Implementing solenoid microcoils for wide-line solid-state NMR

Journal of Magnetic Resonance

Volumn 167, Issue 1, 2004, Pages 87-96

  Yamauchi, K ^a   Janssen, J W G ^a   Kentgens, A P M ^a  

^a RADBOUD UNIVERSITY NIJMEGEN   (Netherlands)

Author keywords

High RF field; Limit of detection; Microcoil; Quadrupolar nuclei; Solid state NMR

Indexed keywords

BANDWIDTH; CAPACITORS; MAGNETIC FIELD EFFECTS; MAGNETIC PERMEABILITY; PERMANENT MAGNETS; SIGNAL TO NOISE RATIO; SINGLE CRYSTALS; SOLENOIDS; ZEOLITES;

HIGH RF-FIELD; LIMIT OF DETECTION; MICROCOILS; QUADRUPOLAR NUCLEI; SOLID-STATE NMR;

NUCLEAR MAGNETIC RESONANCE;

SOLENOIDEA;

BAYSILON; DIMETICONE; MINERAL; SILICONE DERIVATIVE;

ARTICLE; COMPARATIVE STUDY; COMPUTER AIDED DESIGN; EQUIPMENT; EQUIPMENT DESIGN; EVALUATION; INSTRUMENTATION; MAGNETISM; METHODOLOGY; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; REPRODUCIBILITY; SENSITIVITY AND SPECIFICITY; TRANSDUCER;

COMPUTER-AIDED DESIGN; DIMETHYLPOLYSILOXANES; EQUIPMENT DESIGN; EQUIPMENT FAILURE ANALYSIS; MAGNETIC RESONANCE SPECTROSCOPY; MAGNETICS; MINERALS; REPRODUCIBILITY OF RESULTS; SENSITIVITY AND SPECIFICITY; SILICONES; TRANSDUCERS;

EID: 1242287509     PISSN: 10907807     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.jmr.2003.12.003     Document Type: Article

References (26)

1. Hoult D.I., Richards R.E. The signal-to-noise ratio of the nuclear magnetic resonance experiment. J. Magn. Reson. 24:1976;71-85.
2. 1H-NMR for mass-limited, nanoliter-volume samples. Science. 270:1995;1967-1970.
3. Webb A.G., Grant S.C. Signal-to-noise and magnetic susceptibility trade-offs in solenoidal microcoils for NMR. J. Magn. Reson. B. 113:1996;83-87.
4. Webb A.G. Radiofrequency microcoils in magnetic resonance. Prog. Nucl. Magn. Reson. Spectrosc. 31:1997;1-42.
5. Subramanian R., Kelley W.P., Floyd P.D., Tan Z.J., Webb A.G., Sweedler J.V. A microcoil NMR probe for coupling microscale HPLC with on-line NMR spectroscopy. Anal. Chem. 71:1999;5335-5339.
6. Trumbull J.D., Glasgow I.K., Beebe D.J., Magin R.L. Integrating microfabricated fluidic systems and NMR spectroscopy. IEEE Trans. Biomed. Eng. 47:2000;3-7.
7. Massin C., Daridon A., Vincent F., Boero G., Besse P.A., Verpoorte E., de Rooij N.F., Popovic R.S. A Microfabricated probe with integrated coils and channels for on-chip NMR spectroscopy. Ramsey J.M. Micro Total Analysis Systems. 2001;438-440.
8. Peck T.L., Magin R.L., Lauterbur P.C. Design and analysis of microcoils for NMR microscopy. J. Magn. Reson. B. 108:1995;114-124.
9. Wind R.A., Minard K.R., Holtom G.R., Majors P.D., Ackerman E.J., Colson S.D., Cory D.G., Daly D.S., Ellis P.D., Metting N.F., Parkinson C.I., Price J.M., Tang X.W. An integrated confocal and magnetic resonance microscope for cellular research. J. Magn. Reson. 147:2000;371-377.
10. Glover P., Mansfield P. Limits to magnetic resonance microscopy. Rep. Prog. Phys. 65:2002;1489-1511.
11. Ciobanu L., Webb A.G., Pennington C.H. Magnetic resonance imaging of biological cells. Prog. Nucl. Magn. Reson. Spectrosc. 42:2003;69-93.
12. Gan Z., Gor'kov P., Massiot D., Butler L., Samoson A. Solid state NMR of quadrupolar nuclei at very high fields. Ann. Res. Rev. NHMFL. 2001;217.
13. Horvatic M., Berthier C. High field NMR in strongly correlated low-dimensional fermionic systems. Int. J. Mod. Phys. B. 16:2002;3265-3270.
14. van Bentum P.J.M., Maan J.C., van Os J.W.M., Kentgens A.P.M. Strategies for solid-state NMR in high-field Bitter and hybrid magnets. Chem. Phys. Lett. 376:2003;338-345.
15. Blumich B., Blumler P., Eidmann G., Guthausen A., Haken R., Schmitz U., Saito K., Zimmer G. The NMR-mouse: construction, excitation, and applications. Magn. Reson. Imaging. 16:1998;479-484.
16. Minard K.R., Wind R.A. Solenoidal microcoil design. Part I: optimizing RF homogeneity and coil dimensions. Concepts Magn. Reson. 13:2001;128-142.
17. Minard K.R., Wind R.A. Solenoidal microcoil design - part II: optimizing winding parameters for maximum signal-to-noise performance. Concepts Magn. Reson. 13:2001;190-210.
18. Hoult D.I. Sensitivity of NMR experiments. Grant D.M., Harris R.K. Encyclopedia of Nuclear Magnetic Resonance. 1996;4256-4266.
19. Varian/Chemagnetics, NMR acqusition and process software spinsight version 4.3.2, 2003.
20. D. Meeker, Finite Element Method Magnetics (FEMM), 2003. Available from 〈http://femm.berlios.de/〉.
21. Varian/Chemagnetics, Console electronic tests to verify console performance relating to NMR S/N , 1999. Available from 〈ftp://ftp.nmr.varianinc.com/chemagnetics/〉.
22. Minard K.R., Wind R.A. Picoliter H-1 NMR spectroscopy. J. Magn. Reson. 154:2002;336-343.
23. Michal C.A. Nuclear magnetic resonance noise spectroscopy using two-photon excitation. J. Chem. Phys. 118:2003;3451-3454.
24. Li Y., Logan T.M., Edison A.S., Webb A. Design of small volume HX and triple-resonance probes for improved limits of detection in protein NMR experiments. J. Magn. Reson. 164:2003;128-135.
25. Vosegaard T., Jakobsen H.J. Al-27 chemical shielding anisotropy. J. Magn. Reson. 128:1997;135-137.
26. Alemany L.B., Steuernagel S., Amoureux J.P., Callender R.L., Barron A.R. Very fast MAS and MQMAS NMR studies of the spectroscopically challenging minerals kyanite and andalusite on 400, 500, and 800. MHz spectrometers Solid State Nucl. Magn. Reson. 14:1999;1-18.