Large-scale separation of clavine alkaloids from Ipomoea muricata by pH-zone-refining centrifugal partition chromatography

Journal of Chromatography B: Analytical Technologies in the Biomedical and Life Sciences

Volumn 877, Issue 18-19, 2009, Pages 1732-1736

  Maurya, Anupam ^a   Srivastava, Santosh Kumar ^a  

^a CSIR CENTRAL INSTITUTE OF MEDICINAL AND AROMATIC PLANTS   (India)

Author keywords

Chanoclavine; Ipomoea muricata; Lysergol; pH zone refining centrifugal partition chromatography; Preparative chromatography

Indexed keywords

AQUEOUS MOBILE PHASE; CENTRIFUGAL PARTITION CHROMATOGRAPHY; CHANOCLAVINE; CRUDE EXTRACT; IPOMOEA MURICATA; LARGE-SCALE SEPARATION; LYSERGOL; METHYL TERT BUTYL ETHER; PREPARATIVE CHROMATOGRAPHY; STATIONARY PHASE; TOTAL YIELD; TRIETHYLAMINE; TRIFLUOROACETIC ACIDS; TWO-PHASE SOLVENT SYSTEM;

ACETONITRILE; CENTRIFUGATION; CHROMATOGRAPHY; ETHERS; REFINING;

CHROMATOGRAPHIC ANALYSIS;

ACETONITRILE; ALKALOID DERIVATIVE; CHANOCLAVINE; LYSERGOL; PLANT EXTRACT; SOLVENT; TERT BUTYL METHYL ETHER; TRIETHYLAMINE; TRIFLUOROACETIC ACID; UNCLASSIFIED DRUG; WATER;

ARTICLE; CARBON NUCLEAR MAGNETIC RESONANCE; CENTRIFUGATION; DRUG ISOLATION; ELECTROSPRAY MASS SPECTROMETRY; IPOMOEA MURICATA; MEDICINAL PLANT; PARTITION CHROMATOGRAPHY; PH; PLANT SEED; PRIORITY JOURNAL; PROTON NUCLEAR MAGNETIC RESONANCE;

ACETONITRILES; CHROMATOGRAPHY, LIQUID; COUNTERCURRENT DISTRIBUTION; ERGOT ALKALOIDS; HYDROGEN-ION CONCENTRATION; IPOMOEA; METHYL ETHERS;

IPOMOEA;

EID: 66149090799     PISSN: 15700232     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.jchromb.2009.04.036     Document Type: Article

References (28)

1. Charles I., Abou-Chaar, and George A.D. Nature 212 (1966) 618
2. G. Ferrari, Process for the preparation of polyhydroxylated steroids, lysergol and ergolinic alkaloids, US Patent 4,198,344 (1980).
3. G. Ferrari, Method for the extraction of lysergol and ergot alkaloids from plants of the ipomoea genus, US Patent 3,920,663 (1975).
4. S.P.S. Khanuja, J.S. Arya, S.K. Srivastava, A.K. Shasany, T.R. Shanta Kumar, M.P. Darokar, S. Kumar, US Patent 2,003,081,425 (2003).
5. Ashford S.W., Henegar K.E., Anderson A.M., and Wuts P.G.M. J. Org. Chem. 67 (2002) 7147
6. Hofmann A. Experientia 16 (1960) 414
7. D. Wilke, A. Weber, Process for the preparation of chanoclavine, US Patent 4,968,610 (1990).
8. Renault J.-H., Nuzillard J.-M., Crouerour G.L., Thepenier P., Zeches-Hanrot M., and Men-Olivier L.L. J. Chromatogr. A 849 (1999) 421
9. In: Foucault A.P. (Ed). Chromatographic Science Series vol. 68 (1994), Marcel Dekker, New York
10. Foucault A.P., and Chevolot L. J. Chromatogr. A 808 (1998) 3
11. Renault J.-H., Ghédira K., Thépenier P., Lavaud C., Zèches-Hanrot M., and Le Men-Olivier L. Phytochemistry 44 (1997) 1321
12. Wang X., Geng Y., Li F., Shi X., and Liu J. J. Chromatogr. A 1115 (2006) 267
13. Y. Ito, A. Weisz, pH-zone-refining countercurrent chromatography, US Patent 5,332,504 (1994).
14. Weisz A., Scher A.L., Shinomiya K., Fales H.M., and Ito Y. J. Am. Chem. Soc. 116 (1994) 704
15. Ito Y., Shinomiya K., Fales H.M., Weisz A., and Scher A.L. In: Conway W.D., and Petroski R.J. (Eds). ACS Symposium Series vol. 593 (1995), American Chemical Society, Washington, DC 154
16. Ito Y. In: Ito Y., and Conway W.D. (Eds). High-Speed Countercurrent Chromatography (1996), Wiley, New York 121
17. Wang X., Geng Y., Li F., Gao Q., and Shi X. J. Chromatogr. A 1103 (2006) 166
18. Ma Y., Ito Y., Sokoloski E., and Fales H.M. J. Chromatogr. A 685 (1994) 259
19. Ma Y., Ito Y., Torok D.S., and Ziffer H. J. Liquid Chromatogr. 17 (1994) 3507
20. Denekamp C., Mandelbaum A., Weisz A., and Ito Y. J. Chromatogr. A 685 (1994) 253
21. Weisz A., Scher A.L., and Ito Y. J. Chromatogr. A 732 (1996) 283
22. Ma Y., and Ito Y. J. Chromatogr. A 678 (1994) 233
23. Weisz A., Mazzola E.P., Murphy C.M., and Ito Y. J. Chromatogr. A 966 (2002) 111
24. Ma Y., Ito Y., and Foucault A. J. Chromatogr. A 704 (1995) 75
25. Srivastava S.K., Desai H.K., Vobalaboina V., and Pelletier S.W. J. Liquid Chromatogr. Relat. Technol. 22 (1999) 1687
26. Ito Y. J. Chromatogr. A 1065 (2005) 145
27. Flieger M., Kren V., Zelenkova N.F., Sedmera P., Novak J., and Sajdl P. J. Nat. Prod. 53 (1990) 171
28. Kren V., Olsovsky P., Havlicek V., Sedmera P., Witvrouw M., and Clercq E.D. Tetrahedron 53 (1997) 4503