.64
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2: C, 47.41; H, 3.98; N, 17.53. Found: C, 47.02; H, 4.03; N, 17.64.
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50
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70350027462
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note
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