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65449134130
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-1))
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B at 298 K.
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65449119758
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Crystal data for [Cu(Fc-met)(phen, PF6, C28H 28CuF6FeN3O2PS, M, 734.97, triclinic, P1, a, 10.790(5) Å, b= 11.048(5) Å, c, 14.823(5) Å, α, 68.657(5, β, 85.234(5, γ, 64.677(5)°, V, 1482.1(11) Å3, Z, 2. ρ, 1.647 g cm-3. T= 293(2) K, 1.48 ≤ θ ≤ 25° μ, 14.01 cm-1. F(000, 746, GOF =1.004, R1, 0.0538, wR2, 0.1333 for 7444 reflections with I > 2σ (I) and 775 parameters (R1(F2, 0.0712 (all data, w, σ2(Fo2, 0.0904P) 2, 0.0000P]-1, where P, Fo 2, 2Fc2]/3 Bruker SMART APEX CCD diffractometer with Mo Kα X-ray source, The structure was solved and refined using
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2]/3 (Bruker SMART APEX CCD diffractometer with Mo Kα X-ray source). The structure was solved and refined using the SHELX program: Sheldrick, G. M. SHELX-97, Programs for Crystal Structure Solution and Refinement; University of Göttingen, Göttingen, Germany, 1997.
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84961985222
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Roy, M.1
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Jemmis, E.D.4
Nethaji, M.5
Chakravarty, A.R.6
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24
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65449134556
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2 1.8 Pγ 10% mm, beam divergence 0.7 Pγ 10% mrad) and a CW He-Ne Laser of Research Electro-Optics made for 633 nm (12 mW, beam diameter of 0.88 mm, beam divergence of 0.92 mrad). The complex and reagent concentrations corresponded to those in the 20 μL sample solution path length 5 mm). The percentage of DNA cleavage was measured from the band intensities in agarose gels using the UVITECH Gel Documentation System.
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2 1.8 Pγ 10% mm, beam divergence 0.7 Pγ 10% mrad) and a CW He-Ne Laser of Research Electro-Optics made for 633 nm (12 mW, beam diameter of 0.88 mm, beam divergence of 0.92 mrad). The complex and reagent concentrations corresponded to those in the 20 μL sample volume (solution path length 5 mm). The percentage of DNA cleavage was measured from the band intensities in agarose gels using the UVITECH Gel Documentation System.
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25
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0038141911
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Patra, A. K.; Dhar, S.; Nethaji, M.; Chakravarty, A. R. Chem. Commun. 2003, 1562-1563.
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Patra, A.K.1
Dhar, S.2
Nethaji, M.3
Chakravarty, A.R.4
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