Experimental and numerical examination of eddy (Foucault) currents in rotating micro-coils: Generation of heat and its impact on sample temperature

Journal of Magnetic Resonance

Volumn 200, Issue 1, 2009, Pages 6-14

  Aguiar, Pedro M ^a   Jacquinot, Jacques François ^a   Sakellariou, Dimitris ^a  

^a CNRS UMR 3299   (France)

Author keywords

Chemical shift thermometry; Eddy currents; Finite elements calculations; Lead nitrate; MACS; Magic angle coil spinning; Nuclear magnetic resonance; Rotating micro coils

Indexed keywords

FINITE ELEMENTS CALCULATIONS; LEAD NITRATE; MACS; MAGIC ANGLE COIL SPINNING; ROTATING MICRO-COILS;

CHEMICAL ELEMENTS; CHEMICAL SHIFT; CONDUCTIVE MATERIALS; COUPLED CIRCUITS; HEATING; NUCLEAR MAGNETIC RESONANCE; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; RESONANCE; ROTATION; SOLENOIDS; TEMPERATURE SENSORS; THERMOMETERS;

EDDY CURRENTS;

LEAD;

ALGORITHM; ARTICLE; ELECTROMAGNETIC FIELD; ENERGY TRANSFER; HEAT; INSTRUMENTATION; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; TEMPERATURE; THEORETICAL MODEL; THERMOMETER;

ALGORITHMS; ELECTROMAGNETIC FIELDS; ENERGY TRANSFER; HOT TEMPERATURE; LEAD RADIOISOTOPES; MAGNETIC RESONANCE SPECTROSCOPY; MODELS, THEORETICAL; TEMPERATURE; THERMOMETERS;

EID: 68149172920     PISSN: 10907807     EISSN: 10960856     Source Type: Journal    
DOI: 10.1016/j.jmr.2009.05.010     Document Type: Article

References (43)

1. Morris G.A., and Freeman R. Enhancement of nuclear magnetic resonance signals by polarization transfer. Journal of the American Chemical Society 101 (1979) 760-762
2. Pines A., Gibby M.G., and Waugh J.S. Proton-enhanced nuclear induction spectroscopy. Method for high-resolution NMR of dilute spins in solids. Journal of Chemical Physics 56 (1972) 1776-1777
3. Abragam A., and Goldman M. Principles of dynamic nuclear polarisation. Reports on Progress in Physics (1978) 395
4. Maly T., Debelouchina G.T., Bajaj V.S., Hu K.N., Joo C.G., Mak-Jurkauskas M.L., Sirigiri J.R., van der Wel P.C.A., Herzfeld J., Temkin R.J., and Griffin R.G. Dynamic nuclear polarization at high magnetic fields. Journal of Chemical Physics 128 (2008) 052211-052219
5. Martin G.E. Cryogenic NMR probes: applications. In: Grant D.M., and Harris R.K. (Eds). Encyclopedia of Nuclear Magnetic Resonance (2002), Wiley, New York
6. Greenberg Y.S. Application of superconducting quantum interference devices to nuclear magnetic resonance. Reviews of Modern Physics 70 (1998) 175
7. Verpillat F., Ledbetter M.P., Xu S., Michalak D.J., Hilty C., Bouchard L.S., Antonijevic S., Budker D., and Pines A. Remote detection of nuclear magnetic resonance with an anisotropic magnetoresistive sensor. Proceedings of the National Academy of Sciences of the United States of America 105 (2008) 2271-2273
8. Pannetier-Lecoeur M., Fermon C., Biziere N., Scola J., and Watlliang A.L. RF response of superconducting-GMR mixed sensors, application to NQR. IEEE-Inst Electrical Electronics Engineers Inc. (2007) 598-601
9. Pannetier M., Fermon C., Le Goff G., Simola J., and Kerr E. Femtotesla magnetic field measurement with magnetoresistive sensors. Science 304 (2004) 1648-1650
10. Sidles J.A., and Rugar D. Signal-to-noise ratios in inductive and mechanical detection of magnetic resonance. Physical Review Letters 70 (1993) 3506
11. Sidles J.A. Noninductive detection of single-proton magnetic resonance. Applied Physics Letters 58 (1991) 2854
12. Madsen L.A., Leskowitz G.M., and Weitekamp D.P. Observation of force-detected nuclear magnetic resonance in a homogeneous field. Proceedings of The National Academy of Sciences 101 (2004) 12804-12808
13. Manuel J., and Cohen-Tannoudji C. Spectroscopie Hertzienne-Detection Optique De La Resonance Magnetique Par Modulation De L'effet Faraday Paramagnetique Transversal A La Frequence De Larmor. Comptes Rendus Hebdomadaires Des Seances De L Academie Des Sciences 257 (1963) 413
14. Savukov I.M., Lee S.-K., and Romalis M.V. Optical detection of liquid-state NMR. Nature 442 (2006) 1021-1024
15. Chen C.-N., and Hoult D.I. Biomedical Magnetic Resonance Technology (1989), Adam Hilger
16. Hoult D.I. NMR receiver-description and analysis of design. Progress In Nuclear Magnetic Resonance Spectroscopy 12 (1978) 41-77
17. Hoult D.I. The principle of reciprocity in signal strength calculations-a mathematical guide. Concepts In Magnetic Resonance 12 (2000) 173-187
18. Olson D.L., Peck T.L., Webb A.G., Magin R.L., and Sweedler J.V. High-resolution microcoil H-1 NMR for mass-limited, nanoliter-volume samples. Science 270 (1995) 1967-1970
19. Wu N.A., Peck T.L., Webb A.G., Magin R.L., and Sweedler J.V. H-1 NMR spectroscopy on the nanoliter scale for static and online measurements. Analytical Chemistry 66 (1994) 3849-3857
20. Macnaughtan M.A., Hou T., MacNamara E., Santini R.E., and Raftery D. NMR difference probe: a dual-coil probe for NMR difference spectroscopy. Journal of Magnetic Resonance 156 (2002) 97-103
21. Hou T., Smith J., MacNamara E., Macnaughtan M., and Raftery D. Analysis of multiple samples using multiplex sample NMR: selective excitation and chemical shift imaging approaches. Analytical Chemistry 73 (2001) 2541-2546
22. Fisher G., Petucci C., MacNamara E., and Raftery D. NMR probe for the simultaneous acquisition of multiple samples. Journal of Magnetic Resonance 138 (1999) 160-163
23. Yamauchi K., Janssen J.W.G., and Kentgens A.P.M. Implementing solenoid microcoils for wide-line solid-state NMR. Journal of Magnetic Resonance 167 (2004) 87-96
24. Tang J.A., O'Dell L.A., Aguiar P.M., Lucier B.E.G., Sakellariou D., and Schurko R.W. Application of static microcoils and WURST pulses for solid-state ultra-wideline NMR spectroscopy of quadrupolar nuclei. Chemical Physics Letters 466 (2008) 227-234
25. Janssen H., Brinkmann A., van Eck E.R.H., van Bentum P.J.M., and Kentgens A.P.M. Microcoil high-resolution magic angle spinning NMR spectroscopy. Journal of the American Chemical Society 128 (2006) 8722-8723
26. Sakellariou D., Le Goff G., and Jacquinot J.F. High-resolution, high-sensitivity NMR of nanolitre anisotropic samples by coil spinning. Nature 447 (2007) 694-698
27. van Gorkum L.C.M., Hook J.M., Logan M.B., Hanna J.V., and Wasylishen R.E. Solid-state lead-207 NMR of lead(II) nitrate: localized heating effects at high magic angle spinning speeds. Magnetic Resonance in Chemistry 33 (1995) 791-795
28. 207Pb MAS spectra of solid lead nitrate. An accurate, sensitive thermometer for variable-temperature MAS. Journal of Magnetic Resonance Series A 116 (1995) 215-220
29. 7 as high-temperature shift thermometers in variable-temperature Sn-119 Mas NMR. Journal of Magnetic Resonance Series A 113 (1995) 159-163
30. 7-3 sensitive chemical-shift thermometers. Journal of Magnetic Resonance Series A 101 (1993) 299-306
31. Stringer J.A., Bronnimann C.E., Mullen C.G., Zhou D.H.H., Stellfox S.A., Li Y., Williams E.H., and Rienstra C.M. Reduction of RF-induced sample heating with a scroll coil resonator structure for solid-state NMR probes. Journal of Magnetic Resonance 173 (2005) 40-48
32. Grant C.V., Sit S.L., De Angelis A.A., Khuong K.S., Wu C.H., Plesniak L.A., and Opella S.J. An efficient H-1/P-31 double-resonance solid-state NMR probe that utilizes a scroll coil. Journal of Magnetic Resonance 188 (2007) 279-284
33. Gor'kov P.L., Witter R., Chekmenev E.Y., Nozirov F., Fu R., and Brey W.W. Low-E probe for F-19-H-1 NMR of dilute biological solids. Journal of Magnetic Resonance 189 (2007) 182-189
34. Landau L.D., Lifshitz E.M., and Pitaevskii L.P. Electrodynamics of Continuous Media (1960), Pergamon Press, Oxford
35. Abramov A.D. Eddy current losses in rotating magnet fields. Russian Physical Journal (1971) 38-41
36. Lameraner J., and Stafl M. Eddy Currents (1966), Illife Books, London
37. Smythe W.R. Static and Dynamic Electricity (1968), McGraw Hill, New York
38. Meunier G., Sabonnadiere J.C., and Coulomb J.L. The finite element post-processor of FLUX3D (field computation package). IEEE Transactions on Magnetics 27 (1991) 3786
39. van Gorkom L.C.M., Hook J.M., Logan M.B., Hanna J.V., Wasylishen R.E., van Gorkom L.C.M., Hook J.M., Logan M.B., Hanna J.V., and Wasylishen R.E. Solid-state lead-207 NMR of lead (II) nitrate: localized heating effects at high magic angle spinning speeds. Magnetic Resonance in Chemistry 33 (1995) 791-795
40. 207Pb NMR chemical shift and solid-state structure in Pb(II) compounds. The Journal of Physical Chemistry. A 112 (2008) 3046-3052
41. 207Pb NMR detection of spinning-induced temperature gradients in MAS rotors. Solid State Nuclear Magnetic Resonance 5 (1995) 269
42. Malba V., Maxwell R., Evans L.B., Bernhardt A.E., Cosman M., and Yan K. Laser-lathe lithography-a novel method for manufacturing nuclear magnetic resonance microcoils. Biomedical Microdevices 5 (2003) 21-27
43. Mekaru H., Kusumi S., Sato N., Shimizu M., Yamashita M., Shimada O., and Hattori T. Fabrication of a spiral microcoil using a 3D-LIGA process (2007), Springer pp. 393-402