Synthesis, X-ray single-crystal structure determination, and magnetic properties of [Rb(benzo[18]crown-6)]+ salts containing well-ordered fulleride trianions C603-

Chemistry - A European Journal

Volumn 15, Issue 13, 2009, Pages 3261-3267

  Boeddinghaus, M Bele ^a   Salzinger, Michael ^a   Fässler, Thomas F ^a  

^a TECHNICAL UNIVERSITY OF MUNICH   (Germany)

Author keywords

Crystal structure determination; Fullerenes; Jahn teller effect; Magnetic measurements; Polyanions

Indexed keywords

COORDINATION REACTIONS; DIMETHYLFORMAMIDE; FULLERENES; LIGHT METALS; MAGNETIC MOMENTS; MAGNETIC PROPERTIES; MAGNETIC VARIABLES MEASUREMENT; MONITORING; SPIN DYNAMICS; SYNTHESIS (CHEMICAL);

18-CROWN-6; ALKALI-METAL ATOMS; COORDINATION SPHERES; CRYSTAL STRUCTURE DETERMINATION; DIMETHYLFORMAMIDE MOLECULES; FULLERIDE; HIGH QUALITIES; JAHN-TELLER DISTORTIONS; JAHN-TELLER EFFECT; MAGNETIC MEASUREMENTS; POLYANIONS; SPIN SYSTEMS; STRUCTURAL DETAILS; STRUCTURE REFINEMENTS; TETRAHYDROFURAN; TRIANIONS; X-RAY SINGLE-CRYSTAL STRUCTURE DETERMINATIONS;

CRYSTAL STRUCTURE;

EID: 63749125455     PISSN: 09476539     EISSN: 15213765     Source Type: Journal    
DOI: 10.1002/chem.200801923     Document Type: Article

References (30)

1. a) R. M. Fleming, A. P. Ramirez, M. J. Rosseinsky, D. W. Murphy, R. C. Haddon, S. M. Zahurak, A. V. Makhija, Nature 1991, 352, 787-788;
2. b) K. Tanigaki, T. W. Ebbesen, S. Saito, J. Mizuki, J. S. Tsai, Y. Kubo, S. Kuroshima, Nature 1991, 352, 222-223;
3. c) A. F. Hebard, M. J. Rosseinsky, R. C. Haddon, D. W. Murphy, S. H. Glarum, T. T. M. Palstra, A. P. Ramirez, A. R. Kortan, Nature 1991, 350, 600-601.
4. a) K. Prassides, Curr. Opin. Solid State Mater. Sci. 1997, 2, 433-439:
5. b) O. Gunnarsson, Rev. Mod. Phys. 1997, 69, 575-606.
6. a) M. J. Rosseinsky, D. W. Murphy, R. M. Fleming, O. Zhou, Nature 1993, 364, 425-427;
7. b) D. Varshney, High Pressure Res. 2006, 26, 203-222.
8. a) Y. Iwasa, H. Shimoda, Y. Miyamoto, T. Milani, Y. Maniwa, O. Zhou, T. T. M. Palstra, J. Phys. Chem. Solids 1997, 58, 1697-1705;
9. b) P. Durand. Y. Dubilsky, M. J. Rosseinsky, A. Zaopo. Dalton Trans. 2004, 3137-3143.
10. a) C. A. Reed, R. D. Bolskar, Chem. Rev. 2000, 100, 1075;
11. b) J. L. Dunn, H. Li, Phys. Rev. B 2005, 71, 115411 1-9.
12. C. Janiak, S. Mühle, H. Hemling, K. Köhler, Polyhedron 1996, 15, 1559-1563.
13. T. F. Fässler, R. Hoffmann, S. Hoffmann. M. Wörle, Angew. Chem. 2000, 112, 2170-2174;
14. Angew. Chem. Int. Ed. 2000, 39, 2091-2094.
15. a) CrysAlis CCD, Oxford Diffraction Ltd., Version 1.171.32.5;
16. b) CrysAlis RED, Oxford Diffraction Ltd., Version 1.171.32.5;
17. c) G. M. Sheldrick, Shelxs-97, Universität Göttingen, Göttingen, Germany, 1997;
18. d) G. M. Sheldrick, Shelxl-97, Universität Göttingen, Göttingen, Germany 1997.
19. J. H. van Vleck, The Theorie of Electric and Magtietic Susceptibilities, Clarendon Press, Oxford, 1932.
20. M. J. Rosseinsky, Chem. Mater. 1998, 10, 2665-2685.
21. K. Himmel, M. Jansen, Inorg. Chem. 1998, 37, 3437-3439.
22. a) S. Liu, Y.-J. Lu, M. M. Kappes, J. A. Ibers, Science 1991, 254, 408-410;
23. b) A. Hirsch, M. Brettreich, Fullerenes, Wiley-VCH, Weinheim, 2005, pp. 30.
24. K. Himmel, M. Jansen, Eur. J. Inorg. Chem. 1998, 1183-1186.
25. a) K. Himmel, M. Jansen, Z. Anorg. Allg. Chem. 1998. 624, 1-3;
26. b) K. Himmel, M. Jansen, Chem. Commun. 1998, 1205-1206;
27. c) H. Brumm, M. Jansen, Z. Anorg. Allg. Chem. 2001, 627, 1433-1435.
28. P. Paul, Z. Xie, R. Bau, P. D. W. Boyd, C. A. Reed, J. Am. Chem. Soc. 1994, 116, 4145-4146.
29. T. F. Fässler, A. Spiekermann, M. E. Spahr, R. Nesper, Angew. Chem. 1997, 109, 502-504;
30. Angew. Chem. Int. Ed. Engl. 1997, 36, 486-488.