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Volumn 50, Issue 38, 2009, Pages 5392-5394

Chemo-enzymatic asymmetric total synthesis of penienone

Author keywords

[No Author keywords available]

Indexed keywords

5 HYDROXYMETHYL 2 CYCLOHEXENONE; CYCLOHEXANE DERIVATIVE; PENIENONE; UNCLASSIFIED DRUG;

EID: 68049113501     PISSN: 00404039     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.tetlet.2009.07.043     Document Type: Article
Times cited : (8)

References (28)
  • 9
    • 68049092371 scopus 로고    scopus 로고
    • note
    • The enantioselectivity of the lipase-PS-catalyzed trans-esterification step was measured by chiral HPLC (OJ-H, hexane:2-propanol/9:1) of the benzoate derivative of (R)-1 and (S)-1.
  • 10
    • 68049112835 scopus 로고    scopus 로고
    • note
    • 3, 100 MHz), δ: 200.55, 196.34, 147.25, 130.30, 46.53, 36.73, 24.50.
  • 13
    • 68049099577 scopus 로고    scopus 로고
    • note
    • 3), 19.23 (C).
  • 15
    • 68049094409 scopus 로고    scopus 로고
    • note
    • 28 -12.2 (c 1.0, MeOH).
  • 17
    • 68049095423 scopus 로고    scopus 로고
    • note
    • 2).
  • 20
    • 68049100608 scopus 로고    scopus 로고
    • note
    • 3, 100 MHz), δ: 165.25, 152.58, 143.34, 141.03, 136.76, 127.59, 125.34, 122.32, 114.31, 58.51, 34.48, 21.66, 13.28.
  • 21
    • 68049083014 scopus 로고    scopus 로고
    • note
    • (E)-2-Hexen-1-ol was prepared from n-butanal by Horner-Wittig olefination with triethylphosphonoacetate followed by DIBAL-H reduction.
  • 23
    • 68049092370 scopus 로고    scopus 로고
    • note
    • + 213.1249, found 213.1261.
  • 27
    • 68049102506 scopus 로고    scopus 로고
    • note
    • + 243.1355, found 243.1361.
  • 28
    • 68049086075 scopus 로고    scopus 로고
    • note
    • 3).


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.