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Volumn 10, Issue 17, 2008, Pages 3927-3929

2-Trimethylsilylcorannulenyl trifluoromethanesulfonate: An efficient precursor for 1,2-didehydrocorannulene

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EID: 61349195146     PISSN: 15237060     EISSN: None     Source Type: Journal    
DOI: 10.1021/ol801581z     Document Type: Article
Times cited : (25)

References (22)
  • 1
    • 33846206028 scopus 로고    scopus 로고
    • For recent reviews see: a
    • For recent reviews see: (a) Wu, T.-Y.; Siegel, J. S. Chem. Rev. 2006, 106, 4843.
    • (2006) Chem. Rev , vol.106 , pp. 4843
    • Wu, T.-Y.1    Siegel, J.S.2
  • 3
    • 84891008336 scopus 로고    scopus 로고
    • Haley, M. M, Tykwinski, R. R, Eds, Wiley-VCH: Weinheim
    • (c) Sygula, A., Rabideau, P. W. In Carbon Rich Compounds; Haley, M. M., Tykwinski, R. R., Eds.; Wiley-VCH: Weinheim, 2006; p 529.
    • (2006) Carbon Rich Compounds , pp. 529
    • Sygula, A.1    Rabideau, P.W.2
  • 11
    • 61349084005 scopus 로고    scopus 로고
    • The instability of hydroxycorannulene has been noted before: Cheng, P.-G. Ph.D. Thesis, Boston College, Boston, MA, 1996.
    • The instability of hydroxycorannulene has been noted before: Cheng, P.-G. Ph.D. Thesis, Boston College, Boston, MA, 1996.
  • 12
    • 61349103491 scopus 로고    scopus 로고
    • Cheng, P.-C. M.S. Thesis, University of Nevada, Reno, NV, 1992.
    • (a) Cheng, P.-C. M.S. Thesis, University of Nevada, Reno, NV, 1992.
  • 15
    • 61349125298 scopus 로고    scopus 로고
    • 12O 280.0888, found 280.0893.
    • 12O 280.0888, found 280.0893.
  • 16
    • 61349162128 scopus 로고    scopus 로고
    • 6 was synthesized previously on a miligram scale by a different method (ref 9).
    • 6 was synthesized previously on a miligram scale by a different method (ref 9).
  • 17
    • 61349118432 scopus 로고    scopus 로고
    • 11OBr 357.9993, found 357.9994.
    • 11OBr 357.9993, found 357.9994.
  • 18
    • 61349177688 scopus 로고    scopus 로고
    • 5: white solid (from EtOH, mp 94-6 °C; 1H NMR (CDCl3, 300 MHz) δ (strongly concentration dependent) 8.07 (1H. d, J, 8.9 Hz, 7.98 (IH, d, J, 8.9 Hz, 7.91 (lH, d. J, 8.9 Hz, 7.86 (lH, d, J, 8.9 Hz, 7.83 (lH, d, J, 8.8 Hz, 7.80-7.76 (3H, m, 0.76 (9H, s, 13C NMR (CDCl3, 75.5 MHz) d 148.02, 137.16. 136.74, 135.64, 135.09, 134.39, 134.38, 133.89, 131.26, 131.25, 130.86, 128.48, 128.15, 128.14, 127.75, 127.55, 127.28, 127.21, 123.78 (b, 123.61, 119.10 (q, J, 320.3 Hz, 2.75; MS m/z (rel intensity) 470 (6, 455 (49, 339 (24, 338 (74, 337 (53, 322 (27, 264 (26, 263 (100, HRMS (EI, 25 eV) calcd for C24H17O 3F3SiS 470.0619, found 470.0611
    • 3SiS 470.0619, found 470.0611.
  • 22
    • 61349105738 scopus 로고    scopus 로고
    • Recent review: Guitián, E.; Pérez, D.; Pena. D. Top. Organomet. Chem. 2005, 14, 109.
    • (b) Recent review: Guitián, E.; Pérez, D.; Pena. D. Top. Organomet. Chem. 2005, 14, 109.


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.