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84869352134
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This complex crystallizes as 1.4MeCN. Crystallographic data for the complex: C80H100C14Cu2N 20O16, Mr=1866.70, monoclinic, space group C2/c (No. 15, a=25.805 (4, b=13.152 (2, c=29.799 (5) Å, β=117.737 (5) °, V=8951 (3) Å3, Z=4, Dcalcd=1.385 g cm -3, μ (MoKα)=0.706 mm-1, T=293 K. λ=0.7107 Å, ω scan. Of a total of 32288 reflections collected, 8328 were independent (Rint=0.042, The structure was solved by direct methods and refined by full-matrix least squares on F. Final R1 [I > 2σ (I, 0.0984 and wR2=0.1578 all data, GOF=1.498. CCDC 715771
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int=0.042). The structure was solved by direct methods and refined by full-matrix least squares on F. Final R1 [I > 2σ (I)]=0.0984 and wR2=0.1578 (all data) ; GOF=1.498. CCDC 715771.
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67650377063
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Supporting Information is available electronically on the CSJ-Journal Web site, http://www.csj.jp/journals/chem-lett/index.html.
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Supporting Information is available electronically on the CSJ-Journal Web site, http://www.csj.jp/journals/chem-lett/index.html.
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84869353593
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