A practical guide for analysis of nanoindentation data

Journal of the Mechanical Behavior of Biomedical Materials

Volumn 2, Issue 4, 2009, Pages 396-407

  Oyen, Michelle L ^a   Cook, Robert F ^b  

^a UNIVERSITY OF CAMBRIDGE   (United Kingdom)

^b NATIONAL INSTITUTE OF STANDARDS AND TECHNOLOGY   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

DEFORMATION MODES; ELASTIC PLASTICS; EXPERIMENTAL TESTS; FRACTURE BEHAVIORS; HOMOGENEOUS DEFORMATIONS; INDENTATION TESTS; LOAD DISPLACEMENTS; NANOINDENTATION TESTING; PRACTICAL GUIDES;

BRITTLE FRACTURE; DEFORMATION; MATERIALS PROPERTIES; MATERIALS TESTING; MECHANICAL PROPERTIES; NANOINDENTATION; PLASTICS;

BIOLOGICAL MATERIALS;

BIOMATERIAL;

ARTICLE; ELASTICITY; FRACTURE; HARDNESS; MATERIALS TESTING; NANOINDENTATION TECHNIQUE; PLASTICITY; PRIORITY JOURNAL; VISCOSITY; WEIGHT BEARING;

BIOMECHANICS; DATA INTERPRETATION, STATISTICAL; HARDNESS TESTS; HUMANS; NANOTECHNOLOGY; TIME FACTORS;

EID: 67349238321     PISSN: 17516161     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.jmbbm.2008.10.002     Document Type: Article

References (56)

1. Agbezuge L.K., and Deresiewicz H. On the indentation of a consolidating half-space. Israel J. Technol. 12 (1974) 322-338
2. Anstis G.R., Chantikul P., Lawn B.R., and Marshall D.B. A critical evaluation of indentation techniques for measuring fracture toughness. 1. Direct crack measurements. J. Am. Ceram. Soc. 64 (1981) 533-538
3. Ashby M.F. Materials Selection in Mechanical Design. 2nd ed. (1999), Butterworth-Heinemann, Oxford, UK
4. Bembey A.K., Bushby A.J., Boyde A., Ferguson V.L., and Oyen M.L. Hydration effects on the micro-mechanical properties of bone. J. Mater. Res. 21 (2006) 1962-1968
5. Bruet B.J.F., Qi H.J., Boyce M.C., Panas R., Tai K., Frick L., and Ortiz C. Nanoscale morphology and indentation of individual nacre tablets from the gastropod mollusc Trochus niloticus. J. Mater. Res. 20 (2005) 2400-2419
6. Bushby A.J. Nano-indentation using spherical indenters. Non-Destruct. Test. Eval. 17 (2001) 213-234
7. Cheng Y.-T., Ni W., and Cheng C.-M. Nonlinear analysis of oscillatory indentation in elastic and viscoelastic solids. Phys. Rev. Lett. 97 (2006) 075506
8. Constantinides G., Ravi Chandran K.S., Ulm F.-J., and Van Vliet K.J. Grid indentation analysis of composite microstructure and mechanics: Principles and validation. Mater. Sci. Eng. A 430 (2006) 189-202
9. Cook R.F., and Pharr G.M. Direct observation and analysis of indentation cracking in glasses and ceramics. J. Am. Ceram. Soc. 73 (1990) 787-817
10. Cook R.F., and Oyen M.L. Nanoindentation behavior and mechanical properties measurement of polymeric materials. Int. J. Mater. Res. 98 (2007) 370-378
11. Doerner M.F., and Nix W.D. A method for interpreting the data from depth-sensing indentation instruments. J. Mater. Res. 1 (1986) 601-609
12. Feng G., and Ngan A.H.W. Effects of creep and thermal drift on modulus measurement using depth-sensing indentation. J. Mater. Res. 17 (2002) 660-668
13. Field J.S., and Swain M.V. A simple predictive model for spherical indentation. J. Mater. Res. 8 (1993) 297-306
14. Findley W.N., Lai J., and Onaran K. Creep and Relaxation of Nonlinear Viscoelastic Materials (1989), Dover Books, New York
15. Hayes W.C., and Mockros L.F. Viscoelastic properties of human articular cartilage. J. Appl. Physiol. 31 (1971) 562-568
16. Herbert E.G., Oliver W.C., and Pharr G.M. Nanoindentation and the dynamic characterization of viscoelastic solids. J. Phys. D. Appl. Phys 41 (2008) 074021
17. Huang C.Y., Mow V.C., and Ateshian G.A. The role of flow-independent viscoelasticity in the biphasic tensile and compressive responses of articular cartilage. J. Biomech. Eng. 123 (2001) 410-417
18. Huang G., Wang B., and Lu H. Measurements of viscoelastic functions of polymers in the frequency-domain using nanoindentation. Mech. Time-Dep. Mater. 8 (2004) 345-364
19. Johnson K.L. Contact Mechanics (1985), Cambridge University Press, Cambridge, UK
20. Kendall K. The impossibility of comminuting small particles by compression. Nature 272 (1978) 710-711
21. Lawn B.R., Jensen T., and Arora A. Brittleness as an indentation size effect. J. Mater. Sci. 11 (1976) 573-575
22. Lawn B.R., Evans A.G., and Marshall D.B. Elastic-plastic indentation damage in ceramics-the median-radial crack system. J. Amer. Ceram. Soc. 63 (1980) 574-581
23. Lawn B.R. Fracture of Brittle Solids. 2nd ed. (1993), Cambridge Univ. Press, Cambridge, UK
24. Lee E.H., and Radok J.R.M. Contact problem for viscoelastic bodies. J. Appl. Mech. 27 (1960) 438-444
25. Low I.M., Che Z.Y., and Latella B.A. Mapping the structure, composition and mechanical properties of bamboo. J. Mater. Res. 21 (2006) 1969-1976
26. Mak W.L., and Mow V. Biphasic indentation of articular cartilage-I. Theoretical analysis. J. Biomechanics 20 (1987) 703-714
27. Mattice J.M., Lau A.G., Oyen M.L., and Kent R.W. Spherical indentation load-relaxation of soft biological tissues. J. Mater. Res. 21 (2006) 2003-2010
28. Marshall Jr. G.W., Balooch M., Gallagher R.R., Gansky S.A., and Marshall S.J. Mechanical properties of the dentinoenamel junction: AFM studies of nanohardness, elastic modulus, and fracture. J. Biomed. Mater. Res. 54 (2001) 87-95
29. Morris D.J., Myers S.B., and Cook R.F. Sharp probes of varying acuity: Instrumented indentation and fracture behavior. J. Mater. Res. 19 (2004) 165-175
30. Morris D.J., and Cook R.F. Radial fracture during indentation by acute probes: I, description by an indentation wedging model. Int. J. Frac. 136 (2005) 237-264
31. Morris D.J., Vodnick A.M., and Cook R.F. Radial fracture during indentation by acute probes: II, experimental observations of cube corner and Vickers indentation. Int. J. Fracture 136 (2005) 265-284
32. Oliver W.C., and Pharr G.M. Improved technique for determining hardness and elastic modulus using load and displacement sensing indentation experiments. J. Mater. Res. 7 (1992) 1564-1583
33. Oliver D.J., Lawn B.R., Cook R.F., Reitsma M.G., Bradby J.E., Williams J.S., and Munroe P. Giant pop-ins in nanoindented silicon and germanium caused by lateral cracking. J. Mater. Res. 23 (2008) 297-301
34. Oyen M.L., and Cook R.F. Load-displacement behavior during sharp indentation of viscous-elastic-plastic materials. J. Mater. Res. 18 (2003) 139-150
35. Oyen M.L. Spherical indentation creep following ramp loading. J. Mater. Res. 20 (2005) 2094-2100
36. Oyen M.L. Nanoindentation hardness measurements of mineralized tissues. J. Biomech. 39 (2006) 2699-2702
37. Oyen M.L. Analytical techniques for indentation of viscoelastic materials. Phil. Mag. 86 (2006) 5625-5641
38. Oyen M.L. Sensitivity of polymer nanoindentation creep properties to experimental variables. Acta Mater. 55 (2007) 3633-3639
39. Oyen M.L., and Ko C.-C. Examination of local variations in viscous, elastic, and plastic indentation responses in healing bone. J. Mater. Sci. Mater. Med. 18 (2007) 623-628
40. Oyen M.L., and Bushby A.J. Viscoelastic effects in small-scale indentation of biological materials. Int. J. Surface Sci. Eng. 1 (2007) 180-197
41. Oyen M.L. The materials science of bone: Lessons from nature for biomimetic materials synthesis. Mater. Res. Soc. Bull. 33 (2008) 49-55
42. Oyen M.L. Poroelastic nanoindentation responses of hydrated bone. J. Mater. Res. 23 (2008) 1307-1314
43. Oyen M.L., Cook R.F., Moody N.R., and Emerson J.A. Indentation responses of time-dependent films on stiff substrates. J. Mater. Res. 19 (2004) 2487-2497
44. Oyen M.L., and Ko C.C. Indentation variability of natural nanocomposite materials. J. Mater. Res. 23 (2008) 760-767
45. Rar A., Song H., and Pharr G.M. Assessment of new relation for the elastic compliance of a film-substrate system. In: Ozkan C.S., Freund L.B., Cammarata R.C., and Gao H. (Eds). Thin Films: Stresses and Mechanical Properties IX (2002) 431 (Mater. Res. Soc. Symp. Proc. 695, Warrendale, PA paper L10.10.1)
46. Sakai M. The Meyer hardness: A measure for plasticity?. J. Mater. Res. 14 (1999) 3630-3639
47. Selvadurai A.P.S. Stationary damage modeling of poroelastic contact. Int. J. Solids Struct. 41 (2004) 2043-2064
48. Sneddon I.N. The relation between load and penetration in the axisymmetric Boussinesq problem for a punch of arbitrary profile. Int. J. Engng. Sci. 3 (1965) 47-57
49. Swadener J.G., Rho J.-Y., and Pharr G.M. Effects of anisotropy on elastic moduli measured by nanoindentation in human tibial cortical bone. J. Biomed. Mater. Res. 57 (2001) 108-112
50. Tabor D. The Hardness of Metals Oxford University Press (1951), Clarendon Press, London, UK
51. Thurn J., Morris D.J., and Cook R.F. Depth-sensing indentation at macroscopic dimensions. J. Mater. Res. 17 (2002) 2679-2690
52. Toivola Y., Thurn J., and Cook R.F. Structure, electrical and mechanical properties development during curing of low-k hydrogen silsesquioxane films. J. Electrochem. Soc. 149 (2002) F9-F17
53. Wang H.F. Theory of Linear Poroelasticity with Applications to Geomechanics and Hydrogeology (2000), Princeton University Press, New Jersey
54. Xu H.H., Smith D.T., Jahanmir S., Romberg E., Kelly J.R., Thompson V.P., and Rekow E.D. Indentation damage and mechanical properties of human enamel and dentin. J. Dent. Res. 77 (1998) 472-480
55. Zhang C.Y., Zhang Y.W., Zeng K.Y., and Shen L. Nanoindentation of polymers with a sharp indenter. J. Mater. Res. 20 (2005) 1597-1605
56. Zhao M., Srinivasan C., Burgess D.J., and Huey B.D. Rate- and depth-dependent nanomechanical behavior of individual living Chinese hamster ovary cells probed by atomic force microscopy. J. Mater. Res. 21 (2006) 1906-1912