A nonanuclear organostiboxane cage

Organometallics

Volumn 28, Issue 8, 2009, Pages 2637-2639

  Chandrasekhar, Vadapalli ^a   Thirumoorthi, Ramalingam ^a  

^a INDIAN INSTITUTE OF TECHNOLOGY KANPUR   (India)

Author keywords

[No Author keywords available]

Indexed keywords

BOND CLEAVAGE REACTION;

EID: 65649143466     PISSN: 02767333     EISSN: None     Source Type: Journal    
DOI: 10.1021/om900113q     Document Type: Article

References (31)

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23. Crystal data for 1: triclinic; PI; a = 10.8548(17) A, b = 12.1442(19) A, c = 19.956(3) A; a = 95.080(3)°, = 99.305(3)°, y = 103.353(2)°; V = 2504.1(7) A3, T = 273(2) K, Z = 2; pcaicd = 1.422 g cm-3; crystal dimensions 0.2 x 0.2 x 0.1 mm; 20max = 25.00; 13 051 reflections measured; 8680 unique reflections; 564 parameters; R1 = 0.0428; wR2 = 0.1071. Crystal data for 2: monoclinic; P2/n; a = 15.420(3) A, b = 15.122(3) A, c = 25.599(5) A;/5 = 92.52(3)°; V = 5963(2) A3, T = 100(2) K, Z = 2; pcalcd = 1.692 g cm-3; crystal dimensions 0.3 x 0.2 x 0.2 mm; 2#max = 25.00; 30 217 reflections measured; 10 482 unique reflections; 630 parameters; R1 = 0.0395; wR2 = 0.0981. CCDC 716145 and 716146 contain the crystallographic data for this publication.
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