Determination of PCBs in marine sediment using pressurised liquid extraction-gas chromatography-isotope dilution mass spectrometry - method validation

Chemia Analityczna

Volumn 53, Issue 6, 2008, Pages 785-796

  Konieczka, Piotr ^a   Namieśnik, Jacek ^a  

^a GDANSK UNIVERSITY OF TECHNOLOGY   (Poland)

Author keywords

Accelerated solvent extraction; Gas chromatography; Isotope dilution mass spectrometry; Polychlorinated biphenyls; Sediment; Validation

Indexed keywords

EID: 60549092274     PISSN: 00092223     EISSN: None     Source Type: Journal    
DOI: None     Document Type: Article

References (24)

1. Guide to the Expression of Uncertainty in Measurement, 1995:ISO, ISBN 92-67-10188-9, Geneva, Switzerland.
2. Brinkman U.A.Th. and de Kok A., Halogenated Biphenyls, Terphenyls, Naphthalenes, Dibenzodioxins and Related Products, [Kimbrough R.D., Ed.], Elsevier, Amsterdam, 1980, Ch. 1, p. 1.
3. Moore J.W. and Ramamorthy S., Organic Chemicals in Natural Waters, Springer, New York 1984, Ch. 9, p. 168.
4. Tanabe S., Environ. Pollut., 50, 5 (1988).
5. UNEP (United Nations Environment Programme): UNEP 1999 report.
6. Council Directive 85/467/EEC of 1 October 1985 amending for the sixth time Directive 76/769/EEC on the approximation of the laws, regulations and administrative provisions of the Member States relating to restrictions on the marketing and use of certain dangerous substances and preparations (PCBs/PCTs).
7. Council Directive 96/59/EC of 16 September 1996 on the disposal of polychlorinated biphenyls and polychlorinated terphenyls (PCBs/PCTs), (replaces Council Directive 76/403/EEC - ban of use of PCBs in EC in open applications, 1976).
8. Helcom Recommendation 6/1, Recommendation regarding the elimination of use of PCBs and PCTs - adopted 13 March 1995, having regard to article 13, Paragraph b of the Helsinki Convention.
9. Martens D., Gfrerer M., Wenzl T., Zhang A., Gawlik B.M., Schramm K.W., Lankmayr E. and Kettrup A., Anal. Bioanal. Chem., 372, 562 (2002).
10. Santschi P.H., Presley B.J., Wade T.L., Garcia-Romero B. and Baskaran M., Marine Environmental Research, 52, 51 (2001).
11. Kocan A., Petrik J., Jursa S., Chovancova J. and Drobna B., Chemosphere, 43, 595 (2001).
12. Wenzel K. D., Hubert A., Manz M., Weissflog L., Engewald W. and Schüürmann G., Anal. Chem., 70, 4827 (1998).
13. Zhou J.L., Maskaoui K., Qiu Y.W., Hong H.S. and Wang Z.D., Environ. Pollut., 113, 373 (2001).
14. Giergielewicz-Możajska H., Dabrowski Ł. and Namieśnik J., Crit. Rev. Anal. Chem., 31, 149 (2001).
15. Dabrowski Ł., Giergielewicz-Możajska H., Biziuk M., Gaca J. and Namieśnik J., J. Chromatogr. A., 957, 59 (2002).
16. Hubert A., Wenzel K.D., Manz M., Weisflog L., Engewald W. and Schüürmann G., Anal. Chem., 72, 1294 (2000).
17. Thompson S., Budzinski H., LeMenach K., Letellier M. and Garrigues P., Anal. Bioanal. Chem., 372, 196 (2002).
18. Bøwadt S., Johansson B., Fruekilde P., Hansen M., Zilli D., Larsen B. and De Boer J., J. Chromatogr. A., 675, 189 (1994).
19. Nilson T., Bøwadt S. and Björklund E., Chemosphere, 46, 469 (2002).
20. Frame G.M., Fresenius J. Anal. Chem., 357, 701 (1997).
21. Frame G.M., Fresenius J. Anal. Chem., 357, 714 (1997).
22. Eljarrat E., Sauló J., Monjonell A., Caixach J. and Rivera J., Fresenius J. Anal. Chem., 371, 983 (2001).
23. http://www.bipm.org/utils/common/pdf/final_reports/QM/K25/CCQM-K25.pdf
24. International Conference on Harmonization (ICH) of Technical Requirements for the Registration of Pharmaceuticals for Human Use: Text on Validation of Analytical Procedures, ICH-Q2A, Geneva 1994.