Fast acquisition of high-resolution NMR spectra in inhomogeneous fields via intermolecular double-quantum coherences

Journal of Chemical Physics

Volumn 130, Issue 8, 2009, Pages

  Chen, Zhong ^a   Cai, Shuhui ^a   Chen, Zhiwei ^a   Zhong, Jianhui ^b  

^a XIAMEN UNIVERSITY   (China)

^b UNIVERSITY OF ROCHESTER   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

BIOASSAY; BIOCHIPS; CHEMICAL SHIFT; COHERENT LIGHT; LIQUIDS; MAGNETIC FIELDS; MERGERS AND ACQUISITIONS; NUCLEAR MAGNETIC RESONANCE; SPIN DYNAMICS;

ACCURATE MEASUREMENTS; ACQUISITION TIME; ANALYTICAL EXPRESSIONS; BIOLOGICAL SAMPLES; COMBINATORIAL CHEMISTRIES; COUPLED SPINS; FAST ACQUISITIONS; FIELD INHOMOGENEITY; HIGH RESOLUTIONS; IN-VIVO; INDIRECT DIMENSIONS; INHOMOGENEITIES; INHOMOGENEOUS FIELDS; INTER-MOLECULAR MULTIPLE-QUANTUM COHERENCES; INTERMOLECULAR DOUBLE-QUANTUM COHERENCES; J COUPLINGS; LIQUID NMR; MAGNETIC FIELD INHOMOGENEITY; MULTIPLET PATTERNS; NEW MATERIALS; NMR SPECTROSCOPIES; NMR SPECTRUM; ONE-DIMENSIONAL; PEAK AREAS; PULSE SEQUENCES; SINGLE-QUANTUM COHERENCES; SOLUTION SAMPLES; SPECTROSCOPIC INFORMATIONS; SPIN SYSTEMS; STRUCTURAL INFORMATIONS; TWO-DIMENSIONAL;

NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY;

ARTICLE; COMBINATORIAL CHEMISTRY; INSTRUMENTATION; MAGNETISM; METABOLISM; METHODOLOGY; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; TIME;

COMBINATORIAL CHEMISTRY TECHNIQUES; MAGNETIC RESONANCE SPECTROSCOPY; MAGNETICS; METABOLISM; TIME FACTORS;

EID: 61449084745     PISSN: 00219606     EISSN: None     Source Type: Journal    
DOI: 10.1063/1.3076046     Document Type: Article

References (48)

1. D. P. Weitekamp, J. R. Garbow, J. B. Murdoch, and A. Pines, J. Am. Chem. Soc. 0002-7863 10.1021/ja00402a057 103, 3578 (1981).
2. L. D. Hall and T. J. Norwood, J. Chem. Soc., Chem. Commun. 44 (1986).
3. L. D. Hall and T. J. Norwood, J. Chem. Soc., Chem. Commun. 1508 (1986).
4. D. Sakellariou, S. P. Brown, A. Lesage, S. Hediger, M. Bardet, C. A. Meriles, A. Pines, and L. Emsley, J. Am. Chem. Soc. 0002-7863 10.1021/ja0292389 125, 4376 (2003).
5. C. A. Meriles, D. Sakellariou, H. Heise, A. J. Mouĺ, and A. Pines, Science 0036-8075 10.1126/science.1061498 293, 82 (2001).
6. B. Blümich, J. Perlo, and F. Casanova, Prog. Nucl. Magn. Reson. Spectrosc. 52, 197 (2008). 0079-6565
7. J. J. Balbach, M. S. Conradi, D. P. Cistola, C. G. Tang, J. R. Garbow, and W. C. Hutton, Chem. Phys. Lett. 277, 367 (1997). 0009-2614
8. J. Jeener, in Encyclopedia of Nuclear Magnetic Resonance, edited by, D. M. Grant, and, R. K. Harrispp, (Wiley, New York, 2002), Vol. 9, p. 642.
9. S. Vathyam, S. Lee, and W. S. Warren, Science 0036-8075 10.1126/science.272.5258.92 272, 92 (1996).
10. Z. Chen, Z. W. Chen, and J. H. Zhong, J. Am. Chem. Soc. 0002-7863 10.1021/ja036491f 126, 446 (2004).
11. Z. Chen, T. Hou, Z. W. Chen, D. W. Hwang, and L. P. Hwang, Chem. Phys. Lett. 0009-2614 10.1016/j.cplett.2004.01.055 386, 200 (2004).
12. V. Demas, D. Sakellariou, C. A. Meriles, S. Han, J. Reimer, and A. Pines, Proc. Natl. Acad. Sci. U.S.A. 0027-8424 10.1073/pnas.0403016101 101, 8845 (2004).
13. S. Lee, W. Richter, S. Vathyam, and W. S. Warren, J. Chem. Phys. 0021-9606 10.1063/1.471968 105, 874 (1996).
14. Y. Y. Lin, S. Ahn, N. Murali, W. Brey, C. R. Bowers, and W. S. Warren, Phys. Rev. Lett. 0031-9007 10.1103/PhysRevLett.85.3732 85, 3732 (2000).
15. X. Chen, M. J. Lin, Z. Chen, S. H. Cai, and J. H. Zhong, Phys. Chem. Chem. Phys. 1463-9076 10.1039/b709154k 9, 6231 (2007).
16. Y. Q. Lin, Z. Chen, S. H. Cai, and J. H. Zhong, J. Magn. Reson. 1090-7807 10.1016/j.jmr.2007.11.010 190, 298 (2008).
17. D. Z. Balla and C. Faber, Concepts Magn. Reson. Part A 32A, 117 (2008).
18. A. Wiesmath, C. Filip, D. E. Demco, and B. Blümich, J. Magn. Reson. 1090-7807 10.1006/jmre.2001.2299 149, 258 (2001).
19. J. Perlo, V. Demas, F. Casanova, C. A. Meriles, J. Reimer, A. Pines, and B. Blümich, Science 0036-8075 10.1126/science.1108944 308, 1279 (2005).
20. J. Perlo, F. Casanova, and B. Blümich, Science 0036-8075 10.1126/science.1135499 315, 1110 (2007).
21. B. Shapira and L. Frydman, J. Am. Chem. Soc. 0002-7863 10.1021/ja048859u 126, 7184 (2004).
22. B. Shapira and L. Frydman, J. Magn. Reson. 182, 12 (2006). 1090-7807
23. R. A. de Graaf, D. L. Rothman, and K. L. Behar, J. Magn. Reson. 187, 320 (2007). 1090-7807
24. D. Topgaard, D. Sakellariou, and A. Pines, J. Magn. Reson. 1090-7807 10.1016/j.jmr.2005.03.006 175, 1 (2005).
25. D. Topgaard, R. W. Martin, D. Sakellariou, C. A. Meriles, and A. Pines, Proc. Natl. Acad. Sci. U.S.A. 0027-8424 10.1073/pnas.0408296102 101, 17576 (2004).
26. J. Perlo, F. Casanova, and B. Blümich, J. Magn. Reson. 1090-7807 10.1016/j.jmr.2006.03.004 180, 274 (2006).
27. L. Frydman, A. Lupulescu, and T. Scherf, J. Am. Chem. Soc. 0002-7863 10.1021/ja030055b 125, 9204 (2003).
28. W. S. Warren, S. Ahn, M. Mescher, M. Garwood, K. Ugurbil, W. Richter, R. R. Rizi, J. Hopkins, and J. S. Leigh, Science 0036-8075 10.1126/science.281. 5374.247 281, 247 (1998).
29. J. H. Zhong, Z. Chen, and E. Kwok, Magn. Reson. Med. 43, 335 (2000).
30. C. Faber, E. Pracht, and A. Haase, J. Magn. Reson. 1090-7807 10.1016/S1090-7807(03)00006-5 161, 265 (2003).
31. G. Galiana, R. T. Branca, and W. S. Warren, J. Am. Chem. Soc. 0002-7863 10.1021/ja054463m 127, 17574 (2005).
32. D. Z. Balla and C. Faber, MAGMA (N.Y) 20, 183 (2007). 0968-5243
33. D. Z. Balla and C. Faber, J. Chem. Phys. 0021-9606 10.1063/1.2904564 128, 154522 (2008).
34. R. Bowtell, R. M. Bowley, and P. Glover, J. Magn. Reson. 88, 643 (1990). 1090-7807
35. R. Bowtell and P. Robyr, Phys. Rev. Lett. 0031-9007 10.1103/PhysRevLett. 76.4971 76, 4971 (1996).
36. P. Robyr and R. Bowtell, J. Chem. Phys. 0021-9606 10.1063/1.474435 107, 702 (1997).
37. C. Ramanathan and R. Bowtell, J. Chem. Phys. 0021-9606 10.1063/1.1375026 114, 10854 (2001).
38. J. P. Marques and R. Bowtell, Magn. Reson. Med. 0740-3194 10.1002/mrm.10700 51, 148 (2004).
39. C. Faber, C. Heil, B. Zahneisen, D. Z. Balla, and R. Bowtell, J. Magn. Reson. 1090-7807 10.1016/j.jmr.2006.05.002 182, 315 (2006).
40. Y. Y. Lin, N. Lisitza, S. D. Ahn, and W. S. Warren, Science 0036-8075 10.1126/science.290.5489.118 290, 118 (2000).
41. S. Datta, S. Y. Huang, and Y. Y. Lin, J. Chem. Phys. 124, 154501 (2006). 0021-9606
42. M. Mescher, W. Richter, L. DelaBarre, M. Garward, and W. S. Warren, Proceeding of the International Society for Magnetic Resonance in Medicine Eighth Scientific Meeting and Exhibition, Denver Colorado, USA, April 1-7, 2000..
43. Z. Chen, Z. W. Chen, and J. H. Zhong, J. Chem. Phys. 0021-9606 10.1063/1.1417503 115, 10769 (2001).
44. D. Balla and C. Faber, Chem. Phys. Lett. 0009-2614 10.1016/j.cplett.2004. 06.087 393, 464 (2004).
45. C. Faber, J. Magn. Reson. 176, 120 (2005). 1090-7807
46. W. Richter and W. S. Warren, Concepts Magn. Reson. 12, 396 (2000).
47. S. Y. Huang, C. Anklin, J. D. Walls, and Y. Y. Lin, J. Am. Chem. Soc. 0002-7863 10.1021/ja046208s 126, 15936 (2004).
48. G. E. Pereira, J. P. Gaudillere, C. van Leeuwen, G. Hilbert, O. Lavialle, M. Maucourt, C. Deborde, A. Moing, and D. Rolin, J. Agric. Food Chem. 53, 6382 (2005). 0021-8561