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single crystal X-ray diffraction data for UoC-2: triclinic, space group P1̄, a=21.4410(2, b, 23.212(2, c=24.646(3) Å, α, 68.103(7, β=67.490(7, λ, 79.993(7)°, V=10507.0(2) Å3, Z=2, p calcd= 0.622 gcm-3, μ=0.757 mm-1, T=100.0(3) K, 2θmax=40°. Refinement of 1011 parameters on 19544 independent reflections out of 69048 measured reflections (Rint, 0.1218) led to R1=0.0492 (I>2ρ (I, wR2, 0.1371 (all data, and S=0.788 with the largest difference peak and hole of 0.296 and -0.459 e Å-3. Electron density contributions from disordered guest molecules were handled using the SQUEEZE procedure from the PLATON software suit. See also Supplementary Information for details. CCDC 714151 (UoC-1) and 714152 (UoC-2) contain the supplementary crystallographic data
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