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Volumn 48, Issue 3, 2009, Pages 786-788

A strategy for synthesis of ionic metal-organic frameworks

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EID: 61449244753 PISSN: 00201669 EISSN: None Source Type: Journal
DOI: 10.1021/ic800632r Document Type: Article

Times cited : (58)

References (26)

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23
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- Synthesis for [Er4(μ3-OH) 4(μ2-O)0.5OL4(H 2O)3]·Br2.90-·Cl 1.10·2H2O (MOF-1, The mixture of ErCl3 · 6H2O (0.0511 g, 0.134 mmol, H2LBr (0.524 g, 0.198mmol, an aqueous solution of NaOH (1.0 mL, 0.30 mmol, H2O (1 mL, and EtOH (9 mL) was heated in a 23 mL capacity stainless-steel reactor with a Teflon liner at 150 °C for 3 days and then cooled to room temperature. Pale-pink prismy crystals of MOF-1 were obtained. Yield: 0.889 g (90, Anal, caled for C28H42Br2.90Cl, 1.10Er4N8O26.50 (Found, C, 18.13 (17.82, H, 1.44 (1.45, N, 6.04 (5.94, IR data (KBr, cm-1, 3379, 1613, 1448, 1409, 1316, 1176, 774, 674. For [PrL(H2O) 4Cl]·Br·H2O MOF-2, Green crysta
- -1): 3376, 1668, 1616, 1391, 1315, 1170, 969, 840, 777, 667.

24
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- Crystal data for MOF-1: M, 1854.47, T, 113(2) K, λ, 0.71073 Å, orthorhombic, Pnma, a, 25.0161(8) Å, b, 31.9509(12) Å, c, 13.2163(6) Å, V= 10563.6(7) At̊3, Z, 8, Dcalcd, 2.332 Mg m -3, μ, 8.627 mm-1, GoF, 1.180, Rint, 0.0781, R1, 0.0551, wR2(all, 0.1373. CCDC 673122. For MOF-2: M, 497.50, T, 113(2) K, λ, 0.71073 Å, monoclinic, C12/m1, a, 8.7533(18) Å, b, 17.854(4) Å, c, 8.6180(17) Å, V, 1339.3(5) Å3, Z, 4, Dcalcd, 2.467 Mg m-3, μ=6.850 mm-1, GoF, 1.093, Rint, 0.0390, R1, 0.0243, wR2all, 0.0662. CCDC 673123
- 2(all) = 0.0662. CCDC 673123.

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