In situ characterization of elusive salt hydrates-the crystal structures of the heptahydrate and octahydrate of sodium sulfate

Journal of the American Chemical Society

Volumn 130, Issue 52, 2008, Pages 17795-17800

  Oswald, Iain D H ^a   Hamilton, Andrea ^a   Hall, Christopher ^a   Marshall, William G ^b   Prior, Timothy J ^c   Pulham, Colin R ^a  

^a UNIVERSITY OF EDINBURGH   (United Kingdom)

^b RUTHERFORD APPLETON LABORATORY   (United Kingdom)

^c DARESBURY LABORATORY   (United Kingdom)

Author keywords

[No Author keywords available]

Indexed keywords

ANHYDROUS SODIUM SULFATE; AQUEOUS SOLUTIONS; BONDED NETWORKS; DIAMOND-ANVIL CELL; HEPTAHYDRATE; HIGH-PRESSURE CRYSTALLIZATION; IN-SITU; IN-SITU CHARACTERIZATION; INTERMEDIATE PHASE; INTRAMOLECULAR BONDS; MIRABILITE; OCTAHEDRALLY COORDINATED; SALT HYDRATES; SINGLE CRYSTAL X-RAY DIFFRACTION; SINGLE CRYSTAL X-RAY DIFFRACTION METHOD; SODIUM CATIONS; SODIUM IONS; SODIUM SULFATE DECAHYDRATE; STRUCTURAL DIFFERENCES; SULFATE ION; WATER MOLECULE;

CELL MEMBRANES; CRYSTAL STRUCTURE; CRYSTALLIZATION; DIFFRACTION; HYDRATES; HYDRATION; HYDROGEN; METAL IONS; METALLIC GLASS; MOLECULES; POSITIVE IONS; SINGLE CRYSTALS; SOLUTIONS; X RAY DIFFRACTION;

SODIUM SULFATE;

SODIUM ION; SODIUM SULFATE; SULFATE;

ARTICLE; CRYSTAL STRUCTURE; CRYSTALLIZATION;

EID: 67749135574     PISSN: 00027863     EISSN: None     Source Type: Journal    
DOI: 10.1021/ja805429m     Document Type: Article

References (53)

1. Sodium Sulfate: Handbook of Deposits, Processing, Properties, and Use; Garrett, D. E., Ed.; Academic Press: San Diego, CA, 2001.
2. Rasmussen, S. E.; Jørgensen, J.-E.; Lundtoft, B. J. Appl. Cryst. 1996, 29, 42-47.
3. (a) Ohno, H.; Igarashi, M.; Hondoh, T. Earth Planet. Sci. Lett. 2005, 232, 171-178.
4. (b) Ohno, H.; Igarashi, M.; Hondoh, T. Geophys. Res. Lett. 2006, 33, L08501.
5. (a) Grundy, W. M.; Buratti, B. J.; Cheng, A. F.; Emery, J. P.; Lunsford, A.; McKinnon, W. B.; Moore, J. M.; Newman, S. F.; Olkin, C. B.; Reuter, D. C.; Schenk, P. M.; Spencer, J. R.; Stern, S. A.; Throop, H. B.; Weaver, H. A. Science 2007, 12, 234-237.
6. (b) Dalton, J. B.; Prieto-Ballesteros, O.; Kargel, J. S.; Jamieson, C. S.; Jolivet, J.; Quinn, R. Icarus 2005, 177, 472-490.
7. (e) Hall, C.;Hamilton, A.; Icarus 2008, 198, 277-299.
8. Prieto-Ballesteros, O.; Kargel, J. S. Icarus 2005, 173, 212-221.
9. (a) Hamilton, A.; Hall, C.; Pel, L. J. Phys. D 2008, 41, 212002.
10. (b) Rodriguez-Navarro, C.; Doehne, E.; Sebastian, E. Cem. Concr. Res. 2000, 30, 1527-1534.
11. (c) Scherer, G. W. Cem. Concr. Res. 1999, 29, 1347-1358.
12. (d) Espinosa, R. M.; Scherer, G. W. Environ. Geol. 2008, 56, 605-621.
13. (e) Correns, C. W. Discuss. Faraday Soc. 1949, 5, 267-271.
14. (f) Flatt, R. J.; Steiger, M.; Scherer, G. W. Environ. Geol. 2007, 52, 221-237.
15. (g) Rijniers, L. A.; Huinink, H. P.; Pel, L.; Kopinga, K. Phys Rev. Lett. 2005, 94, 07553.
16. (h) Steiger, M. J. Cryst. Growth 2005, 282, 455-469.
17. (i) Steiger, M. J. Cryst. Growth 2005, 282, 470-481.
18. Marliacy, P.; Solimando, R.; Bouroukba, M.; Schuffenecker, L. Thermochim. Acta 2000, 344, 85-94.
19. Loewel, H. Ann. Chim. Phys. 1850, 29, 62-117.
20. Loewel, H. Ann. Chim. Phys. 1851, 33, 334-337.
21. (a) Hartley, H.; Jones, B. M.; Hutchinson, G. A. J. Chem. Soc. 1908, 93, 825-833.
22. (b) de Coppet, L. C. Bull. Soc. Vaudoise Sci. Nat. 1901, 37, 455-462.
23. Mehrotra, B. N. Acta Crystallogr. 1987, A43, C119.
24. Gmelin, L. Handbuch der Anorganischen Chemie; Berlin, 1966; Vol. 21.
25. Genkinger, S.; Putnis, A. Environ. Geol. 2007, 52, 295-303.
26. Steiger, M.; Asmussen, S. Geochim. Cosmochim. Acta 2008, 72, 4291-4306.
27. Hamilton, A.; Hall, C. J. Anal.At. Spectrom. 2008, 23, 840-844.
28. Merrill, L.; Bassett, W. A. Rev. Sci. Instrum. 1974, 45, 290-294.
29. Piermarini, G. J.; Block, S.; Barnett, J. D.; Forman, R. A. J. Appl. Phys. 1975, 46, 2774-2780.
30. Cosier, J.; Glazer, A. M. J. Appl. Crystallogr. 1986, 19, 105-107.
31. Dawson, A.; Allan, D. R.; Parsons, S.; Ruf, M. J. Appl. Crystallogr. 2004, 37, 410-416.
32. Altomare, A.; Cascarano, G.; Giacovazzo, C.; Guagliardi, A. J. Appl. Crystallogr 1994, 27, 1045-1050.
33. Betteridge, P. W.; Carruthers, J. R.; Cooper, R. I.; Prout, K.; Watkin, D. J. J. Appl. Crystallogr. 2003, 36, 1487.
34. Marshall, W. G.; Francis, D. J. J. Appl. Crystsllrer. 2002, 35, 122.
35. Fortes, D. Computational and Experimental Studies of Solids in the Ammonia-Water System. Ph.D. Thesis. Department of Earth Sciences, University College, University of London, 2004.
36. Besson, J. M.; Nelmes, R. J.; Hamel, G.; Loveday, J. S.; Weill, G.; Hull, S. Phys. B 1992, 180-181, 907.
37. (a) Boese, R.; Blaser, D.; Nussbaumer, M.; Krygowski, T. M. Struct. Chem. 1992, 3, 363-368.
38. (b) Konietzny, S.; Fleischer, H.; Parsons, S.; Pulham, C. R. J. Chem. Soc. Dalton Trans. 2001, 3, 304-308.
39. Levy, A. H.; Lisensky, G. C. Acta Crystallogr. 1978, B34, 3502-3510.
40. Brand, H. E. A.; Fortes, A. D.; Wood, I. G.; Knight, K. S.; Vočadlo, L. Phys. Chem. Min. 2008, doi: 10.1007/s00269-008-256-0.
41. De Marignac, J. C. G. Ann. Mines 1857, 12, 1-74.
42. Fabbiani, F. P. A.; Allan, D. R.; Parsons, S.; Pulham, C. R. Acta Crystallogr. 2006, B62, 826-842.
43. Fabbiani, F. P. A.; Pulham, C. R.; Allan, D. R.; David, W. I. F.; Davidson, A. J.; Lennie, A. R.; Parsons, S.; Pulham, C.R.; Warren, J. E. Cryst. Growth Des. 2007, 7, 1115-1124.
44. (a) Fabbiani, F. P. A.; Allan, D. R.; Dawson, A.; D.; David, W. I. F.; McGregor, P. A.; Oswald, I. D. H.; Parsons, S. Chem. Commun. 2003, 24, 3004-3005.
45. (b) Fabbiani, F. P. A.; Allan, D. R.; David, W. I. F.; Moggach, S. A.; Parsons, S.; Pulham, C. R. CrystEngComm. 2004, 6, 504-511.
46. Morrison, C. A.; Walker, M.; Allan, D. R.; Marshall, W. G.; Pulham, C. R. J. Chem. Soc, Dalton Trans. 2007, 20, 2014-2019.
47. Ledru, J.; Imrie, C. T.; Pulham, C. R.; Céolin, R.; Hutchinson, J. M. J. Pharm. Sci. 2007, 96, 2784-2794.
48. Fortes, A. D.; Wood, I. G.; Knight, K. S. Phys. Chem. Min. 2008, 35, 207-221.
49. Dougherty, A. J.; Hogenboom, D. L.; Kargel, J. S.; Zheng, Y. F. Abstract No. 1732; 37th Annual Lunar and Planetary Science Conference; March 13 - 17, 2006; League City, TX.
50. Marion, G. M.; Kargel, J. S.; Catling, D. C.; Jakubowski, S. D. Geochim. Cosmochim. Acta 2005, 69, 259-274.
51. Frank, M. R.; Runge, C. E.; Scott, H. P.; Maglio, S. J.; Olson, J.; Prakapenka, V. B.; Shen, G. Phys. Earth Planet. Inter. 2006, 155, 152-162.
52. Dunitz, J. D.; Bernstein, J. Acc. Chem. Res. 1995, 28, 193-200.
53. Smith, H. G.; Peterson, S. W.; Levy, H. A. J. Chem. Phys. 1968, 48, 5561-5565.