Electrocatalytic activity mapping of model fuel cell catalyst films using scanning electrochemical microscopy

Electrochimica Acta

Volumn 54, Issue 19, 2009, Pages 4525-4533

  Nicholson, P G ^a   Zhou, S ^a   Hinds, G ^a   Wain, A J ^a   Turnbull, A ^a  

^a NATIONAL PHYSICAL LABORATORY   (United Kingdom)

Author keywords

Catalysts; Fuel cells; Hydrogen oxidation; Platinum nanoparticles; SECM

Indexed keywords

ANODE REACTIONS; CARBON MASS; CARBON NANOPARTICLES; CARBON PARTICLES; CATALYST FILMS; CHARACTERISATION; ELECTRO-CATALYTIC ACTIVITIES; FIELD EMISSION-SCANNING ELECTRON MICROSCOPIES; FUEL-CELL CATALYSTS; HYDROGEN OXIDATION; HYDROGEN OXIDATION REACTIONS; MONO-DISPERSED; PHYSICAL CHARACTERISATION; PLATINUM NANOPARTICLES; SCANNING ELECTROCHEMICAL MICROSCOPIES; SECM; TYPE STRUCTURES;

CARBON CLUSTERS; CARBON FILMS; CATALYSTS; CELL MEMBRANES; ELECTROCATALYSIS; ELECTROCHEMICAL SENSORS; HYDROGEN; NANOPARTICLES; OXIDATION; PLATINUM; PROTON EXCHANGE MEMBRANE FUEL CELLS (PEMFC); SCANNING; SCANNING ELECTRON MICROSCOPY; SCANNING PROBE MICROSCOPY; TRANSMISSION ELECTRON MICROSCOPY;

PLATINUM COMPOUNDS;

EID: 65549123066     PISSN: 00134686     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.electacta.2009.03.021     Document Type: Article

References (23)

1. Stamenkovic V.R., Fowler B., Mun B.S., Wang G., Ross P.N., Lucas C.A., and Markovic N.M. Science 315 (2007) 493
2. In: Bard A.J., and Mirkin M.V. (Eds). Scanning Electrochemical Microscopy (2001), Marcel Dekker, New York
3. In: P. Unwin (Ed.), Instrumentation and Electroanalytical Chemistry, vol. 3, Encyclopaedia of Electrochemistry, in: A.J. Bard, M. Stratmann (Eds.), Wiley-VCH, Weinheim, 2003.
4. A. Turnbull, Electrochemical Scanning Probe Microscopy - An Overview, NPL Report DEPC MPE 011, 2005.
5. Kucernak A.R., Chowdhury P.B., Wilde C.P., Kelsall G.H., Zhu Y.Y., and Williams D.E. Electrochim. Acta 45 (2000) 4483
6. Shah B.C., and Hillier A.C. J. Electrochem. Soc. 147 (2000) 3043
7. Jayaraman S., and Hillier A.C. Langmuir 17 (2001) 7857
8. Kallio T., Slevin C., Sundholm G., Holmlund P., and Kontturi K. Electrochem. Commun. 5 (2003) 565
9. Jayaraman S., and Hillier A.C. J. Phys. Chem. B 107 (2003) 5230
10. Jayaraman S., and Hillier A.C. J. Comb. Chem. 6 (2004) 27
11. Black M., Cooper J., and McGinn P. Meas. Sci. Technol. 16 (2005) 182
12. Lu G., Cooper J.S., and McGinn P.J. J. Power Sources 161 (2006) 114
13. Fernandez J.L., and Bard A.J. Anal. Chem. 75 (2005) 2974
14. Fernandez J.L., Walsh D.A., and Bard A.J. J. Am. Chem. Soc. 127 (2005) 365
15. Walsh D.A., Fernandez J.L., and Bard A.J. J. Electrochem. Soc. 153 (2006) E103
16. Eckhard K., Chen X., Turcu F., and Schuhmann W. Phys. Chem. Chem. Phys. 8 (2006) 5365
17. Eckhard K., and Schuhmann W. Electrochim. Acta 53 (2007) 1169
18. Lu G., Cooper J.S., and McGinn P.J. Electrochim. Acta 52 (2007) 5181
19. Nicholson P. On the Fabrication of Model Proton Exchange Membrane Fuel Cell Catalyst Films vol. 3 (2008), NPL, MN
20. Moore R.R., Banks C.E., and Compton R.G. Anal. Chem. 76 (2004) 2682
21. Kwak J., and Bard A.J. Anal. Chem. 61 (1989) 1227
22. P. Nicholson, S. Zhou, G. Hinds, A. Turnbull, Application of SECM to the characterisation of the activity of catalysts used in PEM fuel cells, NPL Report MAT 20, 2008.
23. Deuflhard P. Newton Methods for Nonlinear Problems. Affine Invariance and Adaptive Algorithms. Springer Series in Computational Mathematics vol. 35 (2004), Springer, Berlin