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Volumn 8, Issue 3, 2008, Pages 782-785

An infinite two-dimensional hybrid water-chloride network, self-assembled in a hydrophobic terpyridine iron(II) matrix

(7) Fernandes, Ricardo R a Kirillov, Alexander M a Guedes Da Silva, M Fátima C a,b Ma, Zhen a Da Silva, José A L a Fraústo Da Silva, João J R a Pombeiro, Armando J L a

a INSTITUTO SUPERIOR TÉCNICO (Portugal)

b UNIVERSIDADE LUSÓFONA DE HUMANIDADES E TECNOLOGIAS (Portugal)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 61449142573 PISSN: 15287483 EISSN: 15287505 Source Type: Journal
DOI: 10.1021/cg7010315 Document Type: Article

Times cited : (56)

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- The searching algorithm in the ConQuest Version 1.9 (CSD version 5.28, August 2007) constrained to the presence of any terpyridine moiety and at least one crystallization water molecule and one chloride counter ion resulted in 43 analyzable hits from which 40 compounds contain diverse water-chloride aggregates (there are 29 and 11 examples of infinite (mostly ID) networks and discrete clusters, respectively, See the Supporting Information for the CSD refcodes
- The searching algorithm in the ConQuest Version 1.9 (CSD version 5.28, August 2007) constrained to the presence of any terpyridine moiety and at least one crystallization water molecule and one chloride counter ion resulted in 43 analyzable hits from which 40 compounds contain diverse water-chloride aggregates (there are 29 and 11 examples of infinite (mostly ID) networks and discrete clusters, respectively). See the Supporting Information for the CSD refcodes.

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39
- 61449095635
- Synthesis of 1: FeCl2·2H2O (82 mg, 0.50 mmol) and 4′-phenyl-2,2′: 6′,2″-terpyridine (L, 154 mg, 0.50 mmol) were combined in a THF (20 mL) solution with continuous stirring at room temperature. The resulting deep purple suspension was stirred for 1 h, filtered off, washed with THF (3 × 15 mL, and dried in vacuo to afford a deep purple solid 1 (196 mg, 41, 1 exhibits a high affinity for water and upon recrystallization gives derivatives with a higher varying content of crystallization water. 1 is soluble in H2O, MeOH, EtOH, MeCN, CH2Cl2, and CHCl3. mp > 305 °C dec, Elemental analysis. Found: C 52.96, H 3.76, N 8.36. Calcld. for C42H40Cl4Fe2N6O 5: C 52.42, H 4.19, N 8.73. FAB, MS: m/z: 835, FeL2]Cl2·5H2O, H, 816, F
- 2O (v/v = 9/1) solution of 1.

40
- 61449181272
- Crystal data: 1′: C42H50Cl 2FeN6O10, M, 925.63, triclinic, a, 10.1851(10, b, 12.2125(13, c, 19.5622(19) Å, α, 76.602(6, β, 87.890_(7, γ, 67.321(6)°, U, 2180.3(4) Å3, Τ, 150(2) K, space group P1̄, Z, 2, μ(Mo-Kα, 0.532 mm-1, 32310 reflections measured, 8363 unique (Rint, 0.0719) which were used in all calculations, R1, 0.0469, wR2, 0.0952, Rl, 0.0943, wR2, 0.1121 all data
- 2 = 0.0952, Rl = 0.0943, wR2 = 0.1121 (all data).

41
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42
- 0142247075
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43
- 0141851343
- (c) Kabir, M. K.; Tobita, H.; Matsuo, H.; Nagayoshi, K.; Yamada, K.; Adachi, K.; Sugiyama, Y.; Kitagawa, S.; Kawata, S. Cryst. Growth Des. 2003, 3, 791.
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44
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- Ludwig, R. Angew. Chem., Int. Ed. 2001, 40, 1808.
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- Ludwig, R.¹

45
- 61449176938
- - ring (i.e., minimal cyclic fragment in our water-chloride network) with d(O⋯O) = 2.2-3.2 Å and d(O⋯Cl) = 2.6-3.6 Å, and (ii) at least one crystallization water molecule and one chloride counter ion. All symmetry-related contacts were taken into consideration.
- - ring (i.e., minimal cyclic fragment in our water-chloride network) with d(O⋯O) = 2.2-3.2 Å and d(O⋯Cl) = 2.6-3.6 Å, and (ii) at least one crystallization water molecule and one chloride counter ion. All symmetry-related contacts were taken into consideration.

46
- 61449245587
- - core, see the CSD refcodes: AGETAH, AMIJAH, BEXVIJ, EXOWIX, FANJUA, GAFGIE, HIQCIT, LUNHUX, LUQCEF, PAYBEW, TESDEB, TXCDNA, WAQREL, WIXVUU, ZUHCOW. For 3D network, see the CSD refcode: LUKZEW.
- - core, see the CSD refcodes: AGETAH, AMIJAH, BEXVIJ, EXOWIX, FANJUA, GAFGIE, HIQCIT, LUNHUX, LUQCEF, PAYBEW, TESDEB, TXCDNA, WAQREL, WIXVUU, ZUHCOW. For 3D network, see the CSD refcode: LUKZEW.

47
- 61449236381
- This analysis was run on 1 since we were unable to get 1′ in a sufficient amount due to the varying content of crystallization water in the samples obtained upon recrystallization of 1
- This analysis was run on 1 since we were unable to get 1′ in a sufficient amount due to the varying content of crystallization water in the samples obtained upon recrystallization of 1.

48
- 31144470776
- (a) Das, S.; Bhardwaj, P. K. Cryst. Growth. Des. 2006, 6, 187.
- (2006) Cryst. Growth. Des , vol.6 , pp. 187
- Das, S.¹ Bhardwaj, P.K.²

49
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- (b) Wang, J.; Zheng, L.-L.; Li, C.-J.; Zheng, Y.-Z.; Tong, M.-L. Cryst. Growth. Des. 2006, 6, 357.
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- Wang, J.¹ Zheng, L.-L.² Li, C.-J.³ Zheng, Y.-Z.⁴ Tong, M.-L.⁵

50
- 20444480667
- (c) Ghosh, S. K.; Ribas, J.; El Fallah, M. S.; Bharadwaj, P. K. Inorg. Chem. 2005, 44, 3856.
- (2005) Inorg. Chem , vol.44 , pp. 3856
- Ghosh, S.K.¹ Ribas, J.² El Fallah, M.S.³ Bharadwaj, P.K.⁴

51
- 61449172896
- A temperature below 305 °C has been used to avoid the eventual decomposition of the compound upon rather prolonged heating.
- A temperature below 305 °C has been used to avoid the eventual decomposition of the compound upon rather prolonged heating.

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