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Crystallographic details for 1-0.5H2O(C34H33Br2N8NiOa5, colorless rods, 0.24 X 0.06 X 0.04 mm, space group P21/n, mo- noclinic, a, 11.8792(15) A, b, 10.0604(14) A, c, 13.9968(19) A, b, 97.895(4)°, V, 1656.9(4) A3, Z =2, />calcd, 1.564 mg/m3, F(000, 790, R(F, 0.0877, Rw(F2, 0.1481, GOF =1.141 [I > 2CTI
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Crystallographic details for 1-0.5H2O(C34H33Br2N8NiOa5): colorless rods, 0.24 X 0.06 X 0.04 mm, space group P21/n, mo- noclinic, a = 11.8792(15) A, b = 10.0604(14) A, c = 13.9968(19) A, b = 97.895(4)°, V = 1656.9(4) A3, Z =2, />calcd = 1.564 mg/m3, F(000)= 790, R(F) = 0.0877, Rw(F2) = 0.1481, GOF =1.141 [I > 2CT(I)].
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85153212939
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Crystallographic details for 2-dmf (C22H27Br2N5NiO, brown blocks, 0.16 X 0.16 X 0.10 mm, space group P212121, ortho- rhombic, a, 8.1304(4) A, b, 15.8139(8) A, c, 18.7790(10) A, V, 2414.5(2) A3, Z =4, />calcd, 1.640 mg/m3, F(000, 1200, R(F, 0.0619, Rw(F2, 0.1444, GOF, 1.143 [I > 2CTI
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Crystallographic details for 2-dmf (C22H27Br2N5NiO): brown blocks, 0.16 X 0.16 X 0.10 mm, space group P212121, ortho- rhombic, a = 8.1304(4) A, b = 15.8139(8) A, c = 18.7790(10) A, V = 2414.5(2) A3, Z =4, />calcd = 1.640 mg/m3, F(000)= 1200, R(F) = 0.0619, Rw(F2) = 0.1444, GOF = 1.143 [I > 2CT(I)].
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