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2: C 36.44, H 4.59, N 21.25.
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51
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61549126842
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Crystal data for 4 (C26H39N 13O9P2Ni2, Mw, 857.06, T, 298 K, triclinic, space group P1̄, a, 8.6086(5) Å, b, 14.0222(8) Å, c, 16.3218(9) Å, α, 107.026(2)°, β, 93.350(2)°, γ, 101.663(2)°, V, 1830.4(12) Å3, Z, 2, D calcd, 1.555 g·cm-3, μ, 1.183 mm-1, R1, 0.0431, wR2, 0.0962 all data, goodness-of-fit on F2, 1.111. Crystallographic data have been deposited with the Cambridge Crystallographic Centre as Supplementary Publication No. CCDC 648749
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2 = 1.111. Crystallographic data have been deposited with the Cambridge Crystallographic Centre as Supplementary Publication No. CCDC 648749.
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