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Data for 1: Yield: 0.15 g (37, mp: 195-196 °C. 1H NMR (400 MHz, DMSO-d6, δ 3.70-3.82 (m, 8H, 7.63-7.67 (m, 2H, 7.70-7.76 (m, 2H, 7.80-7.83 (m, 4H, 8.08 (d, 2H, J, 8.4 Hz, 8.26-8.30 (m, 6H, 8.40 (d, 2H, J, 8.8 Hz, 10.10 (br s, 2H, 10.90 (br s, 2H, 13C NMR (DMSO-d6, δ 40.4, 44.0, 108.6, 122.1, 122.6, 123.6, 124.5, 125.3, 125.6, 127.3, 129.2, 129.7, 132.4, 133.7, 140.6, 143.1, 146.1, 180.7, 181.8. HRMS (FAB) calcd for C37H3O N7O4S2F3 [M, 757.1744; found 757.1756; Compound 2: Yield: 0.35 g (53, mp: 207-208 °C. 1H NMR (400 MHz, DMSO-d6, δ 3.74 (m, 8H, 7.60-7.65 (m, 4H, 7.71-7.75 (m, 4H, 7.80-7.82 (m, 2H, 8.13-8.15 (d, 2H, J, 8.4 Hz, 8.26 (m, 3H, 8.51 (br s, 1H, 9.98 (br s, 1H, 10.20 (br s, 1H, 10.90 (br s, 2H, 13C NMR DMSO-d6, δ 40.7, 44.0, 108.9, 109
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+] 730.1619; found 730.1622.
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