메뉴 건너뛰기




Volumn 51, Issue 1, 2007, Pages 1-35

Proton multiple-quantum NMR for the study of chain dynamics and structural constraints in polymeric soft materials

Author keywords

Double quantum NMR; Elastomers; Networks; Poly(butadiene); Poly(dimethylsiloxane); Poly(isoprene); Polymer dynamics; Residual dipolar couplings; Rubber; Swelling; Transverse relaxation

Indexed keywords

CHAIN LENGTH; CORRELATION METHODS; INTERPENETRATING POLYMER NETWORKS; MAGNETIC MOMENTS; MAGNETIZATION; NUCLEAR MAGNETIC RESONANCE; POLYBUTADIENES; POLYDIMETHYLSILOXANE; POLYISOPRENES; QUANTUM THEORY;

EID: 34248662671     PISSN: 00796565     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.pnmrs.2007.01.001     Document Type: Review
Times cited : (369)

References (137)
  • 2
    • 0008628544 scopus 로고
    • The tube concept of macromolecular liquids in the light of NMR experiments
    • Kimmich R., Schnur G., and Köpf M. The tube concept of macromolecular liquids in the light of NMR experiments. Progr. NMR Spectrosc. 20 (1988) 385-421
    • (1988) Progr. NMR Spectrosc. , vol.20 , pp. 385-421
    • Kimmich, R.1    Schnur, G.2    Köpf, M.3
  • 4
    • 0037016104 scopus 로고    scopus 로고
    • Influence of cross-link density and deformation on the NMR relaxation dispersion of natural rubber
    • Kariyo S., and Stapf S. Influence of cross-link density and deformation on the NMR relaxation dispersion of natural rubber. Macromolecules 35 (2002) 9253-9255
    • (2002) Macromolecules , vol.35 , pp. 9253-9255
    • Kariyo, S.1    Stapf, S.2
  • 5
    • 5044234845 scopus 로고    scopus 로고
    • Polymer chain dynamics and NMR
    • Kimmich R., and Fatkullin N. Polymer chain dynamics and NMR. Adv. Polym. Sci. 170 (2004) 1-113
    • (2004) Adv. Polym. Sci. , vol.170 , pp. 1-113
    • Kimmich, R.1    Fatkullin, N.2
  • 6
    • 0023996852 scopus 로고
    • Local dynamics of poly(cis-1,4-butadiene) studied by coupled spin relaxation
    • Fuson M.M., and Grant D.M. Local dynamics of poly(cis-1,4-butadiene) studied by coupled spin relaxation. Macromolecules 21 (1988) 944-949
    • (1988) Macromolecules , vol.21 , pp. 944-949
    • Fuson, M.M.1    Grant, D.M.2
  • 8
    • 0038588840 scopus 로고
    • Effect of the anisotropic chain motion in molten polymers: the solidlike contribution of the nonzero average dipolar coupling to NMR signals theoretical description
    • Cohen-Addad J.P. Effect of the anisotropic chain motion in molten polymers: the solidlike contribution of the nonzero average dipolar coupling to NMR signals theoretical description. J. Chem. Phys. 60 (1973) 2440-2453
    • (1973) J. Chem. Phys. , vol.60 , pp. 2440-2453
    • Cohen-Addad, J.P.1
  • 10
    • 0041754425 scopus 로고
    • Analysis of crosslinked and entangled polymer networks as studied by nuclear magnetic resonance
    • Charlesby A., Folland R., and Steven J.H. Analysis of crosslinked and entangled polymer networks as studied by nuclear magnetic resonance. Proc. R. Soc. Lond. A 355 (1977) 189-207
    • (1977) Proc. R. Soc. Lond. A , vol.355 , pp. 189-207
    • Charlesby, A.1    Folland, R.2    Steven, J.H.3
  • 11
    • 0001573615 scopus 로고
    • Effect of slow molecular motion on damping of transverse nuclear magnetization in amorphous polymers
    • Fedotov V.D., Chernov V.M., and Khazanovich T.N. Effect of slow molecular motion on damping of transverse nuclear magnetization in amorphous polymers. Vysokomol. Soed. A20 (1978) 919-926
    • (1978) Vysokomol. Soed. , vol.A20 , pp. 919-926
    • Fedotov, V.D.1    Chernov, V.M.2    Khazanovich, T.N.3
  • 12
    • 5644220789 scopus 로고
    • Slow dynamics of entangled polydimethylsiloxane chains observed by proton transverse magnetic relaxation
    • Cohen-Addad J.P., Domard M., and Boileau S. Slow dynamics of entangled polydimethylsiloxane chains observed by proton transverse magnetic relaxation. J. Chem. Phys. 75 (1981) 4107-4114
    • (1981) J. Chem. Phys. , vol.75 , pp. 4107-4114
    • Cohen-Addad, J.P.1    Domard, M.2    Boileau, S.3
  • 14
    • 0026142076 scopus 로고
    • Nature of proton nmr transverse relaxation function of polyethylene melts. 1. Monodispersed polyethylenes
    • Brereton M.G., Ward I.M., Boden N., and Wright P. Nature of proton nmr transverse relaxation function of polyethylene melts. 1. Monodispersed polyethylenes. Macromolecules 24 (1991) 2068-2074
    • (1991) Macromolecules , vol.24 , pp. 2068-2074
    • Brereton, M.G.1    Ward, I.M.2    Boden, N.3    Wright, P.4
  • 16
    • 0013385135 scopus 로고
    • NMR and fractal properties of polymeric liquids and gels
    • Cohen-Addad J.P. NMR and fractal properties of polymeric liquids and gels. Progr. NMR Spectrosc. 25 (1993) 1-316
    • (1993) Progr. NMR Spectrosc. , vol.25 , pp. 1-316
    • Cohen-Addad, J.P.1
  • 17
    • 0030576827 scopus 로고    scopus 로고
    • Effect of residual dipolar interactions on the NMR relaxation in cross-linked elastomers
    • Sotta P., Fülber C., Demco D.E., Blümich B., and Spiess H.W. Effect of residual dipolar interactions on the NMR relaxation in cross-linked elastomers. Macromolecules 29 (1996) 6222-6230
    • (1996) Macromolecules , vol.29 , pp. 6222-6230
    • Sotta, P.1    Fülber, C.2    Demco, D.E.3    Blümich, B.4    Spiess, H.W.5
  • 18
    • 0037052436 scopus 로고    scopus 로고
    • Relationship between the transverse NMR decay and the dipolar interaction in elastomers: a comparison of two models
    • Knörgen M., Menge H., Hempel G., Schneider H., and Ries M.E. Relationship between the transverse NMR decay and the dipolar interaction in elastomers: a comparison of two models. Polymer 43 (2002) 4091-4096
    • (2002) Polymer , vol.43 , pp. 4091-4096
    • Knörgen, M.1    Menge, H.2    Hempel, G.3    Schneider, H.4    Ries, M.E.5
  • 19
    • 0344976127 scopus 로고    scopus 로고
    • Litvinov V.M., and De P.P. (Eds), Rapra Technology Ltd., Shawbury
    • In: Litvinov V.M., and De P.P. (Eds). Spectroscopy of Rubbers and Rubbery Materials (2002), Rapra Technology Ltd., Shawbury
    • (2002) Spectroscopy of Rubbers and Rubbery Materials
  • 20
    • 0037665254 scopus 로고    scopus 로고
    • The dynamics and physical structure of polymers above the glass transition-transverse relaxation studies of linear chains, star polymers and networks
    • Klein P.G., and Ries M.E. The dynamics and physical structure of polymers above the glass transition-transverse relaxation studies of linear chains, star polymers and networks. Progr. NMR Spectrosc. 42 (2003) 31-52
    • (2003) Progr. NMR Spectrosc. , vol.42 , pp. 31-52
    • Klein, P.G.1    Ries, M.E.2
  • 21
    • 0020193548 scopus 로고
    • Single chain diffusion process and proton magnetic relaxation in polymer melts
    • Cohen-Addad J.P. Single chain diffusion process and proton magnetic relaxation in polymer melts. J. Phys. 43 (1982) 1509-1528
    • (1982) J. Phys. , vol.43 , pp. 1509-1528
    • Cohen-Addad, J.P.1
  • 22
    • 0020735842 scopus 로고
    • Strongly entangled polymer chains in a melt. Description of n.m.r. properties associated with a submolecule model
    • Cohen-Addad J.P., and Dypeyre R. Strongly entangled polymer chains in a melt. Description of n.m.r. properties associated with a submolecule model. Polymer 24 (1983) 400-408
    • (1983) Polymer , vol.24 , pp. 400-408
    • Cohen-Addad, J.P.1    Dypeyre, R.2
  • 23
    • 0024733879 scopus 로고
    • NMR transverse relaxation function calculated for the Rouse model
    • Brereton M.G. NMR transverse relaxation function calculated for the Rouse model. Macromolecules 22 (1989) 3667-3674
    • (1989) Macromolecules , vol.22 , pp. 3667-3674
    • Brereton, M.G.1
  • 24
    • 0025388049 scopus 로고
    • NMR transverse relaxation function calculated for constrained polymer chains: application to entanglements and networks
    • Brereton M.G. NMR transverse relaxation function calculated for constrained polymer chains: application to entanglements and networks. Macromolecules 23 (1990) 1119-1131
    • (1990) Macromolecules , vol.23 , pp. 1119-1131
    • Brereton, M.G.1
  • 26
    • 0000266537 scopus 로고
    • Molecular motion anisotropy as reflected by a "Pseudosolid" nuclear spin echo: observation of chain constraints in molten cis-1,4-polybutadiene
    • Cohen-Addad J.P., and Vogin R. Molecular motion anisotropy as reflected by a "Pseudosolid" nuclear spin echo: observation of chain constraints in molten cis-1,4-polybutadiene. Phys. Rev. Lett. 33 (1974) 940-943
    • (1974) Phys. Rev. Lett. , vol.33 , pp. 940-943
    • Cohen-Addad, J.P.1    Vogin, R.2
  • 27
    • 0041974919 scopus 로고    scopus 로고
    • End-linked calibrated polypropylene-oxide chains. NMR approach to segmental fluctuations
    • Cohen-Addad J.P., Pellicioli L., and Nusselder J.J.H. End-linked calibrated polypropylene-oxide chains. NMR approach to segmental fluctuations. Polym. Gels Netw. 5 (1997) 201-221
    • (1997) Polym. Gels Netw. , vol.5 , pp. 201-221
    • Cohen-Addad, J.P.1    Pellicioli, L.2    Nusselder, J.J.H.3
  • 28
    • 0019533970 scopus 로고
    • Pseudo-solid echoes of proton and deuteron NMR in polyethylene melts
    • Collignon J., Sillescu H., and Spiess H.W. Pseudo-solid echoes of proton and deuteron NMR in polyethylene melts. Colloid Polym. Sci. 259 (1981) 220-226
    • (1981) Colloid Polym. Sci. , vol.259 , pp. 220-226
    • Collignon, J.1    Sillescu, H.2    Spiess, H.W.3
  • 29
    • 0030834664 scopus 로고    scopus 로고
    • Molecular ordering and the direct measurement of weak proton-proton dipolar interactions in a rubber network
    • Callaghan P.T., and Samulski E.T. Molecular ordering and the direct measurement of weak proton-proton dipolar interactions in a rubber network. Macromolecules 30 (1997) 113-122
    • (1997) Macromolecules , vol.30 , pp. 113-122
    • Callaghan, P.T.1    Samulski, E.T.2
  • 30
    • 0031146904 scopus 로고    scopus 로고
    • A simplified approach to the interpretation of nuclear spin correlations in entangled polymeric liquids
    • Ball R.C., Callaghan P.T., and Samulski E.T. A simplified approach to the interpretation of nuclear spin correlations in entangled polymeric liquids. J. Chem. Phys. 106 (1997) 7352-7361
    • (1997) J. Chem. Phys. , vol.106 , pp. 7352-7361
    • Ball, R.C.1    Callaghan, P.T.2    Samulski, E.T.3
  • 31
    • 0000153162 scopus 로고    scopus 로고
    • Characterization of polymer networks using the dipolar correlation effect on the stimulated echo and field-cycling nuclear-magnetic resonance relaxometry
    • Fischer E., Grinberg F., Kimmich R., and Hafner S. Characterization of polymer networks using the dipolar correlation effect on the stimulated echo and field-cycling nuclear-magnetic resonance relaxometry. J. Chem. Phys. 109 (1998) 846-854
    • (1998) J. Chem. Phys. , vol.109 , pp. 846-854
    • Fischer, E.1    Grinberg, F.2    Kimmich, R.3    Hafner, S.4
  • 32
    • 0001767162 scopus 로고    scopus 로고
    • Influence of the cross-link density and the filler content on segment dynamics in dry and swollen natural rubber studied by the NMR dipolar-correlation effect
    • Grinberg F., Garbarczyk M., and Kuhn W. Influence of the cross-link density and the filler content on segment dynamics in dry and swollen natural rubber studied by the NMR dipolar-correlation effect. J. Chem. Phys. 111 (1999) 11222-11231
    • (1999) J. Chem. Phys. , vol.111 , pp. 11222-11231
    • Grinberg, F.1    Garbarczyk, M.2    Kuhn, W.3
  • 34
    • 0001687258 scopus 로고
    • An exact expression for the transverse nuclear magnetic resoance relaxation of a dynamic scale invariant polymer chain governed by a single relaxation time
    • Brereton M.G. An exact expression for the transverse nuclear magnetic resoance relaxation of a dynamic scale invariant polymer chain governed by a single relaxation time. J. Chem. Phys. 94 (1991) 2136-2142
    • (1991) J. Chem. Phys. , vol.94 , pp. 2136-2142
    • Brereton, M.G.1
  • 36
    • 33744475619 scopus 로고    scopus 로고
    • Chain dynamics in elastomers as investigated by proton multiple-quantum NMR
    • Saalwächter K., and Heuer A. Chain dynamics in elastomers as investigated by proton multiple-quantum NMR. Macromolecules 39 (2006) 3291-3303
    • (2006) Macromolecules , vol.39 , pp. 3291-3303
    • Saalwächter, K.1    Heuer, A.2
  • 37
    • 0041382225 scopus 로고    scopus 로고
    • 1H multiple-quantum nuclear magnetic resonance investigations of molecular order distributions in poly(dimethylsiloxane) networks: Evidence for a linear mixing law in bimodal systems
    • 1H multiple-quantum nuclear magnetic resonance investigations of molecular order distributions in poly(dimethylsiloxane) networks: Evidence for a linear mixing law in bimodal systems. J. Chem. Phys. 119 (2003) 3468-3482
    • (2003) J. Chem. Phys. , vol.119 , pp. 3468-3482
    • Saalwächter, K.1    Ziegler, P.2    Spyckerelle, O.3    Haidar, B.4    Vidal, A.5    Sommer, J.-U.6
  • 38
    • 34347098764 scopus 로고
    • Beziehungen zwischen elastischen Konstanten und Dehnungsdoppelbrechung hochelastischer Stoffe
    • Kuhn W., and Grün F. Beziehungen zwischen elastischen Konstanten und Dehnungsdoppelbrechung hochelastischer Stoffe. Kolloid-Z. 101 (1942) 248-271
    • (1942) Kolloid-Z. , vol.101 , pp. 248-271
    • Kuhn, W.1    Grün, F.2
  • 40
    • 0037008065 scopus 로고    scopus 로고
    • Rescaling approach to molecular orientation for NMR and optical properties of polymer networks
    • Ries M.E., Brereton M.G., Ward I.M., Cail J.I., and Stepto R.F.T. Rescaling approach to molecular orientation for NMR and optical properties of polymer networks. Macromolecules 35 (2002) 5665-5669
    • (2002) Macromolecules , vol.35 , pp. 5665-5669
    • Ries, M.E.1    Brereton, M.G.2    Ward, I.M.3    Cail, J.I.4    Stepto, R.F.T.5
  • 41
    • 0025698311 scopus 로고
    • Uniaxiality induced in a strained poly(dimethylsiloxane) network
    • Sotta P., and Deloche B. Uniaxiality induced in a strained poly(dimethylsiloxane) network. Macromolecules 23 (1990) 1999-2007
    • (1990) Macromolecules , vol.23 , pp. 1999-2007
    • Sotta, P.1    Deloche, B.2
  • 42
    • 0027558599 scopus 로고
    • NMR study of the molecular anisotropy induced in a strained rubber network
    • Brereton M.G. NMR study of the molecular anisotropy induced in a strained rubber network. Macromolecules 26 (1993) 1152-1157
    • (1993) Macromolecules , vol.26 , pp. 1152-1157
    • Brereton, M.G.1
  • 43
    • 0031209138 scopus 로고    scopus 로고
    • Nuclear magnetic resonance line shape from strained Gaussian networks
    • Warner M., Callaghan P.T., and Samulski E.T. Nuclear magnetic resonance line shape from strained Gaussian networks. Macromolecules 30 (1997) 4733-4736
    • (1997) Macromolecules , vol.30 , pp. 4733-4736
    • Warner, M.1    Callaghan, P.T.2    Samulski, E.T.3
  • 45
    • 0033154099 scopus 로고    scopus 로고
    • Contributions to the total orientation of deformed elastomers arising from the network structure and chain interactions as measured by NMR
    • Ries M.E., Brereton M.G., Klein P.G., Ward I.M., Ekanayake P., Menge H., and Schneider H. Contributions to the total orientation of deformed elastomers arising from the network structure and chain interactions as measured by NMR. Macromolecules 32 (1999) 4961-4968
    • (1999) Macromolecules , vol.32 , pp. 4961-4968
    • Ries, M.E.1    Brereton, M.G.2    Klein, P.G.3    Ward, I.M.4    Ekanayake, P.5    Menge, H.6    Schneider, H.7
  • 46
    • 0000142456 scopus 로고
    • Multiple-quantum NMR studies of clustering in solids
    • Baum J., and Pines A. Multiple-quantum NMR studies of clustering in solids. J. Am. Chem. Soc. 108 (1986) 7447-7454
    • (1986) J. Am. Chem. Soc. , vol.108 , pp. 7447-7454
    • Baum, J.1    Pines, A.2
  • 47
    • 0344430130 scopus 로고    scopus 로고
    • Detection of heterogeneities in dry and swollen polymer networks by proton low-field NMR spectroscopy
    • Saalwächter K. Detection of heterogeneities in dry and swollen polymer networks by proton low-field NMR spectroscopy. J. Am. Chem. Soc. 125 (2003) 14684-14685
    • (2003) J. Am. Chem. Soc. , vol.125 , pp. 14684-14685
    • Saalwächter, K.1
  • 48
    • 0037323982 scopus 로고    scopus 로고
    • Chain orientation and slow dynamics in elastomers by mixed magic-Hahn echo decays
    • Fechete R., Demco D.E., and Blümich B. Chain orientation and slow dynamics in elastomers by mixed magic-Hahn echo decays. J. Chem. Phys. 118 (2003) 2411-2421
    • (2003) J. Chem. Phys. , vol.118 , pp. 2411-2421
    • Fechete, R.1    Demco, D.E.2    Blümich, B.3
  • 49
    • 0001273648 scopus 로고    scopus 로고
    • 1H dipolar-encoded longitudinal magnetization, double- and triple-quantum nuclear magnetic resonance in cross-linked elastomers
    • 1H dipolar-encoded longitudinal magnetization, double- and triple-quantum nuclear magnetic resonance in cross-linked elastomers. J. Chem. Phys. 111 (1999) 402-415
    • (1999) J. Chem. Phys. , vol.111 , pp. 402-415
    • Schneider, M.1    Gasper, L.2    Demco, D.E.3    Blümich, B.4
  • 51
    • 13244278055 scopus 로고    scopus 로고
    • Chain order in filled SBR elastomers: a proton multiple-quantum NMR study
    • Saalwächter K., Klüppel M., Luo H., and Schneider H. Chain order in filled SBR elastomers: a proton multiple-quantum NMR study. Appl. Magn. Reson. 27 (2004) 401-417
    • (2004) Appl. Magn. Reson. , vol.27 , pp. 401-417
    • Saalwächter, K.1    Klüppel, M.2    Luo, H.3    Schneider, H.4
  • 52
    • 9744254863 scopus 로고    scopus 로고
    • Swelling heterogeneities in end-linked model networks: a combined proton multiple-quantum NMR and computer simulation study
    • Saalwächter K., Kleinschmidt F., and Sommer J.-U. Swelling heterogeneities in end-linked model networks: a combined proton multiple-quantum NMR and computer simulation study. Macromolecules 37 (2004) 8556-8568
    • (2004) Macromolecules , vol.37 , pp. 8556-8568
    • Saalwächter, K.1    Kleinschmidt, F.2    Sommer, J.-U.3
  • 53
    • 14644418436 scopus 로고    scopus 로고
    • Artifacts in transverse proton NMR relaxation studies of elastomers
    • Saalwächter K. Artifacts in transverse proton NMR relaxation studies of elastomers. Macromolecules 38 (2005) 1508-1512
    • (2005) Macromolecules , vol.38 , pp. 1508-1512
    • Saalwächter, K.1
  • 54
    • 0032671157 scopus 로고    scopus 로고
    • 1H NMR spin diffusion coefficients for mobile polymers through transverse relaxation measurements
    • 1H NMR spin diffusion coefficients for mobile polymers through transverse relaxation measurements. Macromolecules 32 (1999) 4686-4691
    • (1999) Macromolecules , vol.32 , pp. 4686-4691
    • Mellinger, F.1    Wilhelm, M.2    Spiess, H.W.3
  • 55
    • 36149017694 scopus 로고
    • Exchange narrowing in paramagnetic resonance
    • Andersen P.W., and Weiss P.R. Exchange narrowing in paramagnetic resonance. Rev. Mod. Phys. 25 (1953) 269-276
    • (1953) Rev. Mod. Phys. , vol.25 , pp. 269-276
    • Andersen, P.W.1    Weiss, P.R.2
  • 56
    • 7644244681 scopus 로고    scopus 로고
    • Study of filled SBR elastomers using NMR and mechanical measurements
    • Luo H., Klüppel M., and Schneider H. Study of filled SBR elastomers using NMR and mechanical measurements. Macromolecules 37 (2004) 8000-8009
    • (2004) Macromolecules , vol.37 , pp. 8000-8009
    • Luo, H.1    Klüppel, M.2    Schneider, H.3
  • 57
    • 0029309476 scopus 로고
    • The effect of field inhomogeneities and molecular diffusion on the NMR transverse relaxation behavior of polymer melts
    • Whittaker A.K., Bremner T., and Zelaya F.O. The effect of field inhomogeneities and molecular diffusion on the NMR transverse relaxation behavior of polymer melts. Polymer 36 (1995) 2159-2164
    • (1995) Polymer , vol.36 , pp. 2159-2164
    • Whittaker, A.K.1    Bremner, T.2    Zelaya, F.O.3
  • 58
    • 18744383659 scopus 로고    scopus 로고
    • Chemical shift-related artifacts in NMR determinations of proton residual dipolar couplings in elastomers
    • Saalwächter K., Herrero B., and López-Manchado M.A. Chemical shift-related artifacts in NMR determinations of proton residual dipolar couplings in elastomers. Macromolecules 38 (2005) 4040-4042
    • (2005) Macromolecules , vol.38 , pp. 4040-4042
    • Saalwächter, K.1    Herrero, B.2    López-Manchado, M.A.3
  • 60
    • 28144436582 scopus 로고    scopus 로고
    • Chain order and crosslink density of elastomers as investigated by proton multiple-quantum NMR
    • Saalwächter K., Herrero B., and López-Manchado M.A. Chain order and crosslink density of elastomers as investigated by proton multiple-quantum NMR. Macromolecules 38 (2005) 9650-9660
    • (2005) Macromolecules , vol.38 , pp. 9650-9660
    • Saalwächter, K.1    Herrero, B.2    López-Manchado, M.A.3
  • 62
    • 33644540466 scopus 로고    scopus 로고
    • Multiple-quantum NMR on structure, orientation, morphology and dynamics of polymers, biomolecules and ordered tissues
    • Buda A.A., Demco D.E., Bertmer M., and Blümich B. Multiple-quantum NMR on structure, orientation, morphology and dynamics of polymers, biomolecules and ordered tissues. Comptes Rendus Chimie 9 (2006) 346-356
    • (2006) Comptes Rendus Chimie , vol.9 , pp. 346-356
    • Buda, A.A.1    Demco, D.E.2    Bertmer, M.3    Blümich, B.4
  • 63
    • 2942529159 scopus 로고    scopus 로고
    • Enhanced sensitivity to residual dipolar couplings of elastomers by higher-order multiple-quantum NMR
    • Fechete R., Demco D.E., and Blümich B. Enhanced sensitivity to residual dipolar couplings of elastomers by higher-order multiple-quantum NMR. J. Magn. Reson. 169 (2004) 19-26
    • (2004) J. Magn. Reson. , vol.169 , pp. 19-26
    • Fechete, R.1    Demco, D.E.2    Blümich, B.3
  • 64
    • 10444227174 scopus 로고    scopus 로고
    • Multispin moments edited by multiple-quantum NMR: application to elastomers
    • Voda M.A., Demco D.E., Perlo J., Orza R.A., and Blümich B. Multispin moments edited by multiple-quantum NMR: application to elastomers. J. Magn. Reson. 172 (2005) 98-109
    • (2005) J. Magn. Reson. , vol.172 , pp. 98-109
    • Voda, M.A.1    Demco, D.E.2    Perlo, J.3    Orza, R.A.4    Blümich, B.5
  • 65
    • 33646620078 scopus 로고
    • Time-reversal experiments in dipolar-coupled spin systems
    • Rhim W.-K., Pines A., and Waugh J.S. Time-reversal experiments in dipolar-coupled spin systems. Phys. Rev. B 3 (1971) 684-696
    • (1971) Phys. Rev. B , vol.3 , pp. 684-696
    • Rhim, W.-K.1    Pines, A.2    Waugh, J.S.3
  • 66
    • 33947577104 scopus 로고
    • Solid-state NMR imaging by magic sandwich echoes
    • Matsui S. Solid-state NMR imaging by magic sandwich echoes. Chem. Phys. Lett. 179 (1991) 187-190
    • (1991) Chem. Phys. Lett. , vol.179 , pp. 187-190
    • Matsui, S.1
  • 67
    • 0001152650 scopus 로고
    • Origin of the self-reinforcement in PDMS bimodal networks
    • Smith T.L., Haidar B., and Hedrick J.L. Origin of the self-reinforcement in PDMS bimodal networks. Rubber Chem. Technol. 63 (1990) 256-264
    • (1990) Rubber Chem. Technol. , vol.63 , pp. 256-264
    • Smith, T.L.1    Haidar, B.2    Hedrick, J.L.3
  • 68
    • 0037126746 scopus 로고    scopus 로고
    • Topological structure and nonaffine swelling of bimodal polymer networks
    • Sommer J.U., and Lay S. Topological structure and nonaffine swelling of bimodal polymer networks. Macromolecules 35 (2002) 9832-9843
    • (2002) Macromolecules , vol.35 , pp. 9832-9843
    • Sommer, J.U.1    Lay, S.2
  • 69
    • 0032613686 scopus 로고    scopus 로고
    • Comparison of structural properties of different polymer network types as obtained by computer simulations
    • Lay S., Sommer J.-U., and Blumen A. Comparison of structural properties of different polymer network types as obtained by computer simulations. J. Chem. Phys. 110 (1999) 12173-12182
    • (1999) J. Chem. Phys. , vol.110 , pp. 12173-12182
    • Lay, S.1    Sommer, J.-U.2    Blumen, A.3
  • 70
    • 1842425286 scopus 로고    scopus 로고
    • Concentrated solutions of partly deuterated triblock polybutadiene. Segmental analysis of NMR properties
    • Schillé E., Cohen Addad J.-P., and Guillermo A. Concentrated solutions of partly deuterated triblock polybutadiene. Segmental analysis of NMR properties. Macromolecules 37 (2004) 2144-2150
    • (2004) Macromolecules , vol.37 , pp. 2144-2150
    • Schillé, E.1    Cohen Addad, J.-P.2    Guillermo, A.3
  • 71
    • 0020203252 scopus 로고
    • Segmental order in a uniaxially constrained polydimethylsiloxane network-A deuterium magnetic-resonance study
    • Deloche B., Beltzung M., and Herz J. Segmental order in a uniaxially constrained polydimethylsiloxane network-A deuterium magnetic-resonance study. J. Phys. (Paris) Lett. 43 (1982) L763-L769
    • (1982) J. Phys. (Paris) Lett. , vol.43
    • Deloche, B.1    Beltzung, M.2    Herz, J.3
  • 72
    • 0000881037 scopus 로고
    • Evidence of nonaffine and inhomogeneous deformation of network chains in strained rubber-elastic networks by deuterium magnetic resonance
    • Gronski W., Stadler R., and Jacobi M.M. Evidence of nonaffine and inhomogeneous deformation of network chains in strained rubber-elastic networks by deuterium magnetic resonance. Macromolecules 17 (1984) 741-748
    • (1984) Macromolecules , vol.17 , pp. 741-748
    • Gronski, W.1    Stadler, R.2    Jacobi, M.M.3
  • 73
    • 0000335302 scopus 로고
    • Evidence for short-range orientational couplings between chain segments in strained rubbers: a deuterium magnetic resonance investigation
    • Sotta P., Deloche B., Herz J., Lapp A., Durand D., and Rabadeux J.-C. Evidence for short-range orientational couplings between chain segments in strained rubbers: a deuterium magnetic resonance investigation. Macromolecules 20 (1987) 2769-2774
    • (1987) Macromolecules , vol.20 , pp. 2769-2774
    • Sotta, P.1    Deloche, B.2    Herz, J.3    Lapp, A.4    Durand, D.5    Rabadeux, J.-C.6
  • 74
    • 42749107058 scopus 로고    scopus 로고
    • Strain-dependent localization, microscopic deformations, and macroscopic normal tensions in model polymer networks
    • Svaneborg C., Grest G.S., and Everaers R. Strain-dependent localization, microscopic deformations, and macroscopic normal tensions in model polymer networks. Phys. Rev. Lett. 93 (2004) 257801
    • (2004) Phys. Rev. Lett. , vol.93 , pp. 257801
    • Svaneborg, C.1    Grest, G.S.2    Everaers, R.3
  • 75
    • 18644382401 scopus 로고    scopus 로고
    • Disorder effects on the strain response of model polymer networks
    • Svaneborg C., Grest G.S., and Everaers R. Disorder effects on the strain response of model polymer networks. Polymer 46 (2005) 4283-4295
    • (2005) Polymer , vol.46 , pp. 4283-4295
    • Svaneborg, C.1    Grest, G.S.2    Everaers, R.3
  • 76
    • 0001410396 scopus 로고
    • Short-range nematic-like orientational order in strained elastomers: a deuterium magnetic resonance study
    • Deloche B., and Samulski E.T. Short-range nematic-like orientational order in strained elastomers: a deuterium magnetic resonance study. Macromolecules 14 (1981) 575-581
    • (1981) Macromolecules , vol.14 , pp. 575-581
    • Deloche, B.1    Samulski, E.T.2
  • 77
    • 0020703224 scopus 로고
    • Investigations of polymer chains in oriented fluid phases with deuterium nuclear magnetic resonance
    • Samulski E.T. Investigations of polymer chains in oriented fluid phases with deuterium nuclear magnetic resonance. Polymer 26 (1985) 177-189
    • (1985) Polymer , vol.26 , pp. 177-189
    • Samulski, E.T.1
  • 78
    • 0006276745 scopus 로고
    • Oligomers as molecular probes of orientational order in strained elastomeric networks
    • Jacobi M.M., Stadler R., and Gronski W. Oligomers as molecular probes of orientational order in strained elastomeric networks. Macromolecules 19 (1986) 2884-2887
    • (1986) Macromolecules , vol.19 , pp. 2884-2887
    • Jacobi, M.M.1    Stadler, R.2    Gronski, W.3
  • 82
    • 27744440571 scopus 로고    scopus 로고
    • Segmental order in endlinked polymer networks: a Monte Carlo study
    • Sommer J.-U., and Saalwächter K. Segmental order in endlinked polymer networks: a Monte Carlo study. Eur. Phys. J. E 18 (2005) 167-182
    • (2005) Eur. Phys. J. E , vol.18 , pp. 167-182
    • Sommer, J.-U.1    Saalwächter, K.2
  • 83
    • 1642496767 scopus 로고    scopus 로고
    • When does a molecules become a polymer?
    • Ding Y., Kisliuk A., and Sokolov A.P. When does a molecules become a polymer?. Macromolecules 37 (2004) 161-166
    • (2004) Macromolecules , vol.37 , pp. 161-166
    • Ding, Y.1    Kisliuk, A.2    Sokolov, A.P.3
  • 84
    • 0041754424 scopus 로고    scopus 로고
    • Analytical solutions for multiple-quantum-coherence dynamics among two or three dipolar-coupled, spin-frac(1, 2) nuclei
    • Roy A.K., and Gleason K.K. Analytical solutions for multiple-quantum-coherence dynamics among two or three dipolar-coupled, spin-frac(1, 2) nuclei. J. Magn. Reson. A 120 (1996) 139-147
    • (1996) J. Magn. Reson. A , vol.120 , pp. 139-147
    • Roy, A.K.1    Gleason, K.K.2
  • 85
    • 0037136185 scopus 로고    scopus 로고
    • 1H double-quantum magic-angle spinning NMR spectroscopy
    • 1H double-quantum magic-angle spinning NMR spectroscopy. Chem. Phys. Lett. 362 (2002) 331-340
    • (2002) Chem. Phys. Lett. , vol.362 , pp. 331-340
    • Saalwächter, K.1
  • 87
    • 0024302277 scopus 로고
    • NMR and gel elasticity interrelationship
    • Cohen-Addad J.P. NMR and gel elasticity interrelationship. Macromolecules 22 (1989) 147-151
    • (1989) Macromolecules , vol.22 , pp. 147-151
    • Cohen-Addad, J.P.1
  • 88
    • 0024664370 scopus 로고
    • 1H-NMR-spin-spin relaxation in cross-linked SBR with and without carbon black filling
    • 1H-NMR-spin-spin relaxation in cross-linked SBR with and without carbon black filling. Polym. Bull. 21 (1989) 475-482
    • (1989) Polym. Bull. , vol.21 , pp. 475-482
    • Simon, G.1    Götschmann, B.2    Matzen, D.3    Schneider, H.4
  • 89
    • 0030420029 scopus 로고    scopus 로고
    • Two-dimensional proton magnetization-exchange NMR spectroscopy in cross-linked elastomers
    • Demco D.E., Hafner S., Fülber C., Graf R., and Spiess H.W. Two-dimensional proton magnetization-exchange NMR spectroscopy in cross-linked elastomers. J. Chem. Phys. 105 (1996) 11285-11296
    • (1996) J. Chem. Phys. , vol.105 , pp. 11285-11296
    • Demco, D.E.1    Hafner, S.2    Fülber, C.3    Graf, R.4    Spiess, H.W.5
  • 90
    • 0013373592 scopus 로고    scopus 로고
    • Evidence for a linear nmr-elasticity interrelationship in polymeric gels
    • Cohen-Addad J.P., Thanh B.P., and Montes H. Evidence for a linear nmr-elasticity interrelationship in polymeric gels. Macromolecules 30 (1997) 4374-4380
    • (1997) Macromolecules , vol.30 , pp. 4374-4380
    • Cohen-Addad, J.P.1    Thanh, B.P.2    Montes, H.3
  • 92
    • 0035811337 scopus 로고    scopus 로고
    • 13C NMR spectroscopy, and dynamic mechanical experiments
    • 13C NMR spectroscopy, and dynamic mechanical experiments. Macromolecules 34 (2001) 4051-4060
    • (2001) Macromolecules , vol.34 , pp. 4051-4060
    • Litvinov, V.M.1    Dias, A.A.2
  • 93
    • 0037162224 scopus 로고    scopus 로고
    • Residual dipolar coupling for the assessment of cross-link density changes in γ-irradiated silica-PDMS composite materials
    • Maxwell R.S., and Balazs B. Residual dipolar coupling for the assessment of cross-link density changes in γ-irradiated silica-PDMS composite materials. J. Chem. Phys. 116 (2002) 10492-10502
    • (2002) J. Chem. Phys. , vol.116 , pp. 10492-10502
    • Maxwell, R.S.1    Balazs, B.2
  • 94
    • 0942288559 scopus 로고    scopus 로고
    • 1H multiple-quantum nuclear magnetic resonance investigations of molecular order in polymer networks: II. Intensity decay and restricted slow dynamics
    • 1H multiple-quantum nuclear magnetic resonance investigations of molecular order in polymer networks: II. Intensity decay and restricted slow dynamics. J. Chem. Phys. 120 (2004) 454-664
    • (2004) J. Chem. Phys. , vol.120 , pp. 454-664
    • Saalwächter, K.1
  • 95
    • 0001676099 scopus 로고
    • Long-time dynamics in poly(dimethylsiloxane) networks studied by deuterium nuclear magnetic resonance
    • Sotta P., and Deloche B. Long-time dynamics in poly(dimethylsiloxane) networks studied by deuterium nuclear magnetic resonance. J. Chem. Phys. 100 (1994) 4591-4600
    • (1994) J. Chem. Phys. , vol.100 , pp. 4591-4600
    • Sotta, P.1    Deloche, B.2
  • 96
    • 0000807961 scopus 로고    scopus 로고
    • Synchronous helical pulse sequences in magic-angle spinning nuclear magnetic resonance: Double-quantum recoupling of multiple-spin systems
    • Brinkmann A., Edén M., and Levitt M.H. Synchronous helical pulse sequences in magic-angle spinning nuclear magnetic resonance: Double-quantum recoupling of multiple-spin systems. J. Chem. Phys. 112 (2000) 8539-8554
    • (2000) J. Chem. Phys. , vol.112 , pp. 8539-8554
    • Brinkmann, A.1    Edén, M.2    Levitt, M.H.3
  • 97
    • 0002863631 scopus 로고
    • Volume dependence of the elastic equation of state. 2. Solution-cured poly(dimethylsiloxane)
    • Brotzman R.W., and Eichinger B.E. Volume dependence of the elastic equation of state. 2. Solution-cured poly(dimethylsiloxane). Macromolecules 14 (1981) 1445-1448
    • (1981) Macromolecules , vol.14 , pp. 1445-1448
    • Brotzman, R.W.1    Eichinger, B.E.2
  • 98
    • 0000295467 scopus 로고
    • NMR observation of the swelling process of polydimethylsiloxane networks. Average orientational order of monomeric units
    • Cohen-Addad J.P., Domard M., and Herz J. NMR observation of the swelling process of polydimethylsiloxane networks. Average orientational order of monomeric units. J. Chem. Phys. 76 (1982) 2744-2753
    • (1982) J. Chem. Phys. , vol.76 , pp. 2744-2753
    • Cohen-Addad, J.P.1    Domard, M.2    Herz, J.3
  • 99
    • 0021387974 scopus 로고
    • Polymeric gels. NMR study of elementary chain swelling. Effect of trapped topological constraints
    • Cohen-Addad J.P., Domard M., Lorentz G., and Herz J. Polymeric gels. NMR study of elementary chain swelling. Effect of trapped topological constraints. J. Phys. 45 (1984) 575-586
    • (1984) J. Phys. , vol.45 , pp. 575-586
    • Cohen-Addad, J.P.1    Domard, M.2    Lorentz, G.3    Herz, J.4
  • 100
    • 0024305368 scopus 로고
    • NMR approach to the characterization of the swelling process of polyethylene networks
    • Schmit C., and Cohen-Addad J.P. NMR approach to the characterization of the swelling process of polyethylene networks. Macromolecules 22 (1989) 142-146
    • (1989) Macromolecules , vol.22 , pp. 142-146
    • Schmit, C.1    Cohen-Addad, J.P.2
  • 102
    • 0000263659 scopus 로고
    • Effects of nematic-like interaction in rubber elasticity theory
    • Jarry J.-P., and Monnerie L. Effects of nematic-like interaction in rubber elasticity theory. Macromolecules 12 (1979) 316-320
    • (1979) Macromolecules , vol.12 , pp. 316-320
    • Jarry, J.-P.1    Monnerie, L.2
  • 103
    • 0024091873 scopus 로고
    • Rubber elasticity: a phenomenological approach including orientational correlations
    • Deloche B., and Samulski E.T. Rubber elasticity: a phenomenological approach including orientational correlations. Macromolecules 21 (1988) 3107-3111
    • (1988) Macromolecules , vol.21 , pp. 3107-3111
    • Deloche, B.1    Samulski, E.T.2
  • 104
    • 12044258429 scopus 로고
    • Experimental evidence for inhomogenious swelling and deformation in statistical gels
    • Mendes Jr. E., Lindner P., Buzier M., Boué F., and Bastide J. Experimental evidence for inhomogenious swelling and deformation in statistical gels. Phys. Rev. Lett. 66 (1991) 1595-1598
    • (1991) Phys. Rev. Lett. , vol.66 , pp. 1595-1598
    • Mendes Jr., E.1    Lindner, P.2    Buzier, M.3    Boué, F.4    Bastide, J.5
  • 105
    • 0021505348 scopus 로고
    • Effect of crosslinking density on the orientational order generated in strained networks: A deuterium magnetic resonance study
    • Dubault A., Deloche B., and Herz J. Effect of crosslinking density on the orientational order generated in strained networks: A deuterium magnetic resonance study. Polymer 25 (1984) 1405-1410
    • (1984) Polymer , vol.25 , pp. 1405-1410
    • Dubault, A.1    Deloche, B.2    Herz, J.3
  • 106
    • 0000004798 scopus 로고
    • Effects of trapped entanglements on the chain ordering in strained rubbers: a deuterium magnetic resonance investigation
    • Dubault A., Deloche B., and Herz J. Effects of trapped entanglements on the chain ordering in strained rubbers: a deuterium magnetic resonance investigation. Macromolecules 20 (1987) 2096-2099
    • (1987) Macromolecules , vol.20 , pp. 2096-2099
    • Dubault, A.1    Deloche, B.2    Herz, J.3
  • 107
    • 0038190941 scopus 로고    scopus 로고
    • Biaxial deformation of a polymer network measured via deuteron quadrupolar interactions
    • Callaghan P.T., and Samulski E.T. Biaxial deformation of a polymer network measured via deuteron quadrupolar interactions. Macromolecules 36 (2003) 724-735
    • (2003) Macromolecules , vol.36 , pp. 724-735
    • Callaghan, P.T.1    Samulski, E.T.2
  • 108
    • 0020204638 scopus 로고
    • Behavior of the spin-spin relaxation time for natural rubber vulcanizates under large deformation
    • Oikawa H., and Murakami K. Behavior of the spin-spin relaxation time for natural rubber vulcanizates under large deformation. Polymer 23 (1982) 1737-1741
    • (1982) Polymer , vol.23 , pp. 1737-1741
    • Oikawa, H.1    Murakami, K.2
  • 109
    • 0023967162 scopus 로고
    • Proton magnetic relaxation observation of weak gel stretching. Evidence for affine deformation
    • Cohen-Addad J.P., Huchot P., and Viallat A. Proton magnetic relaxation observation of weak gel stretching. Evidence for affine deformation. Polym. Bull. 19 (1988) 257-264
    • (1988) Polym. Bull. , vol.19 , pp. 257-264
    • Cohen-Addad, J.P.1    Huchot, P.2    Viallat, A.3
  • 110
    • 0026420843 scopus 로고
    • Vulcanized polybutadiene. Swelling and NMR observation of stretching
    • Cohen-Addad J.P., and Huchot P. Vulcanized polybutadiene. Swelling and NMR observation of stretching. Macromolecules 24 (1991) 6591-6599
    • (1991) Macromolecules , vol.24 , pp. 6591-6599
    • Cohen-Addad, J.P.1    Huchot, P.2
  • 111
    • 0035811346 scopus 로고    scopus 로고
    • NMR images of proton residual dipolar coupling from strained elastomers
    • Schneider M., Demco D.E., and Blümich B. NMR images of proton residual dipolar coupling from strained elastomers. Macromolecules 34 (2001) 4019-4026
    • (2001) Macromolecules , vol.34 , pp. 4019-4026
    • Schneider, M.1    Demco, D.E.2    Blümich, B.3
  • 115
    • 0033111008 scopus 로고    scopus 로고
    • 2H homonuclear and heteronuclear multiple-quantum-filtered NMR spectroscopy
    • 2H homonuclear and heteronuclear multiple-quantum-filtered NMR spectroscopy. J. Magn. Reson. 137 (1999) 295-310
    • (1999) J. Magn. Reson. , vol.137 , pp. 295-310
    • Eliav, U.1    Navon, G.2
  • 117
    • 0001805571 scopus 로고
    • The dipolar-correlation effect on the stimulated echo. Application to polymer melts
    • Kimmich R., Fischer E., Callaghan P., and Fatkullin N. The dipolar-correlation effect on the stimulated echo. Application to polymer melts. J. Magn. Reson. 117 (1995) 53-61
    • (1995) J. Magn. Reson. , vol.117 , pp. 53-61
    • Kimmich, R.1    Fischer, E.2    Callaghan, P.3    Fatkullin, N.4
  • 118
    • 0032474393 scopus 로고    scopus 로고
    • The molecular weight dependence of nuclear spin correlations in entangled polymeric liquids
    • Callaghan P.T., and Samulski E.T. The molecular weight dependence of nuclear spin correlations in entangled polymeric liquids. Macromolecules 31 (1998) 3693-3705
    • (1998) Macromolecules , vol.31 , pp. 3693-3705
    • Callaghan, P.T.1    Samulski, E.T.2
  • 119
    • 34248666586 scopus 로고    scopus 로고
    • R. Graf, Hochauflösende Doppelquanten-NMR-Spektroskopie an amorphen Polymeren, Dissertation, Universität Mainz, Shaker Verlag, Aachen, 1998.
  • 120
    • 0034830484 scopus 로고    scopus 로고
    • Local order and chain dynamics in molten polymer-blocks revealed by proton double-quantum NMR
    • Dollase T., Graf R., Heuer A., and Spiess H.W. Local order and chain dynamics in molten polymer-blocks revealed by proton double-quantum NMR. Macromolecules 34 (2001) 298-309
    • (2001) Macromolecules , vol.34 , pp. 298-309
    • Dollase, T.1    Graf, R.2    Heuer, A.3    Spiess, H.W.4
  • 121
    • 0037150305 scopus 로고    scopus 로고
    • Structure of a PDMS layer grafted onto a silica surface studied by means of DSC and solid-state NMR
    • Litvinov V.M., Barthel H., and Weis J. Structure of a PDMS layer grafted onto a silica surface studied by means of DSC and solid-state NMR. Macromolecules 35 (2002) 4356-4364
    • (2002) Macromolecules , vol.35 , pp. 4356-4364
    • Litvinov, V.M.1    Barthel, H.2    Weis, J.3
  • 123
    • 41349088122 scopus 로고    scopus 로고
    • Chain segment order in ultrathin polymer films: a deuterium NMR study
    • Primak S.V., Jin T., Dagger A.C., Finotello D., and Mann E.K. Chain segment order in ultrathin polymer films: a deuterium NMR study. Phys. Rev. E 65 (2002) 031804
    • (2002) Phys. Rev. E , vol.65 , pp. 031804
    • Primak, S.V.1    Jin, T.2    Dagger, A.C.3    Finotello, D.4    Mann, E.K.5
  • 126
    • 0026819697 scopus 로고
    • Polybutadiene. Kinetics of cross-link formation observed from pseudosolid NMR of protons
    • Cohen-Addad J.P., Soyez E., Viallat A., and Queslel J.P. Polybutadiene. Kinetics of cross-link formation observed from pseudosolid NMR of protons. Macromolecules 25 (1992) 1259-1266
    • (1992) Macromolecules , vol.25 , pp. 1259-1266
    • Cohen-Addad, J.P.1    Soyez, E.2    Viallat, A.3    Queslel, J.P.4
  • 127
    • 0000942937 scopus 로고    scopus 로고
    • Poly(dimethylsiloxane) chains cross-linked at random. Percolation and NMR approaches
    • Cohen-Addad J.P., and Montes H. Poly(dimethylsiloxane) chains cross-linked at random. Percolation and NMR approaches. Macromolecules 30 (1997) 3678-3684
    • (1997) Macromolecules , vol.30 , pp. 3678-3684
    • Cohen-Addad, J.P.1    Montes, H.2
  • 128
    • 0142041057 scopus 로고    scopus 로고
    • Characterization of chemical and physical networks in rubbery materials using proton NMR magnetization relaxation
    • Litvinov V.M., and De P.P. (Eds), Rapra Technology Ltd., Shawbury Ch. 10
    • Litvinov V.M. Characterization of chemical and physical networks in rubbery materials using proton NMR magnetization relaxation. In: Litvinov V.M., and De P.P. (Eds). Spectroscopy of Rubbers and Rubbery Materials (2002), Rapra Technology Ltd., Shawbury 353-400 Ch. 10
    • (2002) Spectroscopy of Rubbers and Rubbery Materials , pp. 353-400
    • Litvinov, V.M.1
  • 130
    • 33745793828 scopus 로고    scopus 로고
    • Spatial inhomogeneities of polystyrene gels prepared from semidilute solutions
    • Liu R.G., and Oppermann W. Spatial inhomogeneities of polystyrene gels prepared from semidilute solutions. Macromolecules 39 (2006) 4159-4167
    • (2006) Macromolecules , vol.39 , pp. 4159-4167
    • Liu, R.G.1    Oppermann, W.2
  • 131
    • 0034684893 scopus 로고    scopus 로고
    • Comparison of residual dipolar interactions in uncross-linked and cross-linked natural rubber by high-resolution solid-state NMR spectroscopy
    • Eulry V., Tekely P., Humbert F., Canet D., and Marcilloux J. Comparison of residual dipolar interactions in uncross-linked and cross-linked natural rubber by high-resolution solid-state NMR spectroscopy. Polymer 41 (2000) 3405-3410
    • (2000) Polymer , vol.41 , pp. 3405-3410
    • Eulry, V.1    Tekely, P.2    Humbert, F.3    Canet, D.4    Marcilloux, J.5
  • 133
    • 0035307855 scopus 로고    scopus 로고
    • 13C multiple-spin correlation in solid-state NMR: combining REDOR recoupling and multiple-quantum spectroscopy
    • 13C multiple-spin correlation in solid-state NMR: combining REDOR recoupling and multiple-quantum spectroscopy. J. Chem. Phys. 114 (2001) 5707-5728
    • (2001) J. Chem. Phys. , vol.114 , pp. 5707-5728
    • Saalwächter, K.1    Spiess, H.W.2
  • 134
    • 0000339577 scopus 로고
    • Pulsed nuclear resonance spectroscopy
    • Emshwiller M., Hahn E.L., and Kaplan D. Pulsed nuclear resonance spectroscopy. Phys. Rev. 118 (1960) 414-424
    • (1960) Phys. Rev. , vol.118 , pp. 414-424
    • Emshwiller, M.1    Hahn, E.L.2    Kaplan, D.3
  • 135
    • 45149145322 scopus 로고
    • Rotational-echo double-resonance NMR
    • Gullion T., and Schaefer J. Rotational-echo double-resonance NMR. J. Magn. Reson. 81 (1989) 196-200
    • (1989) J. Magn. Reson. , vol.81 , pp. 196-200
    • Gullion, T.1    Schaefer, J.2
  • 136
    • 0036004924 scopus 로고    scopus 로고
    • An investigation of poly(dimethylsiloxane) chain dynamics and order in its inclusion compound with γ-cyclodextrin by Fast-MAS solid-state NMR spectroscopy
    • Saalwächter K. An investigation of poly(dimethylsiloxane) chain dynamics and order in its inclusion compound with γ-cyclodextrin by Fast-MAS solid-state NMR spectroscopy. Macromol. Rapid. Commun. 23 (2002) 286-291
    • (2002) Macromol. Rapid. Commun. , vol.23 , pp. 286-291
    • Saalwächter, K.1
  • 137
    • 0036960265 scopus 로고    scopus 로고
    • The application of MAS recoupling methods in the intermediate motional regime
    • Saalwächter K., and Fischbach I. The application of MAS recoupling methods in the intermediate motional regime. J. Magn. Reson. 157 (2002) 17-30
    • (2002) J. Magn. Reson. , vol.157 , pp. 17-30
    • Saalwächter, K.1    Fischbach, I.2


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.