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The polymerization of compound 2 was not conducted because its high viscosity made the mixing process difficult
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The polymerization of compound 2 was not conducted because its high viscosity made the mixing process difficult.
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26
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Compound 6 was synthesized according to the procedure: Musa, O, National Starch and Chemical Company, U.S. Patent 6,803,406, October 12, 2004
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The die shear tests were conducted at 150°C because the upper temperature limit for the die shear testing equipment is 150°C. Exposure to 250°C for 2 min prior to the die shear measurements is to simulate the rework condition.
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The die shear tests were conducted at 150°C because the upper temperature limit for the die shear testing equipment is 150°C. Exposure to 250°C for 2 min prior to the die shear measurements is to simulate the rework condition.
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The cured sample was prepared by heating a mixture of 98 wt % compound 1 and 2 wt % USP-90MD at 120°C for 10 min.
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The cured sample was prepared by heating a mixture of 98 wt % compound 1 and 2 wt % USP-90MD at 120°C for 10 min.
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