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Volumn 82, Issue 8, 2009, Pages 1044-1051

Microwave-assisted synthesisof monodisperse nickel nanoparticles using a complex of nickel formate with long-chainamine ligands

Author keywords

[No Author keywords available]

Indexed keywords

ALKYL AMINES; AVERAGE SIZE; DODECYL AMINES; FACE-CENTERED CUBIC; MICROWAVE-ASSISTED; MONODISPERSE; NI NANOPARTICLES; NI2+ ION; NICKEL FORMATE; NICKEL NANOPARTICLES; OLEYLAMINE; REACTION TEMPERATURE;

EID: 68949170489     PISSN: 00092673     EISSN: 13480634     Source Type: Journal    
DOI: 10.1246/bcsj.82.1044     Document Type: Article
Times cited : (13)

References (49)
  • 44
    • 68949180589 scopus 로고    scopus 로고
    • Note
    • 45, 46 An aqueous solution of nickel dichloride (12 mmol) was mixed with acetylacetone (24 mmol) and an aqueous solution of potassium hydroxide (24 mmol). The resulting solution was stirred for 10 min. Then tmen (15 mmol) was added into the mixture and the solution was stirred for 20 min. The complex was extracted with 1, 2-dichloromethane and purified by recrystallizing from 1, 2- dichloromethane under air atmosphere Preparation of the Ni2+ complex [Ni(acac)2(tmen)]; Crystalline [Ni(acac)2(tmen)] was prepared in the following procedure.45, 46 An aqueous solution of nickel dichloride (12 mmol) was mixed with acetylacetone (24 mmol) and an aqueous solution of potassium hydroxide (24 mmol). The resulting solution was stirred for 10 min. Then tmen (15 mmol) was added into the mixture and the solution was stirred for 20 min. The complex was extracted with 1, 2-dichloromethane and purified by recrystallizing from 1, 2- dichloromethane under air atmosphere.


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.