Technetium and rhenium in five-coordinate symmetrical and dissymmetrical nitrido complexes with alkyl phosphino-thiol ligands. Synthesis and structural characterization

Inorganic Chemistry

Volumn 47, Issue 24, 2008, Pages 11972-11983

  Bolzati, Cristina ^a   Cavazza Ceccato, Mario ^b   Agostini, Stefania ^b   Tisato, Francesco ^a   Bandoli, Giuliano ^b  

^a CNR   (Italy)

^b UNIVERSITY OF PADOVA   (Italy)

Author keywords

[No Author keywords available]

Indexed keywords

LIGAND; PHOSPHINE DERIVATIVE; RADIOPHARMACEUTICAL AGENT; RHENIUM; TECHNETIUM; THIOCARBAMIC ACID DERIVATIVE; THIOL DERIVATIVE;

ARTICLE; BRAIN; CHEMICAL STRUCTURE; CHEMISTRY; CONFORMATION; ELECTROSPRAY MASS SPECTROMETRY; HEART; HUMAN; METHODOLOGY; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; POSITRON EMISSION TOMOGRAPHY; RADIOGRAPHY; SCINTISCANNING; SINGLE PHOTON EMISSION COMPUTER TOMOGRAPHY; SYNTHESIS; X RAY CRYSTALLOGRAPHY;

BRAIN; CRYSTALLOGRAPHY, X-RAY; HEART; HUMANS; LIGANDS; MAGNETIC RESONANCE SPECTROSCOPY; MODELS, MOLECULAR; MOLECULAR CONFORMATION; PHOSPHINES; POSITRON-EMISSION TOMOGRAPHY; RADIOPHARMACEUTICALS; RHENIUM; SPECTROMETRY, MASS, ELECTROSPRAY IONIZATION; SULFHYDRYL COMPOUNDS; TECHNETIUM; THIOCARBAMATES; TOMOGRAPHY, EMISSION-COMPUTED, SINGLE-PHOTON;

EID: 60849105386     PISSN: 00201669     EISSN: None     Source Type: Journal    
DOI: 10.1021/ic801436d     Document Type: Article

References (46)

1. Eckelman, W. C.; Erba, P. A.; Schwaiger, M.; Wagner, H. N. J.; Alberto, R.; Mazzi, U. J. Nucl. Med. Biol. 2007, 34, 1-4.
2. Levin, C. S. Eur. J. Nucl. Med. Mol. Imaging 2005, 32, S325-S345.
3. Mahmood, A.; Limpa-Amara, N.; MacKenzie, J. D.; Zimmerman, R. E.; El Fakhri, G.; Moore, S. C.; Jones, A. G. In Proceedings of the Seventh International Symposium on Technetium in Chemistry and Nuclear Medicine. Mazzi U, Ed.; 7 Servizi Grafici Editoriali snc: Padova, Italy, 2006; 465-470.
4. Madsen, M. T. J. Nucl. Med. 2007, 48, 661-673.
5. Wagner, H. N., Jr. J. Nucl. Med. 2006, 47, 13N-39N.
6. Duatti, A.; Marchi, A.; Pasqualini, R. J. Chem. Soc., Dalton Trans. 1990, 3729-3733.
7. Bolzati, C.; Boschi, A.; Uccelli, L.; Malagò, E.; Bandoli, G.; Tisato, F.; Refosco, F.; Pasqualini, R.; Duatti, A. Inorg. Chem. 1999, 38, 4473-4479.
8. (a) Bolzati, C.; Boschi, A.; Duatti, A.; Prakash, S.; Uccelli, L.; Refosco, F.; Tisato, F.; Bandoli, G. J. Am. Chem. Soc. 2000, 122, 4510-4511.
9. (b) Boschi, A.; Bolzati, C.; Benini, E.; Malagò, E.; Uccelli, L.; Duatti, A.; Piffanelli, A.; Refosco, F.; Tisato, F. Bioconjugate Chem. 2001, 12, 1035-1042.
10. (c) Bolzati, C.; Boschi, A.; Uccelli, L.; Tisato, F.; Refosco, F.; Cagnolini, A.; Duatti, A.; Prakash, S.; Bandoli, G.; Vittadini, A. J. Am. Chem. Soc. 2002, 124, 11468-11479.
11. (a) Pasqualini, R.; Duatti, A.; Bellande, E.; Comazzi, V.; Brucato, V.; Hoffschir, D.; Fagret, D.; Comet, M. J. Nucl. Med. 1994, 35, 334-341.
12. (b) Pasqualini, R.; Bellande, E.; Comazzi, V.; Lainé, J.; Lécayon, M.; Hoffschir, D.; Duatti, A. J. Nucl. Med. 1993, 34, 18 P. No 63 abstract.
13. (c) Zhang, J; Wang, X.; Li, C. Y. J. Nucl. Med. Biol. 2002, 29, 665-669.
14. (d) Bolzati, C.; Uccelli, L.; Boschi, A.; Malagò, E.; Duatti, A.; Tisato, F.; Refosco, F.; Pasqualini, R.; Piffanelli, A. J. Nucl. Med. Biol. 2000, 27, 369-374.
15. (e) Boschi, A.; Bolzati, C.; Uccelli, L.; Duatti, A.; Benini, E.; Refosco, F.; Tisato, F.; Piffanelli, A. Nucl. Med. Commun. 2002, 23, 689-693.
16. (f) Boschi, A.; Uccelli, L.; Bolzati, C.; Duatti, A.; Sabba, N.; Moretti, E.; Di Domenico, G.; Zavattini, G.; Refosco, F.; Giganti, M. J. Nucl. Med. 2003, 44, 806-814.
17. (g) Liu, S.; He, Z.; Hsieh, W. Y.; Kim, Y. Nucl. Med. Biol. 2006, 33, 419-432.
18. (a) Hatada, K.; Riou, L. M.; Ruiz, M.; Yamamichi, Y.; Duatti, A.; Lima, R. L.; Goode, A. R.; Watson, D. D.; Gorge, A.; Beller, G. A.; Glover, D. K. J. Nucl. Med. 2004, 45, 2095-2101.
19. (b) Hatada, K.; Ruiz, M.; Riou, L. M.; Lima, R. L.; Goode, A. R.; Watson, D. D.; Beller, G. A.; Glover, D. K. J. Nucl. Cardiol. 2006, 6, 779-790.
20. (a) Bolzati, C.; Refosco, F.; Tisato, F.; Bandoli, G.; Dolmella, A. Inorg. Chim. Acta 1992, 201, 7-10.
21. (b) Tisato, F.; Refosco, F.; Bandoli, G.; Bolzati, C.; Moresco, A. J. Chem. Soc., Dalton Trans. 1994, 1453-1461.
22. Bolzati, C.; Malagò, E.; Boschi, A.; Cagnolini, A.; Porchia, M.; Bandoli, G. New J. Chem. 1999, 23, 807-809.
23. Bolzati, C.; Benini, E.; Cavazza-Ceccato, M.; Cazzola, E.; Malagò, E.; Agostini, S.; Tisato, F.; Refosco, F.; Bandoli, G. Bioconjugate Chem. 2006, 17, 419-428.
24. (a) Baldas, J.; Boas, J. F.; Bonnymann, J.; Williams, G. A. J. Chem. Soc., Dalton Trans. 1984, 2394.
25. (b) Abram, U.; Lorenz, B.; Kaden, L.; Scheller, D. Polyhedron 1988, 7, 285-289.
26. Sheldrick, G. M. Acta Crystallogr. 2008, A64, 112-122.
27. Tolmann, C. A. Chem. Rev. 1977, 77, 313-348.
28. Tubaro, M.; Traldi, P.; Bolzati, C.; Tisato, F.; Refosco, F.; Benini, E.; Cavazza-Ceccato, M. Rapid Commun. Mass Spectrom. 2005, 19, 1874-1880.
29. (a) Freiberg, E.; Davis, W. M.; Nicholson, T.; Davison, A.; Jones, A.; G Inorg. Chem. 2002, 41, 5667-5674.
30. (b) Pérez-Lourido, P.; Romero, J.; Garcìa-Vázquez, J. A.; Sousa, A.; Maresca, K. P.; Zubieta, J. Inorg. Chem. 1999, 38, 1511-1519.
31. (c) Pérez-Lourido, P.; Romero, J.; Garcýá- Vázquez, J. A.; Sousa, A.; Maresca, K. P.; Zubieta, J. Inorg. Chem. 1999, 38, 1293-1298.
32. (d) Pérez-Lourido, P.; Romero, J.; García-Vázquez, J. A.; Sousa, A.; Maresca, K. P.; Zubieta, J. Inorg. Chem. 1999, 38, 3709-3715.
33. (e) Pèz-Lourido, P.; Romero, J.; Garcìa-Vázquez, J. A.; Sousa, A.; Maresca, K. P.; Rose, D. J.; Zubieta, J. Inorg. Chem. 1998, 37, 3331-3336.
34. (f) Rose, D. J.; Maresca, K. P.; Kettler, P. B.; Da Chang, Y.; Soghomomian, V.; Chen, Q.; Abrams, M. J.; Larsen, S. K. Zubieta J. Inorg. Chem. 1996, 35, 3548-3558.
35. Addison, A. W.; Rao, T. N.; Reedijk, J.; Van Riĵn, J.; Verschoor, G. C. J. Chem. Soc., Dalton Trans. 1984, 1349-1356.
36. (a) Bandoli, G.; Tisato, F.; Dolmella, A.; Agostini, S. Coord. Chem. Rew. 2006, 250, 561-573.
37. (b) Bandoli, G.; Dolmella, A.; Porchia, M.; Refosco, F.; Tisato, F. Coord. Chem. Rew. 2001, 214, 43-90.
38. (a) Allen, F. H. Acta Crystallogr. 2002, B58, 380-388.
39. (b) Macrae, C. F.; Edgington, P. R.; McCabe, P.; Pidcock, E.; Shields, G. P.; Taylor, R.; Towler, M.; van de Streek, J. J. Appl. Crystallogr. 2006, 39, 453-457.
40. Rossi, R.; Marchi, A.; Martelli, L.; Magon, L.; Peruzzini, M.; Casellato, U.; Graziani, R. J. Chem. Soc., Dalton Trans. 1993, 723-729.
41. Abram, U.; Ritter, S. Inorg. Chim. Acta 1994, 216, 31-36.
42. (a) Bolzati, C.; Refosco, F.; Cagnolini, A.; Tisato, F.; Boschi, A.; Duatti, A.; Uccelli, L.; Dolmella, A.; Marotta, E.; Tubaro, M. Eur. J. Inorg. Chem. 2004, 1902-1913.
43. (b) Fletcher, S. R.; Skapski, A. C. J. Chem. Soc., Dalton Trans. 1972, 1079-1082.
44. Blower, P. J.; Dilworth, J. R. Coord. Chem. Rev. 1987, 76, 121-185.
45. Dilworth, J. R.; Hutson, A. J.; Morton, S.; Harman, M.; Hursthouse, M. B.; Zubieta, J.; Archer, C. M.; Kelly, J. D. Polyhedron 1992, 11, 2151-2155.
46. Maina, T.; Pecorale, A.; Dolmella, A.; Bandoli, G.; Mazzi, U. J. Chem. Soc., Dalton Trans. 1994, 2437-2443.