Double-quantum homonuclear NMR correlation spectroscopy of quadrupolar nuclei subjected to magic-angle spinning and high magnetic field

Journal of Magnetic Resonance

Volumn 200, Issue 2, 2009, Pages 251-260

  Wang, Q ^a,b,c   Hu, B ^a   Lafon, O ^a   Trebosc J ^a   Deng, F ^b   Amoureux, J P ^a  

^a UNIV LILLE   (France)

^b Wuhan National Laboratory for Optoelectronics   (China)

^c UNIVERSITY OF CHINESE ACADEMY OF SCIENCES   (China)

Author keywords

Double quanta spectroscopy; Fast MAS; Half integer quadrupolar nuclei; Solid state NMR

Indexed keywords

ALUMINOPHOSPHATES; DIPOLAR RECOUPLING; DOUBLE-QUANTA SPECTROSCOPY; DOUBLE-QUANTUM; FAST MAS; HALF-INTEGER QUADRUPOLAR NUCLEI; HIGH MAGNETIC FIELDS; HOMONUCLEAR; MAGIC ANGLE SPINNING; NEW APPLICATIONS; NMR CORRELATION SPECTROSCOPY; QUADRUPOLAR NUCLEUS; RADIO-FREQUENCY FIELDS; RECOUPLING; SOLID-STATE NMR;

COHERENT LIGHT; MAGNETIC FIELDS; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; SOLID STATE PHYSICS;

NUCLEAR MAGNETIC RESONANCE;

ALUMINUM DERIVATIVE; PHOSPHATE;

ALGORITHM; ARTICLE; CHEMICAL MODEL; COMPUTER SIMULATION; ELECTROMAGNETIC FIELD; METHODOLOGY; NUCLEAR MAGNETIC RESONANCE; SENSITIVITY AND SPECIFICITY; SPIN LABELING;

ALGORITHMS; ALUMINUM COMPOUNDS; COMPUTER SIMULATION; ELECTROMAGNETIC FIELDS; MODELS, CHEMICAL; NUCLEAR MAGNETIC RESONANCE, BIOMOLECULAR; PHOSPHATES; SENSITIVITY AND SPECIFICITY; SPIN LABELS;

CITRUS MAXIMA;

EID: 69949160151     PISSN: 10907807     EISSN: 10960856     Source Type: Journal    
DOI: 10.1016/j.jmr.2009.07.009     Document Type: Article

References (58)

1. Dusold S., and Sebald A. Dipolar recoupling under magic-angle-spinning conditions. Annu. Rep. NMR Spectrosc. 41 (2000) 185-264
2. Levitt M.H. In: Grant D.M., and Harris R.K. (Eds). Symmetry-Based Pulse Sequences in Magic-Angle Spinning Solid-State NMR in Encyclopedia of Nuclear Magnetic Resonance vol. 9 (2002), Wiley, Chichester
3. Ding S., and McDowell C.A. Spectral spin diffusion of a spin-3/2 system in rotating solids. Mol. Phys. 85 (1995) 283-298
4. Dowell N.G., Ashbrook S.E., and Wimperis S. Relative orientation of quadrupole tensors from high-resolution NMR of powdered solids. J. Phys. Chem. A 106 (2002) 9470-9478
5. Duer M.J. Determination of structural data from multiple-quantum magic-angle spinning NMR experiments. Chem. Phys. Lett. 277 (1997) 167-174
6. Duer M.J., and Painter A.J. Correlating quadrupolar nuclear spins: a multiple-quantum NMR approach. Chem. Phys. Lett. 313 (1999) 763-770
7. Eden M., and Frydman L. Quadrupolar-driven recoupling of homonuclear dipolar interactions in the nuclear magnetic resonance of rotating solids. J. Chem. Phys. 114 (2001) 4116-4123
8. Eden M., Grinshtein J., and Frydman L. High-resolution 3D exchange NMR spectroscopy and the mapping of connectivities between half-integer quadrupolar nuclei. J. Am. Chem. Soc. 124 (2002) 9708-9709
9. Eden M., and Frydman L. Homonuclear NMR correlations between half-integer quadrupolar nuclei undergoing magic-angle spinning. J. Phys. Chem. B 107 (2003) 14598-14611
10. Kentgens A.P.M., van Eck E.R.H., Ajithkumar T.G., Anupold T., Past J., Reinhold A., and Samoson A. New opportunities for double rotation NMR of half-integer quadrupolar nuclei. J. Magn. Reson. 178 (2006) 212-219
11. 3. Chem. Phys. Lett. 432 (2006) 152-156
12. 11B exchange NMR study in mesoporous boron carbon nitride at 21.8 T. Solid State Nucl. Magn. Reson. 31 (2007) 193-196
13. Nijman M., Ernst M., Kentgens A.P.M., and Meier B.H. Rotational-resonance NMR experiments in half-integer quadrupolar spin-systems. Mol. Phys. 98 (2000) 161-178
14. Hartmann P., Jäger C., and Zwanziger J.W. Off-angle correlation spectroscopy applied to spin-1/2 and quadrupolar nuclei. Solid State Nucl. Magn. Reson. 13 (1999) 245-254
15. 4 magic angle. J. Am. Chem. Soc. 125 (2003) 2398-2399
16. Vega S. Fictitious spin-1/2 operator formalism for multiple quantum NMR. J. Chem. Phys. 68 (1978) 5518-5527
17. Oas T.G., Griffin R.G., and Levitt M.H. Rotary resonance recoupling of dipolar interactions in solid-state nuclear magnetic resonance spectroscopy. J. Chem. Phys. 89 (1988) 692-695
18. Nielsen N.C., Bildsoe H., Jakobsen H.J., and Levitt M.H. Double-quantum homonuclear rotary resonance: efficient dipolar recovery in magic-angle spinning nuclear magnetic resonance. J. Chem. Phys. 101 (1994) 1805-1812
19. Baldus M., Rovnyak D., and Griffin R.G. Radio-frequency-mediated dipolar recoupling among half-integer quadrupolar spins. J. Chem. Phys. 112 (2000) 5902-5909
20. Wi S., Logan J.W., Sakellariou D., Walls J.D., and Pines A. Rotary resonance recoupling for half-integer quadrupolar nuclei in solid-state nuclear magnetic resonance spectroscopy. J. Chem. Phys. 117 (2002) 7024-7033
21. Painter J., and Duer M.J. Double-quantum-filtered nuclear magnetic resonance spectroscopy applied to quadrupolar nuclei in solids. J. Chem. Phys. 116 (2002) 710-722
22. Mali G., Fink G., and Taulelle F. Double-quantum homonuclear correlation magic-angle sample spinning nuclear magnetic resonance spectroscopy of dipolar-coupled quadrupolar nuclei. J. Chem. Phys. 120 (2004) 2835-2845
23. Mali G., and Kaucic V. Enhancing sensitivity or resolution of homonuclear correlation experiment for half-integer quadrupolar nuclei. J. Magn. Reson. 171 (2004) 48-56
24. Eden M., Annersten H., and Zazzi A. Pulse-assisted homonuclear dipolar recoupling of half-integer quadrupolar spins in magic-angle spinning NMR. Chem. Phys. Lett. 410 (2005) 24-30
25. Eden M., Zhou D., and Yu J. Improved double-quantum NMR correlation spectroscopy of dipolar-coupled quadrupolar spins. Chem. Phys. Lett. 431 (2006) 397-403
26. 27Al single- and double-resonance MAS NMR experiments. J. Phys. Chem. C112 (2008) 7210-7222
27. Lo A.Y.H., and Eden M. Efficient symmetry-based homonuclear dipolar recoupling of quadrupolar spins: double-quantum NMR correlations in amorphous solids. Phys. Chem. Chem. Phys. 10 (2008) 6635-6644
28. Mali G., Kaucic V., and Taulelle F. Measuring distances between half-integer quadrupolar nuclei and detecting relative orientations of quadrupolar and dipolar tensors by double-quantum homonuclear dipolar recoupling nuclear magnetic resonance experiments. J. Chem. Phys. 128 (2008) 204503
29. Brinkmann A., Kentgens A.P.M., Anupold T., and Samoson A. Symmetry-based recoupling in double-rotation NMR spectroscopy. J. Chem. Phys. 129 (2008) 174507
30. Carravetta M., Edén M., Zhao X., Brinkmann A., and Levitt M.H. Symmetry principles for the design of radiofrequency pulse sequences in the nuclear magnetic resonance of rotating solids. Chem. Phys. Lett. 321 (2000) 205-215
31. Brinkmann A., and Eden M. Second order average Hamiltonian theory of symmetry-based pulse schemes in the nuclear magnetic resonance of rotating solids: application to triple-quantum dipolar recoupling. J. Chem. Phys. 120 (2004) 11726-11745
32. Brinkmann A., Schmedt auf der Günne J., and Levitt M.H. Homonuclear zero-quantum recoupling in fast magic-angle spinning nuclear magnetic resonance. J. Magn. Reson. 156 (2002) 79-96
33. Bak M., Rasmussen J.T., and Nielsen N.C. SIMPSON: a general simulation program for solid-state NMR spectroscopy. J. Magn. Reson. 147 (2000) 296-330
34. Bak M., and Nielsen N.C. REPULSION: a novel approach to efficient powder averaging in solid-state NMR. J. Magn. Reson. 125 (1997) 132-139
35. Massiot D., Fayon F., Alonso B., Trebosc J., and Amoureux J.P. Chemical bonding differences evidenced from J-coupling in solid-state NMR experiments involving quadrupolar nuclei. J. Magn. Reson. 164 (2003) 160-164
36. Goiffon A., Jumas J.C., Aurin M.M., and Philippot E. J. Solid State Chem. 61 (1986) 384-396
37. Rocha J., Kolodziejski W., He H., and Klinowski J. Solid state NMR studies of hydrated porous aluminophosphate VPI-5. J. Am. Chem. Soc. 114 (1992) 4884-4888
38. 27Al MAS NMR spectroscopy study of the high-temperature phase transformation of microporous VPI-5. J. Phys. Chem. 100 (1996) 17889
39. McCusker L.B., Barlocher Ch., Jahn E., and Bulow M. Zeolites 11 (1991) 308
40. Derouane E.G., He H., Derouane-Abd Hamid S.B., and Ivanova I.I. In situ MAS NMR investigations of molecular sieves and zeolite-catalyzed reactions. Catal. Lett. 58 (1999) 1-19
41. 4-14. Enhanced resolution and information by MQMAS. Microporous Mater. 6 (1996) 331-340
42. 4-14. Microporous Mesoporous Mater. 57 (2003) 211-214
43. Madhu P.K., Golbourt A., Frydman L., and Vega S. Sensitivity enhancement of the MQMAS NMR experiment by fast amplitude modulation of the pulses. Chem. Phys. Lett. 307 (1999) 41-47
44. Yao Z., Kwak H.T., Sakellariou D., Emsley L., and Grandinetti P.J. Sensitivity enhancement of the central transition NMR signal of quadrupolar nuclei under magic-angle spinning. Chem. Phys. Lett. 327 (2001) 85-90
45. Kentgens A.P.M., and Verhagen R. Advantages of double-frequency sweeps in static, MAS and MQMAS NMR of spin-3/2 nuclei. Chem. Phys. Lett. 300 (1999) 435-443
46. Siegel R., Nakashima T.T., and Wasylishen R.E. Signal enhancement of NMR spectra of half-integer quadrupolar nuclei in solids using hyperbolic secant pulses. Chem. Phys. Lett. 388 (2004) 441-445
47. Dey K.K., Prasad S., Ash J.T., Deschamps M., and Grandinetti P.J. Spectral editing in solid state MAS NMR of quadrupolar nuclei using selective satellite inversion. J. Magn. Reson. 185 (2007) 326-330
48. 4-D. Microporous Mesoporous Mater. 39 (2000) 281-289
49. Vosegaard T., Larsen F.H., Jakobsen H.J., Ellis P.D., and Nielsen N.C. Sensitivity-enhanced multiple quantum MAS NMR of half-integer quadrupolar nuclei. J. Am. Chem. Soc. 119 (1997) 9055-9056
50. Lefort R., W Wiench J., Pruski M., and Amoureux J.P. Optimization of data acquisition and processing in Carr-Purcell-Meiboom-Gill multiple-quantum magic angle spinning nuclear magnetic resonance. J. Chem. Phys. 116 (2002) 2493-2501
51. Mao K., Wiench J., Lin V.S.Y., and Pruski M. Indirectly detected through-bond chemical shift correlation NMR spectroscopy in solids under fast MAS: studies of organic-inorganic hybrid materials. J. Magn. Reson. 196 (2009) 92-95
52. Kwak H.T., Srinivasan P., Quine J., Massiot D., and Gan Z. Satellite transition rotational resonance of homonuclear quadrupolar spins: magic-angle effect on spin-echo decay and inversion recovery. Chem. Phys. Lett. 376 (2003) 75-82
53. Iuga D., Morais C., Gan Z., Neuville D.R., Cormier L., and Massiot D. NMR heteronuclear correlation between quadrupolar nuclei in solids. J. Am. Chem. Soc. 127 (2005) 11540-11541
54. Frydman L., and Harwood J.S. Isotropic spectra of half-integer quadrupolar spins from bidimensional magic-angle spinning NMR. J. Am. Chem. Soc. 117 (1995) 5367-5368
55. Gan Z. Isotropic NMR spectra of half-integer quadrupolar nuclei using satellite transitions and magic-angle spinning. J. Am. Chem. Soc. 122 (2000) 3242-3243
56. Trebosc J., Amoureux J.P., and Gan Z. Comparison of high-resolution solid-state NMR MQMAS and STMAS methods for half-integer quadrupolar nuclei. Solid State NMR 31 (2007) 1-9
57. Edén M. Determination of absolute quadrupolar tensor orientations by double-quantum NMR on powders. Chem. Phys. Lett. 470 (2009) 318-324
58. Lin J., Bayro M.J., Griffin R.G., and Khaneja N. Dipolar recoupling in solid state NMR by phase alternating pulse sequences. J. Magn. Reson. 197 (2009) 145-152