메뉴 건너뛰기




Volumn 94, Issue 3, 2009, Pages 456-464

Quantification of radiation induced crosslinking in a commercial, toughened silicone rubber, TR55 by 1H MQ-NMR

Author keywords

Crosslinking; NMR; Radiation; Silicones

Indexed keywords

DEGRADATION; IONIZING RADIATION; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; RADIATION; RADIATION EFFECTS; SILICONES; SPIN DYNAMICS;

EID: 59349107035     PISSN: 01413910     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.polymdegradstab.2008.10.028     Document Type: Article
Times cited : (32)

References (46)
  • 4
    • 0038431764 scopus 로고
    • Changes in silicone polymeric fluids due to high energy radiation
    • Charlesby A. Changes in silicone polymeric fluids due to high energy radiation. Proc R Soc Lond A230 1180 (1955) 120-135
    • (1955) Proc R Soc Lond , vol.A230 , Issue.1180 , pp. 120-135
    • Charlesby, A.1
  • 5
    • 0000469288 scopus 로고
    • Radiation chemistry of polydimethylsiloxane, crosslinking and gas yields
    • Miller A.A. Radiation chemistry of polydimethylsiloxane, crosslinking and gas yields. J Am Chem Soc 82 (1960) 3519-3523
    • (1960) J Am Chem Soc , vol.82 , pp. 3519-3523
    • Miller, A.A.1
  • 7
    • 41949093040 scopus 로고
    • Effect of radiation on organopolysiloxanes
    • Warrick E.L. Effect of radiation on organopolysiloxanes. Ind Eng Chem 24 (1955) 842-848
    • (1955) Ind Eng Chem , vol.24 , pp. 842-848
    • Warrick, E.L.1
  • 8
    • 0031461306 scopus 로고    scopus 로고
    • Hardness measurements of silicone rubber and polyurethane rubber cured by ionizing radiation
    • Basfar A.A. Hardness measurements of silicone rubber and polyurethane rubber cured by ionizing radiation. Radiat Phys Chem 50 (1997) 607-610
    • (1997) Radiat Phys Chem , vol.50 , pp. 607-610
    • Basfar, A.A.1
  • 9
    • 0032260503 scopus 로고    scopus 로고
    • Poly(dimethylsiloxane) elastomers from aqueous emulsions: III. Effect of blended silica fillers and gamma-radiation-induced crosslinking
    • Mark J.E., and McCarthy D.W. Poly(dimethylsiloxane) elastomers from aqueous emulsions: III. Effect of blended silica fillers and gamma-radiation-induced crosslinking. Rubber Chem Technol 71 (1998) 941-948
    • (1998) Rubber Chem Technol , vol.71 , pp. 941-948
    • Mark, J.E.1    McCarthy, D.W.2
  • 10
    • 0034578957 scopus 로고    scopus 로고
    • Characterization of radiation-induced aging in silica-reinforced polysiloxane composites
    • Chien A., Maxwell R., Chambers D., Balazs B., and LeMay J. Characterization of radiation-induced aging in silica-reinforced polysiloxane composites. Radiat Phys Chem 59 (2000) 493-500
    • (2000) Radiat Phys Chem , vol.59 , pp. 493-500
    • Chien, A.1    Maxwell, R.2    Chambers, D.3    Balazs, B.4    LeMay, J.5
  • 11
    • 0038637691 scopus 로고    scopus 로고
    • The effects of gamma-radiation on the thermal, mechanical, and segmental dynamics of a silica filled room temperature vulcanized polysiloxane rubber
    • Maxwell R., Cohenour R., Sung W., Solyom D., and Patel M. The effects of gamma-radiation on the thermal, mechanical, and segmental dynamics of a silica filled room temperature vulcanized polysiloxane rubber. Polym Degrad Stab 80 (2003) 443-450
    • (2003) Polym Degrad Stab , vol.80 , pp. 443-450
    • Maxwell, R.1    Cohenour, R.2    Sung, W.3    Solyom, D.4    Patel, M.5
  • 12
    • 0000427642 scopus 로고
    • Gamma-radiation of para-substituted polystyrenes
    • Burlant W., Serment V., and Neerman J. Gamma-radiation of para-substituted polystyrenes. J Polym Sci 58 (1962) 491-502
    • (1962) J Polym Sci , vol.58 , pp. 491-502
    • Burlant, W.1    Serment, V.2    Neerman, J.3
  • 17
    • 0013385135 scopus 로고
    • NMR and fractal properties of polymeric liquids and gels
    • Cohen Addad J.P. NMR and fractal properties of polymeric liquids and gels. Prog NMR Spectrosc 25 (1993) 1-316
    • (1993) Prog NMR Spectrosc , vol.25 , pp. 1-316
    • Cohen Addad, J.P.1
  • 19
    • 34248662671 scopus 로고    scopus 로고
    • Proton multiple-quantum NMR for the study of chain dynamics and structural constraints in polymeric soft materials
    • Saalwächter K. Proton multiple-quantum NMR for the study of chain dynamics and structural constraints in polymeric soft materials. Prog NMR Spectrosc 51 (2007) 1-35
    • (2007) Prog NMR Spectrosc , vol.51 , pp. 1-35
    • Saalwächter, K.1
  • 20
    • 0041382225 scopus 로고    scopus 로고
    • 1H multiple-quantum nuclear magnetic resonance investigations of molecular order distributions in poly(dimethylsiloxane) networks: evidence for a linear mixing law in bimodal systems
    • 1H multiple-quantum nuclear magnetic resonance investigations of molecular order distributions in poly(dimethylsiloxane) networks: evidence for a linear mixing law in bimodal systems. J Chem Phys 119 (2003) 3468-3482
    • (2003) J Chem Phys , vol.119 , pp. 3468-3482
    • Saalwächter, K.1    Ziegler, P.2    Spyckerelle, O.3    Haidar, B.4    Vidal, A.5    Sommer, J.U.6
  • 21
    • 33744475619 scopus 로고    scopus 로고
    • Chain dynamics in elastomers as investigated by proton multiple-quantum NMR
    • Saalwächter K., and Heuer A. Chain dynamics in elastomers as investigated by proton multiple-quantum NMR. Macromolecules 39 (2006) 3291-3303
    • (2006) Macromolecules , vol.39 , pp. 3291-3303
    • Saalwächter, K.1    Heuer, A.2
  • 22
    • 28144436582 scopus 로고    scopus 로고
    • Chain order and cross-link density of elastomers as investigated by proton multiple-quantum NMR
    • Saalwächter K., Herrero B., and Lopez-Manchado M.A. Chain order and cross-link density of elastomers as investigated by proton multiple-quantum NMR. Macromolecules 38 (2005) 9650-9660
    • (2005) Macromolecules , vol.38 , pp. 9650-9660
    • Saalwächter, K.1    Herrero, B.2    Lopez-Manchado, M.A.3
  • 23
    • 0037162224 scopus 로고    scopus 로고
    • Residual dipolar coupling for the assessment of cross-link density changes in gamma-irradiated silica-PDMS composite materials
    • Maxwell R.S., and Balazs B. Residual dipolar coupling for the assessment of cross-link density changes in gamma-irradiated silica-PDMS composite materials. J Chem Phys 116 (2002) 10492-10502
    • (2002) J Chem Phys , vol.116 , pp. 10492-10502
    • Maxwell, R.S.1    Balazs, B.2
  • 24
    • 0019006999 scopus 로고
    • Crosslink density and solvent swelling of filled and unfilled stocks
    • French D.M. Crosslink density and solvent swelling of filled and unfilled stocks. J Appl Polym Sci 25 (1980) 665-682
    • (1980) J Appl Polym Sci , vol.25 , pp. 665-682
    • French, D.M.1
  • 25
    • 0001721155 scopus 로고
    • Ammonia-induced tensile set and swelling in silica-filled silicone-rubber
    • Vondracek P., and Pouchelon A. Ammonia-induced tensile set and swelling in silica-filled silicone-rubber. Rubber Chem Technol 63 (1990) 202-214
    • (1990) Rubber Chem Technol , vol.63 , pp. 202-214
    • Vondracek, P.1    Pouchelon, A.2
  • 27
    • 0344016993 scopus 로고
    • Production of cyclic molecules during gamma-irradiation of linear polydimethylsiloxane
    • Tanny G.B., and St Pierre L.E. Production of cyclic molecules during gamma-irradiation of linear polydimethylsiloxane. J Polym Sci Polym Lett 9 (1971) 863-868
    • (1971) J Polym Sci Polym Lett , vol.9 , pp. 863-868
    • Tanny, G.B.1    St Pierre, L.E.2
  • 28
    • 0031118655 scopus 로고    scopus 로고
    • Irradiation of plastics: damage and gas evolution
    • Evans D., and Crook M. Irradiation of plastics: damage and gas evolution. MRS Bull 22 (1997) 36-46
    • (1997) MRS Bull , vol.22 , pp. 36-46
    • Evans, D.1    Crook, M.2
  • 29
    • 10544255446 scopus 로고
    • Radiation induced bonding of hexamethyldisiloxane to silica
    • Chahal R.S., and St Pierre L.E. Radiation induced bonding of hexamethyldisiloxane to silica. Can J Chem 47 (1969) 2311-2314
    • (1969) Can J Chem , vol.47 , pp. 2311-2314
    • Chahal, R.S.1    St Pierre, L.E.2
  • 30
    • 0001301155 scopus 로고
    • Dose effects in crosslinking of irradiated polysiloxane
    • Delides C.G., and Shepherd I.W. Dose effects in crosslinking of irradiated polysiloxane. Radiat Phys Chem 10 (1977) 379-385
    • (1977) Radiat Phys Chem , vol.10 , pp. 379-385
    • Delides, C.G.1    Shepherd, I.W.2
  • 31
    • 0024903119 scopus 로고
    • The influence of irradiation temperature and oxygen on crosslink formation and segment mobility in gamma-irradiated polydimethylsiloxanes
    • Menhofer H., Zluticky J., and Heusinger H. The influence of irradiation temperature and oxygen on crosslink formation and segment mobility in gamma-irradiated polydimethylsiloxanes. Radiat Phys Chem 33 (1989) 561-566
    • (1989) Radiat Phys Chem , vol.33 , pp. 561-566
    • Menhofer, H.1    Zluticky, J.2    Heusinger, H.3
  • 33
    • 3042683473 scopus 로고    scopus 로고
    • Studies on the aminolysis of RTV silicone rubber and modifications of degradation products
    • Chang C.L., Don T.M., Lee H.S.J., and Sha Y.O. Studies on the aminolysis of RTV silicone rubber and modifications of degradation products. Polym Degrad Stab 85 (2004) 769-777
    • (2004) Polym Degrad Stab , vol.85 , pp. 769-777
    • Chang, C.L.1    Don, T.M.2    Lee, H.S.J.3    Sha, Y.O.4
  • 34
    • 33745547795 scopus 로고    scopus 로고
    • A novel method for monitoring chemical degradation of crosslinked rubber by stress relaxation under tension
    • Mitra S., Ghanbari-Siahkali A., and Almdal K. A novel method for monitoring chemical degradation of crosslinked rubber by stress relaxation under tension. Polym Degrad Stab 91 (2006) 2520-2526
    • (2006) Polym Degrad Stab , vol.91 , pp. 2520-2526
    • Mitra, S.1    Ghanbari-Siahkali, A.2    Almdal, K.3
  • 35
    • 33745511428 scopus 로고    scopus 로고
    • Chemiluminescence as a condition monitoring method for thermal aging and lifetime prediction of an HTPB elastomer
    • Celina M., Trujillo A.B., Gillen K.T., and Minier L.M. Chemiluminescence as a condition monitoring method for thermal aging and lifetime prediction of an HTPB elastomer. Polym Degrad Stab 91 (2006) 2365-2374
    • (2006) Polym Degrad Stab , vol.91 , pp. 2365-2374
    • Celina, M.1    Trujillo, A.B.2    Gillen, K.T.3    Minier, L.M.4
  • 36
    • 33745610202 scopus 로고    scopus 로고
    • Thermal stability of foamed polysiloxane rubbers: headspace analysis using solid phase microextraction and analysis of solvent extractable material using conventional GC-MS
    • Hall A.D., and Patel M. Thermal stability of foamed polysiloxane rubbers: headspace analysis using solid phase microextraction and analysis of solvent extractable material using conventional GC-MS. Polym Degrad Stab 91 (2006) 2532-2539
    • (2006) Polym Degrad Stab , vol.91 , pp. 2532-2539
    • Hall, A.D.1    Patel, M.2
  • 37
    • 33645163463 scopus 로고    scopus 로고
    • Thermal degradation behaviors of some branched and linear polysiloxanes
    • Zhou W.J., Yang H., Guo X.Z., and Lu J.J. Thermal degradation behaviors of some branched and linear polysiloxanes. Polym Degrad Stab 91 (2006) 1471-1475
    • (2006) Polym Degrad Stab , vol.91 , pp. 1471-1475
    • Zhou, W.J.1    Yang, H.2    Guo, X.Z.3    Lu, J.J.4
  • 39
    • 31444443545 scopus 로고    scopus 로고
    • Initiation of polymer degradation via transfer of infectious species
    • Celina M., Clough R.L., and Jones G.D. Initiation of polymer degradation via transfer of infectious species. Polym Degrad Stab 91 (2006) 1036-1044
    • (2006) Polym Degrad Stab , vol.91 , pp. 1036-1044
    • Celina, M.1    Clough, R.L.2    Jones, G.D.3
  • 40
    • 0002624408 scopus 로고
    • Oxyluminescence from polypropylene
    • Ashby G.E. Oxyluminescence from polypropylene. J Polym Sci 50 (1961) 99-112
    • (1961) J Polym Sci , vol.50 , pp. 99-112
    • Ashby, G.E.1
  • 43
    • 84981375199 scopus 로고
    • Molecular-weight distribution in random cross-linking of polymers - modality of the molecular-weight distribution
    • Tobita H., Yamamoto Y., and Ito K. Molecular-weight distribution in random cross-linking of polymers - modality of the molecular-weight distribution. Macromol Theor Simul 3 (1994) 1033-1049
    • (1994) Macromol Theor Simul , vol.3 , pp. 1033-1049
    • Tobita, H.1    Yamamoto, Y.2    Ito, K.3
  • 44
    • 0041696222 scopus 로고
    • Molecular weight distribution of irradiated polymers
    • Kimura T. Molecular weight distribution of irradiated polymers. J Phys Soc Jpn 17 (1962) 1884-1896
    • (1962) J Phys Soc Jpn , vol.17 , pp. 1884-1896
    • Kimura, T.1
  • 45
    • 56249094478 scopus 로고    scopus 로고
    • Constitutive modeling of radiation effects on the permanent set in a silicone elastomer
    • Maiti A., Gee R., Chinn S., and Maxwell R.S. Constitutive modeling of radiation effects on the permanent set in a silicone elastomer. Polym Degrad Stab 93 (2008) 2226-2229
    • (2008) Polym Degrad Stab , vol.93 , pp. 2226-2229
    • Maiti, A.1    Gee, R.2    Chinn, S.3    Maxwell, R.S.4


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.