Validation of high-throughput measurement system with microwave-assisted extraction, fully automated sample preparation device, and gas chromatography-electron capture detector for determination of polychlorinated biphenyls in whale blubber

Chemosphere

Volumn 74, Issue 8, 2009, Pages 1069-1078

  Fujita, Hiroyuki ^a   Honda, Katsuhisa ^a   Hamada, Noriaki ^b   Yasunaga, Genta ^c   Fujise, Yoshihiro ^c  

^a EHIME UNIVERSITY   (Japan)

^b MIURA CO LTD   (Japan)

^c T   (Japan)

Author keywords

Gas chromatography electron capture detector; Microwave assisted extraction; Polychlorinated biphenyls; Sample preparation device; Whale blubber

Indexed keywords

ACCURACY TESTS; COD LIVER OIL; CONCENTRATED SOLUTIONS; CONCENTRATION OF; CONCENTRATION VALUES; CRUDE EXTRACTS; GAS CHROMATOGRAPHY-ELECTRON CAPTURE DETECTOR; HIGH-THROUGHPUT MEASUREMENTS; MARINE ECOSYSTEMS; MEASUREMENT SYSTEMS; MICROWAVE-ASSISTED EXTRACTION; MINKE WHALES; N HEXANES; PCB CONGENERS; QUANTIFICATION LIMITS; SAMPLE PREPARATION DEVICE; WHALE BLUBBER;

CHROMATOGRAPHIC ANALYSIS; CHROMATOGRAPHY; DETECTORS; ECOSYSTEMS; ELECTROCHEMICAL SENSORS; ELECTROCHROMIC DEVICES; ELECTRONS; ELECTROOPTICAL DEVICES; EXTRACTION; GASES; HEXANE; MICROWAVES; ORGANIC POLLUTANTS; POLYCHLORINATED BIPHENYLS; PRINTED CIRCUITS; PURIFICATION; REDUCTION; TOLUENE;

GAS CHROMATOGRAPHY;

COD LIVER OIL; HEXANE; POLYCHLORINATED BIPHENYL DERIVATIVE; TOLUENE;

AUTOMATION; CONCENTRATION (COMPOSITION); EXTRACTION METHOD; FAT RESERVE; GAS CHROMATOGRAPHY; MEASUREMENT METHOD; PCB; WHALE;

ACCURACY; ADIPOSE TISSUE; ANIMAL TISSUE; ARTICLE; CONTROLLED STUDY; ELECTRON CAPTURE DETECTION; EQUIPMENT DESIGN; EXTRACTION; GAS CHROMATOGRAPHY; LIQUID LIQUID EXTRACTION; MASS FRAGMENTOGRAPHY; MICROWAVE ASSISTED EXTRACTION; MINKE WHALE; MINKE WHALE BLUBBER; NONHUMAN; PURIFICATION; SAMPLING; SAPONIFICATION; VALIDATION PROCESS;

ADIPOCYTES; ANALYTIC SAMPLE PREPARATION METHODS; ANIMALS; CHROMATOGRAPHY, GAS; ELECTRONS; MASS SPECTROMETRY; MICROWAVES; PESTICIDE RESIDUES; POLYCHLORINATED BIPHENYLS; REFERENCE STANDARDS; SENSITIVITY AND SPECIFICITY; WHALES;

BALAENOPTERA ACUTOROSTRATA; CETACEA;

EID: 59249106612     PISSN: 00456535     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.chemosphere.2008.10.053     Document Type: Article

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