Donor-dictated interlocking co-complexation reactions of LiNHDipp with dimethylzinc: Synthesis and structures of new methyl(amido)zincates

Inorganic Chemistry

Volumn 48, Issue 12, 2009, Pages 5320-5327

  Clegg, William ^b   Graham, David V ^a   Herd, Emma ^a   Hevia, Eva ^a   Kennedy, Alan R ^a   McCall, Matthew D ^a   Russo, Luca ^b  

^a UNIVERSITY OF STRATHCLYDE   (United Kingdom)

^b NEWCASTLE UNIVERSITY   (United Kingdom)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 67149107493     PISSN: 00201669     EISSN: None     Source Type: Journal    
DOI: 10.1021/ic900313b     Document Type: Article

References (35)

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34. The presence of a dynamic process in solution was confirmed by a variable temperature NMR study, which shows that the relevant resonance for the methyl groups of 5 (at -0.33 ppm at T = 300 K in deuterated toluene) splits into two singlets (at 0.15 and 0.05 ppm, relative integration 2:1) when the temperature is decreased to 208 K.
35. 3].