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Volumn 8, Issue 8, 2008, Pages 2824-2833

New in situ condensation reaction of amino diphosphonic acids: A series of bicyclic phosphonate derivatives and three novel water clusters

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EID: 61549088153     PISSN: 15287483     EISSN: 15287505     Source Type: Journal    
DOI: 10.1021/cg7011149     Document Type: Article
Times cited : (29)

References (51)
  • 5
    • 54649083741 scopus 로고    scopus 로고
    • Clearfield, A. In Metal Phosphonate Chemistry; Karlin, K. D., Eds.; Progress in Inorganic Chemistry, 47; John Wiley & Sons: New York, 1998; p 371, and references therein.
    • (e) Clearfield, A. In Metal Phosphonate Chemistry; Karlin, K. D., Eds.; Progress in Inorganic Chemistry, Vol. 47; John Wiley & Sons: New York, 1998; p 371, and references therein.
  • 25
    • 0032543688 scopus 로고    scopus 로고
    • For typical examples of designing water clusters via crystal engineering, see for example:a
    • For typical examples of designing water clusters via crystal engineering, see for example:(a) Barbour, L. J.; Orr, G. W.; Atwood, J. L. Nature 1998, 393, 671.
    • (1998) Nature , vol.393 , pp. 671
    • Barbour, L.J.1    Orr, G.W.2    Atwood, J.L.3
  • 38
    • 61549096806 scopus 로고
    • German Patent 263991
    • Kurze, R. German Patent 263991, 1989.
    • (1989)
    • Kurze, R.1
  • 40
    • 61549111199 scopus 로고    scopus 로고
    • Sheldrick, G. M. SHEXTL (Xprep, SADABS, XS, XL) Crystallographic Software Package, Version 5.1; Bruker-AXS: Madison, WI, 1998
    • Sheldrick, G. M. SHEXTL (Xprep, SADABS, XS, XL) Crystallographic Software Package, Version 5.1; Bruker-AXS: Madison, WI, 1998.
  • 50
    • 61549119367 scopus 로고    scopus 로고
    • 2: C 36.44, H 4.59, N 21.25.
    • 2: C 36.44, H 4.59, N 21.25.
  • 51
    • 61549126842 scopus 로고    scopus 로고
    • Crystal data for 4 (C26H39N 13O9P2Ni2, Mw, 857.06, T, 298 K, triclinic, space group P1̄, a, 8.6086(5) Å, b, 14.0222(8) Å, c, 16.3218(9) Å, α, 107.026(2)°, β, 93.350(2)°, γ, 101.663(2)°, V, 1830.4(12) Å3, Z, 2, D calcd, 1.555 g·cm-3, μ, 1.183 mm-1, R1, 0.0431, wR2, 0.0962 all data, goodness-of-fit on F2, 1.111. Crystallographic data have been deposited with the Cambridge Crystallographic Centre as Supplementary Publication No. CCDC 648749
    • 2 = 1.111. Crystallographic data have been deposited with the Cambridge Crystallographic Centre as Supplementary Publication No. CCDC 648749.


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