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Volumn 38, Issue 4, 2009, Pages 324-325

Hyperchromic effect of silyl groups on the UV-visible spectrum of 5,10,15,20-tetraphenylporphyrin

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Indexed keywords

EID: 67650509119 PISSN: 03667022 EISSN: 13480715 Source Type: Journal
DOI: 10.1246/cl.2009.324 Document Type: Article

Times cited : (17)

References (19)

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- 2: mp > 300° C; ′HNMR (CDCl3, δ -2.75 (s, 2H, 0.23 (s, 36H, 0.57 (s, 24H, 7.81 (d, 8H, J, 7.9 Hz, 8.19 (d, 8H, J, 7.9 Hz, 8.86 (s, 8H, 13CNMR (CDCl3, δ -3.8, 2.1, 120.2, 132.0, 134.1, 138.8, 142.0; 29SiNMR (CDCl 3, δ -21.2, 19.2; IR (KBr) 3320, 3060, 3010, 2950, 2890, 1560, 1470, 1400, 1250, 1100, 970, 830, 800cm-1; UV-vis (CHCl 3) λmax (ε/M-1 cm-1) 422 (510000, 518 (20000, 553 (12000, 593 (6400, 647 nm (5900, ESI-MS m/z, ) 1135.4 [M, H, 100, Anal. Calcd for C64H 86N4Si8: C, 67.66; H, 7.63; N, 4.93, Found: C, 67.54; H, 7.88; N, 4.90
- 8: C, 67.66; H, 7.63; N, 4.93%. Found: C, 67.54; H, 7.88; N, 4.90%.

12
- 84869339344
- 16: C, 60.00; H, 8.43; N, 3.50%. Found: C, 60.09; H, 8.43; N, 3.50%.
- 16: C, 60.00; H, 8.43; N, 3.50%. Found: C, 60.09; H, 8.43; N, 3.50%.

13
- 84869347051
- 8: C, 68.51; H, 7.95; N, 4.70%. Found: C, 68.76; H, 8.05; N, 4.73%.
- 8: C, 68.51; H, 7.95; N, 4.70%. Found: C, 68.76; H, 8.05; N, 4.73%.

14
- 84869347056
- 16: C, 60.87; H, 8.64; N, 3.38%. Found: C, 60.68; H, 8.54; N, 3.36%.
- 16: C, 60.87; H, 8.64; N, 3.38%. Found: C, 60.68; H, 8.54; N, 3.36%.

15
- 67650493762
- Crystallographic data reported in this manuscript have been deposited with the Cambridge Crystallographic Data Centre as supplementary publication no. CCDC-718841. Copies of the data can be obtained free of charge via www.ccdc.cam.ac.uk/conts/retrieving.html (or from the Cambridge Crystallographic Data Centre, 12, Union Road, Cambridge, CB2 1EZ, UK; fax: +44 1223 336033; or deposit@ccdc.cam.ac.uk).
- Crystallographic data reported in this manuscript have been deposited with the Cambridge Crystallographic Data Centre as supplementary publication no. CCDC-718841. Copies of the data can be obtained free of charge via www.ccdc.cam.ac.uk/conts/retrieving.html (or from the Cambridge Crystallographic Data Centre, 12, Union Road, Cambridge, CB2 1EZ, UK; fax: +44 1223 336033; or deposit@ccdc.cam.ac.uk).

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