Comparison of direct sampling and emulsion analysis using a filter furnace for the determination of lead in crude oil by graphite furnace atomic absorption spectrometry

Spectrochimica Acta - Part B Atomic Spectroscopy

Volumn 64, Issue 6, 2009, Pages 530-536

  Damin, Isabel C F ^a   Dessuy, Morgana B ^a   Castilhos, Tamara S ^a   Silva, Márcia M ^a   Vale, Maria Goreti R ^a   Welz, Bernhard ^b   Katskov, Dmitri A ^c  

^a FEDERAL UNIVERSITY OF RIO GRANDE DO SUL   (Brazil)

^b FEDERAL UNIVERSITY OF SANTA CATARINA   (Brazil)

^c TSHWANE UNIVERSITY OF TECHNOLOGY   (South Africa)

Author keywords

Crude oil; Direct sampling; Filter furnace; Graphite furnace atomic absorption spectrometry; Lead

Indexed keywords

ACID DIGESTION; ANOVA TEST; AQUEOUS SOLUTIONS; CHEMICAL FORMS; COMMERCIAL AVAILABILITY; COMPLEX NATURE; CONFIDENCE LEVELS; CRUDE OIL; DIRECT METHOD; DIRECT SAMPLING; FILTER FURNACE; GRAPHITE FURNACE ATOMIC ABSORPTION SPECTROMETRY; GRAPHITE TUBES; LEAD DETERMINATION; LIMITS OF DETECTION; OIL-IN-WATER EMULSIONS; OPEN-VESSEL; ROUTINE ANALYSIS; SAMPLE PRETREATMENT; SOLID SAMPLING; TRITON X-100;

ABSORPTION; ATOMIC ABSORPTION SPECTROMETRY; ATOMIC SPECTROSCOPY; ATOMS; CRUDE PETROLEUM; EMULSIFICATION; EMULSIONS; FURNACES; GRAPHITE; LEAD; PALLADIUM; PETROLEUM ANALYSIS; TRACE ANALYSIS; TRACE ELEMENTS;

ABSORPTION SPECTROSCOPY;

EID: 67651113917     PISSN: 05848547     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.sab.2009.03.002     Document Type: Article

References (31)

1. Hardaway C., Sneddon J., and Beck J.N. Determination of metals in crude oil by atomic spectroscopy. Anal. Lett. 37 (2004) 2881-2899
2. Sychra V., Lang I., and Šebor G. Analysis of petroleum and petroleum products by atomic absorption spectroscopy and related techniques. Prog. Anal. At. Spectrosc. 4 (1981) 341-426
3. Kowalewska Z., Bulska E., and Hulanicki A. Organic palladium and palladium-magnesium chemical modifiers in direct determination of lead in fractions from distillation of crude oil by electrothermal atomic absorption analysis. Spectrochim. Acta Part B 54 (1999) 835-843
4. Korn M.G.A., dos Santos D.S.S., Welz B., Vale M.G.R., Teixeira A.P., Lima D.C., and Ferreira S.L.C. Atomic spectrometric methods for the determination of metals and metalloids in automotive fuels - a review. Talanta 73 (2007) 1-11
5. Welz A.B., and Sperling M. Absorption Spectrometry. third ed., (1999), Wiley-VCH, Weinheim, New York
6. Lang I., Šebor G., Sychra V., Kolihova D., and Weisser O. Determination of metals in petroleum samples by atomic-absorption spectrometry.2. Determination of nickel. Anal. Chim. Acta 84 (1976) 229-305
7. Lang I., Šebor G., Weisser O., and Sychra V. Determination of metals in petroleum samples by atomic-absorption spectrometry.3. Effect of added alkali-metals on determination of vanadium in organic solutions. Anal. Chim. Acta 88 (1977) 313-318
8. Šebor G., Lang I., Kolihova D., and Weisser O. Effect of the type of organo-metallic iron and copper-compounds on the determination of both metals in petroleum samples by flame atomic-absorption spectroscopy. Analyst 107 (1982) 1350-1355
9. Duyck C., Miekeley N., da Silveira C.L.P., Aucélio R.Q., Campos R.C., Grinberg P., and Brandão G.P. The determination of trace elements in crude oil and its heavy fractions by atomic spectrometry. Spectrochim. Acta Part B 62 (2007) 939-951
10. de la Guardia M., and Lizondo M.J. Direct determination of nickel in fuel oil by atomic absorption spectrometry using emulsions. At. Spectrosc. 6 (1983) 208-211
11. Aucélio R.Q., Curtius A.J., and Welz B. Sequential determination of Sb and Sn in used lubricating oil by electrothermal atomic absorption spectrometry using Ru as a permanent modifier and micro-emulsion sample introduction. J. Anal. At. Spectrom. 15 (2000) 1389-1393
12. Aucélio R.Q., and Curtius A.J. Evaluation of electrothermal atomic absorption spectrometry for trace determination of Sb, As and Se in gasoline and kerosene using micro-emulsion sample introduction and two approaches for chemical modification. J. Anal. At. Spectrom. 17 (2002) 242-247
13. Burguera J.L., Avila-Gómez R.M., Burguera M., Salager R.A., Salager J.L., Bracho C.L., Burguera-Pascu M., Burguera-Pascu C., Brunetto R., Gallignani M., and Peña Y.P. Optimum phase-behavior formulation of surfactant/oil/water systems for the determination of chromium in heavy crude oil and in bitumen-in-water emulsion. Talanta 61 (2003) 353-361
14. Campos R.C., Santos H.R., and Grinberg P. Determination of copper, iron, lead and nickel in gasoline by electrothermal atomic absorption spectrometry using three-component solutions. Spectrochim. Acta Part B 57 (2002) 15-28
15. Reyes M.N.M., and Campos R.C. Graphite furnace atomic absorption spectrometric determination of Ni and Pb in diesel and gasoline samples stabilized as microemulsion using conventional and permanent modifiers. Spectrochim. Acta Part B 60 (2005) 615-624
16. Ozcan M., and Akman S. Determination of Cu, Co and Pb in gasoline by electrothermal atomic absorption spectrometry using aqueous standard addition in gasoline-ethanol-water three-component system. Spectrochim. Acta Part B 60 (2005) 399-402
17. Vale M.G.R., Oleszczuk N., and dos Santos W.N.L. Current status of direct solid sampling for elctrothermal atomic absorption spectrometry-a critical review of the development between 1995 and 2005. Appl. Spectrosc. Rev. 41 (2006) 377-400
18. Welz B., Borges D.L.G., Vale M.G.R., and Heitmann U. Progress in direct solid sampling analysis using line source and high-resolution continuum source electrothermal atomic absorption spectrometry. Anal. Bioanal. Chem. 389 (2007) 2085-2095
19. Kurfürst U. Solid Sample Analysis - Direct and Slurry Sampling Using ET AAS and ETV-ICP (1998), Springer, Berlin
20. Belarra M.A., Resano M., and Castillo J.R. Discrimination of the causes of imprecision in the direct determination of metals in organic solid samples by electrothermal atomization atomic absorption spectrometry. J. Anal. At. Spectrom. 13 (1998) 489-494
21. Brandão G.P., de Campos R.C., de Castro E.V.R., and de Jesus H.C. Direct determination of nickel in petroleum by solid sampling-graphite furnace atomic absorption spectrometry. Anal. Bioanal. Chem. 386 (2006) 2249-2253
22. Brandão G.P., Campos R.C., Castro E.V.R., and Jesus H.C. Determination of copper, iron and vanadium in petroleum by direct sampling electrothermal atomic absorption spectrometry. Spectrochim. Acta Part B 62 (2007) 962-969
23. Silva M.M., Damin I.C.F., Vale M.G.R., and Welz B. Feasibility of using solid sampling graphite furnace atomic absorption spectrometry for speciation analysis of volatile and non-volatile compounds of nickel and vanadium in crude oil. Talanta 71 (2007) 1877-1885
24. Dittert I.M., Silva J.S.A., Araujo R.G.O., Curtius A.J., Welz B., and Becker-Ross H. Direct and simultaneous determination of Cr and Fe in crude oil using high-resolution continuum source graphite furnace atomic absorption spectrometry. Spectrochim. Acta Part B 64 (2009) 537-543
25. Katskov D.A., Marais P.J.J.G., and Tittarelli P. Design, operation and analytical characteristics of the filter furnace, a new atomizer for electrothermal atomic absorption spectrometry. Spectrochim. Acta Part B 51 (1996) 1169-1189
26. Katskov D.A. Graphite filter atomizer in atomic absorption spectrometry. Spectrochim. Acta Part B 62 (2007) 897-917
27. Anselmi A., Tittarelli P., and Katskov D.A. Determination of trace elements in automotive fuels by filter furnace atomic absorption spectrometry. Spectrochim. Acta Part B 57 (2002) 403-411
28. Damin I.C.F., Vale M.G.R., Silva M.M., Welz B., Lepri F.G., dos Santos W.N.L., and Ferreira S.L.C. Palladium as chemical modifier for the stabilization of volatile nickel and vanadium compounds in crude oil using graphite furnace atomic absorption spectrometry. J. Anal. At. Spectrom. 20 (2005) 1332-1336
29. Dessuy M.B., Vale M.G.R., Souza A.S., Ferreira S.L.C., Welz B., and Katskov D.A. Method development for the determination of lead in wine using electrothermal atomic absorption spectrometry comparing platform and filter furnace atomizers and different chemical modifiers. Talanta 74 (2008) 1321-1329
30. Amorim F.A.C., Lima D.C., Amaro J.A.A., Vale M.G.R., and Ferreira S.L.C. Methods for vanadium determination in fuel oil by GF AAS with microemulsification and acid digestion sampling. J. Braz. Chem. Soc. 18 8 (2007) 1566-1570
31. Silva I.A., Campos R.C., Curtius A.J., and Sella S.M. Determination of lead and copper in kerosene by electrothermal atomic absorption spectrometry: stabilization of metal in organic media by a three-component solution. J. Anal. At. Spectrom. 8 (1993) 749-754