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-1): 3672 (w), 3649 (w), 2892 (w), 1652 (s), 1614 (s), 1551 (s), 1437 (s), 1370 (s), 1158 (s), 1106 (m), 1055 (m), 768 (m), 725 (w).
-
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54
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70349415883
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note
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2 = 0.1004 (all data) and S = 1.031. Data were collected on a Bruker Apex II CCD diffractometer with graphite-monochromated Mo Kα radiation (λ = 0.71073 Å). The structure was solved with direct methods and refined with full-matrix least-squares (SHELX-97). Selected bond lengths (Å) and angles (°) for compound 1 are listed in Table S1, supporting information.
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