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Volumn 48, Issue 12, 2009, Pages 5403-5411

Centric and non-centric Ca 3Au ∼7.5Ge ∼3.5: Electron-poor derivatives of La 3AI 11· syntheses, structures, and bonding analyses

(2) Lin, Qisheng a,b Corbett, John D a,b

a IOWA STATE UNIVERSITY (United States)

b IOWA STATE UNIVERSITY (United States)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 67149144585 PISSN: 00201669 EISSN: None Source Type: Journal
DOI: 10.1021/ic900383d Document Type: Article

Times cited : (15)

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- Reactions with nominal CaAux. Ge4-x compositions (x, 1.33, 2.0, 2.67, and 3.33) were run to check for the presence of coloring problems (see text) with CaAu2Gc2. Powder diffraction analyses revealed that CaAu2Ge2 (ThCr2Si2 type)phase occurs only for x ≤ 2.0. The refined lattice parameters (a, 4.4407(9) Å, c, 10.266(2) Å) showed no change (within 2σ) between x, 2.0 and x, 1.33, indicating a line compound. Single crystal diffraction on a stoichiometric reaction product converged at R1, 1.59, wR2, 3.65, GOF, 1.206. The Ca and Au atoms were refined on the Wyckoff 2a and 4d special positions, respectively, and Ge. on 4e with x, 0.3817(1, These basically agree with, but improve on, the literature data [a, 4.43(2, c, 10.232, zGe, 0.379, which were obtained without absorption corrections.35
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