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Crystal data for 1 · 2SbCl3:C10H 14Cl6S2Sb, Mr, 654.53 0.32 × 0.28 × 0.22 mm, monoclinic, P 21/c, a, 7.5028(5) Å, b, 9.2150(6) Å, c, 14.6331(10) Å, β, 101.955(1)°, V, 989.76(11) Å3, Z, 2, Z′, 0.5, Fcalcd, 2.196 g cm-3, μ, 3.737 mm-1, 2θmax, 54.00°, T, 173(2) K, 10898 reflections collected, 2165 reflections independent [Rint, 0.0220, 95 parameters R1, 0.0207, wR2, 0.0505 for reflections with I > 2σI, and R1, 0.0217, wR2, 0.0512 for all data, GOF, 1.059, max/min residual electron density +1.217/-0.535 eÅ-3
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-3.
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1542637833
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Robertson, K.N.5
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84869338610
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Crystal data for 2 · 2SbCl3:C10H 12Br2Cl6Sb2, Mr, 748.22 0.42 × 0.24 × 0.12 mm, monoclinic, P 2 1/c, a, 7.6386(4) Å, b, 16.1453(9) Å, c, 8.1907(5) Å, β, 105.532(1)°, V, 937.25(10) Å3, Z, 2, Z′, 0.5, F calcd, 2.553 g cm-3, μ, 7.692 mm-1, 2θmax, 54.00°, T, 173(2) K, 10642 reflections collected, 2117 reflections independent [Rint, 0.0337, 92 parameters R1, 0.0185, wR2, 0.0463 for reflections with I > 2σI, and R1, 0.0189, wR2, 0.0466 for all data, GOF, 1.130, max/min residual electron density +0.710/-0.642 eÅ-3
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