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Volumn 38, Issue 7, 2009, Pages 712-713

Phenanthroline derivatives for electron-transport layer in organic light-emitting devices

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EID: 67650484548     PISSN: 03667022     EISSN: 13480715     Source Type: Journal    
DOI: 10.1246/cl.2009.712     Document Type: Article
Times cited : (13)

References (10)
  • 8
    • 33646115990 scopus 로고    scopus 로고
    • Organic Synthesis via Boranes
    • Aldrich Chemical Company, Milwaukee
    • A. Suzuki, H. C. Brown, Organic Synthesis via Boranes, vol. 3, Suzuki coupling, Aldrich Chemical Company, Milwaukee, 2003.
    • (2003) Suzuki coupling , vol.3
    • Suzuki, A.1    Brown, H.C.2
  • 10
    • 84869344403 scopus 로고    scopus 로고
    • A mixture of 2a (2.1 g, 6.67 mmol, 3 (2.3 g, 13.3 mmol, and saturated ethanolic KOH (1.0 g) in absolute ethanol (20 mL) was heated, and refluxed under nitrogen gas for 24 h. The solvent was evaporated, and the residue was purified by chromatography on silica gel, eluting with CHCl 3/EtOAc (1:1, to provide 1.8 g (46, of Phen 1. 1H NMR (CDCl3, 500 MHz, δ 7.62-7.70 (m, 5H, 7.77-7.87 (m, 8H, 8.09 (s, 1H, 8.21 (d, J=8.0 Hz, 2H, 8.27 (d, J=8.5 Hz, 2H, 8.35 (d, J=8.0 Hz, 2H, 8.42 (d, J=8.0 Hz, 2H, 8.55 (s, 2H, 9.22 (d, J=4.5 Hz, 2H, 13C NMR (CDCl3, 125 MHz, δ 120.98, 122.92, 126.35, 126.39, 126.60, 126.86, 127.41, 127.65, 128.41, 129.09, 129.19, 129.35, 136.06, 136.91, 140.39, 141.79, 141.83, 146.19, 146.46, 150.44, 157.70. MS EI, m/z 587 [M
    • +.


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