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2) was slowly bubbled into the solution. After 7 h, the reaction mixture was concentrated and flash chromatography afforded 3 (311 mg, 74%) as a single diastereomer (cyclohexane/t-BuOMe). White solid. Mp 86-87 °C.
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2) was slowly bubbled into the solution. After 7 h, the reaction mixture was concentrated and flash chromatography afforded 3 (311 mg, 74%) as a single diastereomer (cyclohexane/t-BuOMe). White solid. Mp 86-87 °C.
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