3D HSQC-HSQMBC - Increasing the resolution of long-range proton-carbon correlation experiments

Journal of Magnetic Resonance

Volumn 159, Issue 2, 2002, Pages 145-150

  Uhrín, Dušan ^a  

^a UNIVERSITY OF EDINBURGH   (United Kingdom)

Author keywords

3D; Carbohydrates; HSQMBC; Proton carbon long range correlation

Indexed keywords

CARBON; POLYSACCHARIDE; PROTON;

ARTICLE; CHEMISTRY; METHODOLOGY; NUCLEAR MAGNETIC RESONANCE;

CARBON; NUCLEAR MAGNETIC RESONANCE, BIOMOLECULAR; POLYSACCHARIDES; PROTONS;

EID: 0036923591     PISSN: 10907807     EISSN: None     Source Type: Journal    
DOI: 10.1016/S1090-7807(02)00018-6     Document Type: Article

References (17)

1. L. Müller, Sensitivity enhanced detection of weak nuclei using multiple-quantum coherence, J. Am. Chem. Soc. 101 (1979) 4481-4484.
2. G. Bodenhausen, D.J. Ruben, Natural abundance nitrogen-15 NMR by enhanced heteronuclear spectroscopy, Chem. Phys. Lett. 69 (1980) 185-189.
3. nJ(C,H) heteronuclear coupling constants in small molecules, Magn. Reson. Chem. 39 (2001) 499-530.
4. 13C scalar correlation at natural abundance: Application to oligosaccharide analysis, Magn. Reson. Chem. 40 (2002) 169-174
5. 15N correlations in proteins, J. Am. Chem. Soc. 112 (1990) 9638-9640.
6. D. Uhrín, A. Mele, J. Boyd, M.R. Wormald, R.A. Dwek, New methods for measurement of long-range proton-carbon coupling-constants in oligosaccharides, J. Magn. Reson. 97 (1992) 411-418.
7. K.V.R. Chary, G. Otting, K. Wütrich, J. Magn. Reson. 93 (1991) 218-224.
8. 1H-detected measurement of long-range heteronuclear coupling constants. Application to a trisaccharide, J. Magn. Reson. 92 (1991) 636-641.
9. 13C coupling constants using selective excitation of carbon-13, J. Magn. Reson. A 103 (1993) 97-102.
10. 1 noise, J. Magn. Reson. B 109 (1995) 326-328.
11. R.T. Williamson, B.L. Marquez, W.H. Gerwick, K.E. Kövér, One- and two-dimensional gradient-selected HSQMBC NMR experiments for the eOcient analysis of long-range heteronuclear coupling constants, Magn. Reson. Chem. 38 (2000) 265-273.
12. J.R. Garbow, D.P. Weitekamp, A. Pines, Bilinear rotation decoupling of homonuclear scalar interactions, Chem. Phys. Lett. 93 (1982) 504-509.
13. A. Bax, Broad-band homonuclear decoupling in heteronuclear shift correlation NMR spectroscopy, J. Magn. Reson. 53 (1983) 517-520.
14. G. Mackin, A.J. Shaka, Phase-sensitive two-dimensional HMQC and HMQC-TOCSY spectra obtained using double pulsed-field-gradient spin echoes, J. Magn. Reson. A 118 (1996) 247-255.
15. 1) half-filtered TOCSY experiment for measuring long-range heteronuclear coupling constants, J. Magn. Reson. 130 (1998) 155-161.
16. A. Bax, S.S. Pochapsky, Optimized recording of heteronuclear multidimensional NMR spectra using pulsed field gradients, J. Magn. Reson. 99 (1992) 638-643.
17. M.A. Smith, H. Hu, A.J. Shaka, Improved broadband inversion performance for NMR in liquids, J. Magn. Reson. 151 (2001) 269-283.