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Volumn 65, Issue 39, 2009, Pages 8191-8198

A new approach to 2,2-disubstituted 1-(methylsulfanyl)vinyl phosphonates via an intermediate thiocarbonyl ylide

Author keywords

[No Author keywords available]

Indexed keywords

PHOSPHONIC ACID DERIVATIVE; SULFONE DERIVATIVE; SULFOXIDE; TETRAHYDROFURAN;

EID: 69049103078     PISSN: 00404020     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.tet.2009.07.074     Document Type: Article
Times cited : (14)

References (48)
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    • (2008) Comprehensive Heterocyclic Chemistry 3 , vol.1 05 , pp. 299-389
    • Warkentin, J.1    Plazuk, D.2
  • 16
    • 0000794457 scopus 로고
    • 3 has been prepared by Raasch via the reaction of trimethyl phosphite with bis(trifluoromethyl)thioketone:
    • 3 has been prepared by Raasch via the reaction of trimethyl phosphite with bis(trifluoromethyl)thioketone:. Raasch M.S. J. Org. Chem. 43 (1978) 2500-2508
    • (1978) J. Org. Chem. , vol.43 , pp. 2500-2508
    • Raasch, M.S.1
  • 17
    • 84987527469 scopus 로고
    • Another approach is the Peterson olefination of (methylthio)(trimethylsilyl)methylphosphonate with thioketones, but this method suffers from low yields:
    • Another approach is the Peterson olefination of (methylthio)(trimethylsilyl)methylphosphonate with thioketones, but this method suffers from low yields:. Mikolajczyk M., and Balczewski P. Synthesis (1989) 101-106
    • (1989) Synthesis , pp. 101-106
    • Mikolajczyk, M.1    Balczewski, P.2
  • 24
    • 69049102614 scopus 로고    scopus 로고
    • note
    • In addition to the disubstituted diazomethanes 7a-g, monosubstituted diazomethanes such as diazoethane, methyl diazoacetate, and diethyl diazomethyl phosphonate were tested in reactions with 6. In all cases, complex mixtures of products were formed.
  • 28
    • 0003992985 scopus 로고
    • Report ORNL-5138, Oak Ridge National Laboratory, Oak Ridge, Tennessee
    • Johnson C.K. ORTEP II. Report ORNL-5138 (1976), Oak Ridge National Laboratory, Oak Ridge, Tennessee
    • (1976) ORTEP II
    • Johnson, C.K.1
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    • 0003591858 scopus 로고    scopus 로고
    • Bruker AXS, Madison, WI
    • SAINT (Version 6.02a) (1999), Bruker AXS, Madison, WI
    • (1999) SAINT (Version 6.02a)
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    • 0004283944 scopus 로고    scopus 로고
    • University of Göttingen, Germany
    • Sheldrick G.M. SADABS (1997), University of Göttingen, Germany
    • (1997) SADABS
    • Sheldrick, G.M.1
  • 37
    • 0031059866 scopus 로고    scopus 로고
    • Methods in Enzymology
    • Carter Jr. C.W., and Sweet R.M. (Eds), Academic, New York, NY
    • Otwinowski Z., and Minor W. Methods in Enzymology. In: Carter Jr. C.W., and Sweet R.M. (Eds). Macromolecular Crystallography, Part A Vol. 276 (1997), Academic, New York, NY 307-326
    • (1997) Macromolecular Crystallography, Part A , vol.276 , pp. 307-326
    • Otwinowski, Z.1    Minor, W.2
  • 39
    • 69049087251 scopus 로고    scopus 로고
    • note
    • CCDC 723945-723947 contains the supplementary crystallographic data for this paper. These data can be obtained free of charge from the Cambridge Crystallographic Data Centre, via www.ccdc.cam.ac.uk/data_request/cif.


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.